中空纤维液相微萃取-气相色谱/质谱联用检测水中的氯化苄
建立了一种以中空纤维液相微萃取（HF-LPME）前处理样品,利用气相色谱/质谱（GC/MS）对水中痕量氯化苄进行检测的方法。优化的实验条件为：3.0μL甲苯为萃取溶剂,在中等搅拌速率下室温萃取15 min。方法的线性范围为1~100μg/L,线性相关系数r=0.9995;检出限为0.5μg/L（S/N=3）;相对标准偏差为5.37%（n=5）。用于水库水和被污染河水的测定,加标回收率分别为95.7%和93.6%,结果满意。...
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| Published in | Fēnxī huàxué Vol. 36; no. 11; pp. 1559 - 1562 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | Chinese |
| Published |
山东省分析测试中心,济南,250014
2008
聊城大学化学化工学院,聊城,252059%山东省分析测试中心,济南,250014%聊城大学化学化工学院,聊城,252059 |
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| Online Access | Get full text |
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| Abstract | 建立了一种以中空纤维液相微萃取（HF-LPME）前处理样品,利用气相色谱/质谱（GC/MS）对水中痕量氯化苄进行检测的方法。优化的实验条件为：3.0μL甲苯为萃取溶剂,在中等搅拌速率下室温萃取15 min。方法的线性范围为1~100μg/L,线性相关系数r=0.9995;检出限为0.5μg/L（S/N=3）;相对标准偏差为5.37%（n=5）。用于水库水和被污染河水的测定,加标回收率分别为95.7%和93.6%,结果满意。 |
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| AbstractList | O6; 建立了一种以中空纤维液相微萃取(HF-LPME)前处理样品,利用气相色谱/质谱(GC/MS)对水中痕量氯化苄进行检测的方法.优化的实验条件为:3.0 μL甲苯为萃取溶剂,在中等搅拌速率下室温萃取15 min.方法的线性范围为1～100 μg/L,线性相关系数r=0.9995;检出限为0.5 μg/L(S/N=3);相对标准偏差为5.37%(n=5).用于水库水和被污染河水的测定,加标回收率分别为95.7%和93.6%,结果满意. 建立了一种以中空纤维液相微萃取（HF-LPME）前处理样品,利用气相色谱/质谱（GC/MS）对水中痕量氯化苄进行检测的方法。优化的实验条件为：3.0μL甲苯为萃取溶剂,在中等搅拌速率下室温萃取15 min。方法的线性范围为1~100μg/L,线性相关系数r=0.9995;检出限为0.5μg/L（S/N=3）;相对标准偏差为5.37%（n=5）。用于水库水和被污染河水的测定,加标回收率分别为95.7%和93.6%,结果满意。 |
| Author | 刁春鹏 苑金鹏 李磊 江婷 赵汝松 程传格 柳仁民 |
| AuthorAffiliation | 山东省分析测试中心,济南250014 聊城大学化学化工学院,聊城252059 |
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| Author_FL | YUAN Jin-Peng JIANG Ting DIAO Chun-Peng LIU Ren-Min LI Lei ZHAO Ru-Song CHENG Chuan-Ge |
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| DocumentTitleAlternate | Determination of Benzyl Chloride in Water by Hollow Fiber Liquid Phase Microextraction-Gas Chromatography-Mass Spectrometry |
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| Snippet | 建立了一种以中空纤维液相微萃取（HF-LPME）前处理样品,利用气相色谱/质谱（GC/MS）对水中痕量氯化苄进行检测的方法。优化的实验条件为：3.0μL甲苯为萃取溶剂,在中等搅拌速率下室温萃取15... O6; 建立了一种以中空纤维液相微萃取(HF-LPME)前处理样品,利用气相色谱/质谱(GC/MS)对水中痕量氯化苄进行检测的方法.优化的实验条件为:3.0 μL甲苯为萃取溶剂,在中等搅拌速率下室温萃取15 min.方法的线性范围为1～100 μg/L,线性相关系数r=0.9995;检出限为0.5... |
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| Title | 中空纤维液相微萃取-气相色谱/质谱联用检测水中的氯化苄 |
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