Carbon molecular sieve gas separation membranes based on an intrinsically microporous polyimide precursor
We report the physical characteristics and gas transport properties for a series of pyrolyzed membranes derived from an intrinsically microporous polyimide containing spiro-centers (PIM-6FDA-OH) by step-wise heat treatment to 440, 530, 600, 630 and 800°C, respectively. At 440°C, the PIM-6FDA-OH was...
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| Published in | Carbon (New York) Vol. 62; pp. 88 - 96 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
01.10.2013
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | We report the physical characteristics and gas transport properties for a series of pyrolyzed membranes derived from an intrinsically microporous polyimide containing spiro-centers (PIM-6FDA-OH) by step-wise heat treatment to 440, 530, 600, 630 and 800°C, respectively. At 440°C, the PIM-6FDA-OH was converted to a polybenzoxazole and exhibited a 3-fold increase in CO2 permeability (from 251 to 683 Barrer) with a 50% reduction in selectivity over CH4 (from 28 to 14). At 530°C, a distinct intermediate amorphous carbon structure with superior gas separation properties was formed. A 56% increase in CO2-probed surface area accompanied a 16-fold increase in CO2 permeability (4110Barrer) over the pristine polymer. The graphitic carbon membrane, obtained by heat treatment at 600°C, exhibited excellent gas separation properties, including a remarkable CO2 permeability of 5040Barrer with a high selectivity over CH4 of 38. Above 600°C, the strong emergence of ultramicroporosity (<7Å) as evidenced by WAXD and CO2 adsorption studies elicits a prominent molecular sieving effect, yielding gas separation performance well above the permeability-selectivity trade-off curves of polymeric membranes. |
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| AbstractList | We report the physical characteristics and gas transport properties for a series of pyrolyzed membranes derived from an intrinsically microporous polyimide containing spiro-centers (PIM-6FDA-OH) by step-wise heat treatment to 440, 530, 600, 630 and 800 degree C, respectively. At 440 degree C, the PIM-6FDA-OH was converted to a polybenzoxazole and exhibited a 3-fold increase in CO2 permeability (from 251 to 683 Barrer) with a 50% reduction in selectivity over CH4 (from 28 to 14). At 530 degree C, a distinct intermediate amorphous carbon structure with superior gas separation properties was formed. A 56% increase in CO2-probed surface area accompanied a 16-fold increase in CO2 permeability (4110 Barrer) over the pristine polymer. The graphitic carbon membrane, obtained by heat treatment at 600 degree C, exhibited excellent gas separation properties, including a remarkable CO2 permeability of 5040 Barrer with a high selectivity over CH4 of 38. Above 600 degree C, the strong emergence of ultramicroporosity (<7 A) as evidenced by WAXD and CO2 adsorption studies elicits a prominent molecular sieving effect, yielding gas separation performance well above the permeability-selectivity trade-off curves of polymeric membranes. We report the physical characteristics and gas transport properties for a series of pyrolyzed membranes derived from an intrinsically microporous polyimide containing spiro-centers (PIM-6FDA-OH) by step-wise heat treatment to 440, 530, 600, 630 and 800°C, respectively. At 440°C, the PIM-6FDA-OH was converted to a polybenzoxazole and exhibited a 3-fold increase in CO2 permeability (from 251 to 683 Barrer) with a 50% reduction in selectivity over CH4 (from 28 to 14). At 530°C, a distinct intermediate amorphous carbon structure with superior gas separation properties was formed. A 56% increase in CO2-probed surface area accompanied a 16-fold increase in CO2 permeability (4110Barrer) over the pristine polymer. The graphitic carbon membrane, obtained by heat treatment at 600°C, exhibited excellent gas separation properties, including a remarkable CO2 permeability of 5040Barrer with a high selectivity over CH4 of 38. Above 600°C, the strong emergence of ultramicroporosity (<7Å) as evidenced by WAXD and CO2 adsorption studies elicits a prominent molecular sieving effect, yielding gas separation performance well above the permeability-selectivity trade-off curves of polymeric membranes. We report the physical characteristics and gas transport properties for a series of pyrolyzed membranes derived from an intrinsically microporous polyimide containing spiro-centers (PIM-6FDA-OH) by step-wise heat treatment to 440, 530, 600, 630 and 800°C, respectively. At 440°C, the PIM-6FDA-OH was converted to a polybenzoxazole and exhibited a 3-fold increase in CO₂ permeability (from 251 to 683 Barrer) with a 50% reduction in selectivity over CH₄ (from 28 to 14). At 530°C, a distinct intermediate amorphous carbon structure with superior gas separation properties was formed. A 56% increase in CO₂-probed surface area accompanied a 16-fold increase in CO₂ permeability (4110Barrer) over the pristine polymer. The graphitic carbon membrane, obtained by heat treatment at 600°C, exhibited excellent gas separation properties, including a remarkable CO₂ permeability of 5040Barrer with a high selectivity over CH₄ of 38. Above 600°C, the strong emergence of ultramicroporosity (<7Å) as evidenced by WAXD and CO₂ adsorption studies elicits a prominent molecular sieving effect, yielding gas separation performance well above the permeability-selectivity trade-off curves of polymeric membranes. We report the physical characteristics and gas transport properties for a series of pyrolyzed membranes derived from an intrinsically microporous polyimide containing spiro-centers (PIM-6FDA-OH) by step-wise heat treatment to 440, 530, 600, 630 and 800 degree C, respectively. At 440 degree C, the PIM-6FDA-OH was converted to a polybenzoxazole and exhibited a 3-fold increase in CO sub(2) permeability (from 251 to 683 Barrer) with a 50% reduction in selectivity over CH sub(4) (from 28 to 14). At 530 degree C, a distinct intermediate amorphous carbon structure with superior gas separation properties was formed. A 56% increase in CO sub(2)-probed surface area accompanied a 16-fold increase in CO sub(2) permeability (4110 Barrer) over the pristine polymer. The graphitic carbon membrane, obtained by heat treatment at 600 degree C, exhibited excellent gas separation properties, including a remarkable CO sub(2) permeability of 5040 Barrer with a high selectivity over CH sub(4) of 38. Above 600 degree C, the strong emergence of ultramicroporosity (< 7 AA) as evidenced by WAXD and CO sub(2) adsorption studies elicits a prominent molecular sieving effect, yielding gas separation performance well above the permeability-selectivity trade-off curves of polymeric membranes. |
| Author | Swaidan, Raja Tan, Hua Teng, Baiyang Pinnau, Ingo Han, Yu Litwiller, Eric Salinas, Octavio Ma, Xiaohua |
| Author_xml | – sequence: 1 givenname: Xiaohua surname: Ma fullname: Ma, Xiaohua – sequence: 2 givenname: Raja surname: Swaidan fullname: Swaidan, Raja – sequence: 3 givenname: Baiyang surname: Teng fullname: Teng, Baiyang – sequence: 4 givenname: Hua surname: Tan fullname: Tan, Hua – sequence: 5 givenname: Octavio surname: Salinas fullname: Salinas, Octavio – sequence: 6 givenname: Eric surname: Litwiller fullname: Litwiller, Eric – sequence: 7 givenname: Yu surname: Han fullname: Han, Yu – sequence: 8 givenname: Ingo surname: Pinnau fullname: Pinnau, Ingo email: ingo.pinnau@kaust.edu.sa |
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| Keywords | Methane Membranes Transport properties Separation Porous materials Carbon dioxide Selectivity Molecular gas Permeability Molecular sieves Carbon Precursor Heat treatments Chemical reduction Microporosity Polyimides Transport processes Surface area Polymers Amorphous state structure Inorganic membrane |
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| SubjectTerms | adsorption Amorphous semiconductors, metals, and alloys Carbon Carbon dioxide Chemistry Colloidal state and disperse state Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Disordered solids Exact sciences and technology Fullerenes and related materials; diamonds, graphite Gas separation General and physical chemistry Heat treatment Materials science Membranes methane Permeability Physics Polyimide resins polymers Porous materials Selectivity Specific materials Structure of solids and liquids; crystallography surface area |
| Title | Carbon molecular sieve gas separation membranes based on an intrinsically microporous polyimide precursor |
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