An efficient catalytic degradation of trichloroethene in a percarbonate system catalyzed by ultra-fine heterogeneous zeolite supported zero valent iron-nickel bimetallic composite
[Display omitted] •A novel ultra-fine natural zeolite supported Fe-Ni composite was synthesized.•The catalytic ability and stability of Z-nZVI-Ni increased significantly.•Z-nZVI-Ni demonstrated remarkable performance for TCE degradation.•The hydroxyl radicals (OH) played the dominant role in TCE deg...
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| Published in | Applied catalysis. A, General Vol. 531; pp. 177 - 186 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Netherlands
Elsevier B.V
05.02.2017
Elsevier Science SA |
| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•A novel ultra-fine natural zeolite supported Fe-Ni composite was synthesized.•The catalytic ability and stability of Z-nZVI-Ni increased significantly.•Z-nZVI-Ni demonstrated remarkable performance for TCE degradation.•The hydroxyl radicals (OH) played the dominant role in TCE degradation.•The slow leaching of Fe and Ni presented its extended stability.
Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH). The quantification of OH elucidated by using p-chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH. The transformation products were identified using GC–MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. |
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| AbstractList | Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH
•
). The quantification of OH
•
elucidated by using
p-
chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH
•
. The transformation products were identified using GC-MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH center dot). The quantification of OH center dot elucidated by using p-chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH center dot. The transformation products were identified using GC-MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. (C) 2016 Elsevier B.V. All rights reserved. Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH<img src="http://cdn.els-cdn.com/sd/entities/rad" data-inlimg="/entities/rad" data-loaded="true" />). The quantification of OH<img src="http://cdn.els-cdn.com/sd/entities/rad" data-inlimg="/entities/rad" data-loaded="true" />elucidated by using p- chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH<img src="http://cdn.els-cdn.com/sd/entities/rad" data-inlimg="/entities/rad" data-loaded="true" />. The transformation products were identified using GC–MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH). The quantification of OH elucidated by using p-chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH. The transformation products were identified using GC-MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH ). The quantification of OH elucidated by using chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH . The transformation products were identified using GC-MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH•). The quantification of OH• elucidated by using p-chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH•. The transformation products were identified using GC-MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation.Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH•). The quantification of OH• elucidated by using p-chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH•. The transformation products were identified using GC-MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. [Display omitted] •A novel ultra-fine natural zeolite supported Fe-Ni composite was synthesized.•The catalytic ability and stability of Z-nZVI-Ni increased significantly.•Z-nZVI-Ni demonstrated remarkable performance for TCE degradation.•The hydroxyl radicals (OH) played the dominant role in TCE degradation.•The slow leaching of Fe and Ni presented its extended stability. Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies and physico-chemical properties of the Z-nZVI-Ni composite were determined using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Energy dispersive X-ray spectra (EDS), Brunauer Emmett Teller (BET) adsorption, wide angle X-ray diffractometry (WA-XRD), and Fourier transform infrared spectroscopy (FTIR). The results indicated high dispersion of iron and nickel nano particles on the zeolite sheet with an enhanced surface area. Complete destruction of trichloroethene (TCE) and efficient removal of total organic carbon (TOC) were observed by using Z-nZVI-Ni as a heterogeneous catalyst for a Fenton-like oxidation process employing sodium percarbonate (SPC) as an oxidant. The electron spin resonance (ESR) of Z-nZVI-Ni verified the generation and intensity of hydroxyl radicals (OH). The quantification of OH elucidated by using p-chlorobenzoic acid, a probe indicator, confirmed the higher intensity of OH. The transformation products were identified using GC–MS. The slow iron and nickel leaching offered higher stability and better catalytic activity of Z-nZVI-Ni, demonstrating its prospective long term applications in groundwater for TCE degradation. |
| Author | Danish, Muhammad Miao, Zhouwei Gu, Xiaogang Brusseau, Mark L. Naqvi, Muhammad Zaman, Waqas Qamar Lu, Shuguang Ahmad, Ayyaz Farooq, Usman Fu, Xiaori |
| AuthorAffiliation | c Department of Chemical Engineering, Muhammad Nawaz Sharif University of Engineering and Technology, Multan, Pakistan d Department of Energy, Building and Environment, Mälardalen University, Västerås 72123, Sweden b Soil, Water and Environmental Science Department, School of Earth and Environmental Sciences, The University of Arizona, 429 Shantz Bldg., Tucson, AZ 85721, United States a State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China |
| AuthorAffiliation_xml | – name: d Department of Energy, Building and Environment, Mälardalen University, Västerås 72123, Sweden – name: a State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – name: b Soil, Water and Environmental Science Department, School of Earth and Environmental Sciences, The University of Arizona, 429 Shantz Bldg., Tucson, AZ 85721, United States – name: c Department of Chemical Engineering, Muhammad Nawaz Sharif University of Engineering and Technology, Multan, Pakistan |
| Author_xml | – sequence: 1 givenname: Muhammad surname: Danish fullname: Danish, Muhammad organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – sequence: 2 givenname: Xiaogang surname: Gu fullname: Gu, Xiaogang organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – sequence: 3 givenname: Shuguang surname: Lu fullname: Lu, Shuguang email: lvshuguang@ecust.edu.cn organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – sequence: 4 givenname: Mark L. surname: Brusseau fullname: Brusseau, Mark L. organization: Soil, Water and Environmental Science Department, School of Earth and Environmental Sciences, The University of Arizona, 429 Shantz Bldg., Tucson, AZ 85721, United States – sequence: 5 givenname: Ayyaz surname: Ahmad fullname: Ahmad, Ayyaz organization: Department of Chemical Engineering, Muhammad Nawaz Sharif University of Engineering and Technology, Multan, Pakistan – sequence: 6 givenname: Muhammad surname: Naqvi fullname: Naqvi, Muhammad organization: Department of Energy, Building and Environment, Mälardalen University, Västerås 72123, Sweden – sequence: 7 givenname: Usman surname: Farooq fullname: Farooq, Usman organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – sequence: 8 givenname: Waqas Qamar surname: Zaman fullname: Zaman, Waqas Qamar organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – sequence: 9 givenname: Xiaori surname: Fu fullname: Fu, Xiaori organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China – sequence: 10 givenname: Zhouwei surname: Miao fullname: Miao, Zhouwei organization: State Environmental Protection Key Laboratory of Environmental Risk Assessment and Control on Chemical Process, East China University of Science and Technology, Shanghai 200237, China |
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| Keywords | Groundwater remediation Heterogeneous Fenton catalyst Trichloroethene (TCE) Sodium percarbonate (SPC) Z-nZVI-Ni groundwater remediation sodium percarbonate (SPC) heterogeneous Fenton catalyst |
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| Publisher | Elsevier B.V Elsevier Science SA |
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•A novel ultra-fine natural zeolite supported Fe-Ni composite was synthesized.•The catalytic ability and stability of Z-nZVI-Ni increased... Zeolite supported nano iron-nickel bimetallic composite (Z-nZVI-Ni) was prepared using a liquid-phase reduction process. The corresponding surface morphologies... |
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| SubjectTerms | Bimetals Catalysis Catalytic activity Chemical Engineering Chemical properties Degradation Electron microscopy Electron paramagnetic resonance Electron spin Energy transmission Fourier transforms Groundwater Groundwater remediation Heterogeneous Fenton catalyst Hydroxyl radicals Iron Kemiteknik Leaching Morphology Nickel Organic carbon Oxidation Scanning electron microscopy Sodium percarbonate (SPC) Spectrum analysis Spin resonance Studies Transmission electron microscopy Trichloroethene (TCE) X ray spectra Z-nZVI-Ni Zeolites |
| Title | An efficient catalytic degradation of trichloroethene in a percarbonate system catalyzed by ultra-fine heterogeneous zeolite supported zero valent iron-nickel bimetallic composite |
| URI | https://dx.doi.org/10.1016/j.apcata.2016.11.001 https://www.ncbi.nlm.nih.gov/pubmed/29104369 https://www.proquest.com/docview/2022103485 https://www.proquest.com/docview/1961034621 https://pubmed.ncbi.nlm.nih.gov/PMC5665389 https://urn.kb.se/resolve?urn=urn:nbn:se:kau:diva-74908 https://urn.kb.se/resolve?urn=urn:nbn:se:mdh:diva-33534 |
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