A Facile Synthetic Route to a New SHG Material with Two Types of Parallel π-Conjugated Planar Triangular Units
A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π‐conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO3)2 and Mg(BO2)2⋅H2O as starting materials. Its structure contains honeycomb [Pb2(BO3)]∞ layers with noncoordination [NO3]− ani...
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| Published in | Angewandte Chemie International Edition Vol. 54; no. 12; pp. 3679 - 3682 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
16.03.2015
WILEY‐VCH Verlag |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π‐conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO3)2 and Mg(BO2)2⋅H2O as starting materials. Its structure contains honeycomb [Pb2(BO3)]∞ layers with noncoordination [NO3]− anions located at the interlayer space. Pb2(BO3)(NO3) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase‐matchable. The large SHG coefficient of Pb2(BO3)(NO3) arises from the synergistic effect of the stereoactive lone pairs on Pb2+ cations and parallel alignment of π‐conjugated BO3 and NO3 units. Based on its unique properties, Pb2(BO3)(NO3) may have great potential as a high performance NLO material in photonic applications.
Pb2(BO3)(NO3) is a new second‐harmonic generation (SHG) material that contains parallel π‐conjugated nitrate and borate anions. It was obtained through a facile hydrothermal reaction, shows a remarkable strong SHG response of about 9.0 times that of potassium dihydrogen phosphate (KDP), and is phase‐matchable. |
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| AbstractList | A new SHG material, namely, Pb sub(2)(BO sub(3))(NO sub(3)), which contains parallel pi -conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO sub(3)) sub(2) and Mg(BO sub(2)) sub(2)H sub(2 )O as starting materials. Its structure contains honeycomb [Pb sub(2)(BO sub(3))] sub( [infin]) layers with noncoordination [NO sub(3)] super(-) anions located at the interlayer space. Pb sub(2)(BO sub(3))(NO sub(3)) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase-matchable. The large SHG coefficient of Pb sub(2)(BO sub(3))(NO sub(3)) arises from the synergistic effect of the stereoactive lone pairs on Pb super(2+) cations and parallel alignment of pi -conjugated BO sub(3) and NO sub(3) units. Based on its unique properties, Pb sub(2)(BO sub(3))(NO sub(3)) may have great potential as a high performance NLO material in photonic applications. Pb sub(2)(BO sub(3))(NO sub(3)) is a new second-harmonic generation (SHG) material that contains parallel pi -conjugated nitrate and borate anions. It was obtained through a facile hydrothermal reaction, shows a remarkable strong SHG response of about 9.0 times that of potassium dihydrogen phosphate (KDP), and is phase-matchable. A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π‐conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO3)2 and Mg(BO2)2⋅H2O as starting materials. Its structure contains honeycomb [Pb2(BO3)]∞ layers with noncoordination [NO3]− anions located at the interlayer space. Pb2(BO3)(NO3) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase‐matchable. The large SHG coefficient of Pb2(BO3)(NO3) arises from the synergistic effect of the stereoactive lone pairs on Pb2+ cations and parallel alignment of π‐conjugated BO3 and NO3 units. Based on its unique properties, Pb2(BO3)(NO3) may have great potential as a high performance NLO material in photonic applications. Pb2(BO3)(NO3) is a new second‐harmonic generation (SHG) material that contains parallel π‐conjugated nitrate and borate anions. It was obtained through a facile hydrothermal reaction, shows a remarkable strong SHG response of about 9.0 times that of potassium dihydrogen phosphate (KDP), and is phase‐matchable. A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π-conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO3)2 and Mg(BO2)2⋅H2O as starting materials. Its structure contains honeycomb [Pb2(BO3)]∞ layers with noncoordination [NO3](-) anions located at the interlayer space. Pb2(BO3)(NO3) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase-matchable. The large SHG coefficient of Pb2(BO3)(NO3) arises from the synergistic effect of the stereoactive lone pairs on Pb(2+) cations and parallel alignment of π-conjugated BO3 and NO3 units. Based on its unique properties, Pb2(BO3)(NO3) may have great potential as a high performance NLO material in photonic applications.A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π-conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO3)2 and Mg(BO2)2⋅H2O as starting materials. Its structure contains honeycomb [Pb2(BO3)]∞ layers with noncoordination [NO3](-) anions located at the interlayer space. Pb2(BO3)(NO3) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase-matchable. The large SHG coefficient of Pb2(BO3)(NO3) arises from the synergistic effect of the stereoactive lone pairs on Pb(2+) cations and parallel alignment of π-conjugated BO3 and NO3 units. Based on its unique properties, Pb2(BO3)(NO3) may have great potential as a high performance NLO material in photonic applications. A new SHG material, namely, Pb 2 (BO 3 )(NO 3 ), which contains parallel π‐conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO 3 ) 2 and Mg(BO 2 ) 2 ⋅H 2 O as starting materials. Its structure contains honeycomb [Pb 2 (BO 3 )] ∞ layers with noncoordination [NO 3 ] − anions located at the interlayer space. Pb 2 (BO 3 )(NO 3 ) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase‐matchable. The large SHG coefficient of Pb 2 (BO 3 )(NO 3 ) arises from the synergistic effect of the stereoactive lone pairs on Pb 2+ cations and parallel alignment of π‐conjugated BO 3 and NO 3 units. Based on its unique properties, Pb 2 (BO 3 )(NO 3 ) may have great potential as a high performance NLO material in photonic applications. A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π-conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction by using Pb(NO3)2 and Mg(BO2)2⋅H2O as starting materials. Its structure contains honeycomb [Pb2(BO3)]∞ layers with noncoordination [NO3](-) anions located at the interlayer space. Pb2(BO3)(NO3) shows a remarkable strong SHG response of approximately 9.0 times that of potassium dihydrogen phosphate (KDP) and the material is also phase-matchable. The large SHG coefficient of Pb2(BO3)(NO3) arises from the synergistic effect of the stereoactive lone pairs on Pb(2+) cations and parallel alignment of π-conjugated BO3 and NO3 units. Based on its unique properties, Pb2(BO3)(NO3) may have great potential as a high performance NLO material in photonic applications. |
| Author | Mao, Jiang-Gao Song, Jun-Ling Kong, Fang Hu, Chun-Li Xu, Xiang |
| Author_xml | – sequence: 1 givenname: Jun-Ling surname: Song fullname: Song, Jun-Ling organization: State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002 (P. R. China) http://mjg.fjirsm.ac.cn/ – sequence: 2 givenname: Chun-Li surname: Hu fullname: Hu, Chun-Li organization: State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002 (P. R. China) http://mjg.fjirsm.ac.cn/ – sequence: 3 givenname: Xiang surname: Xu fullname: Xu, Xiang organization: State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002 (P. R. China) http://mjg.fjirsm.ac.cn/ – sequence: 4 givenname: Fang surname: Kong fullname: Kong, Fang organization: State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002 (P. R. China) http://mjg.fjirsm.ac.cn/ – sequence: 5 givenname: Jiang-Gao surname: Mao fullname: Mao, Jiang-Gao email: mjg@fjirsm.ac.cn organization: State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002 (P. R. China) http://mjg.fjirsm.ac.cn/ |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/25630286$$D View this record in MEDLINE/PubMed |
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| ContentType | Journal Article |
| Copyright | 2015 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim. |
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| Issue | 12 |
| Keywords | density functional calculations second-harmonic generation hydrothermal synthesis lone-pair cations |
| Language | English |
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| Notes | ArticleID:ANIE201412344 We thank the National Natural Science Foundation of China (grant numbers 2123006, 21403232, 2137222 , and 21203197) for financial support. SHG=second-harmonic generation. National Natural Science Foundation of China - No. 2123006; No. 21403232; No. 2137222; No. 21203197 istex:D3D7FEA0FED294B03E2CACE289BF36D275F12320 ark:/67375/WNG-GGSBZ6LN-7 We thank the National Natural Science Foundation of China (grant numbers 2123006, 21403232, 2137222 , and 21203197) for financial support. SHG=second‐harmonic generation. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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| PublicationDate | March 16, 2015 |
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| SSID | ssj0028806 |
| Score | 2.5824456 |
| Snippet | A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π‐conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction... A new SHG material, namely, Pb 2 (BO 3 )(NO 3 ), which contains parallel π‐conjugated nitrate and borate anions, was obtained through a facile hydrothermal... A new SHG material, namely, Pb2(BO3)(NO3), which contains parallel π-conjugated nitrate and borate anions, was obtained through a facile hydrothermal reaction... A new SHG material, namely, Pb sub(2)(BO sub(3))(NO sub(3)), which contains parallel pi -conjugated nitrate and borate anions, was obtained through a facile... |
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| SourceType | Aggregation Database Index Database Enrichment Source Publisher |
| StartPage | 3679 |
| SubjectTerms | Anions Borates density functional calculations Honeycomb Hydrothermal reactions hydrothermal synthesis Interlayers lone-pair cations Nitrates Phosphates Potassium second-harmonic generation |
| Title | A Facile Synthetic Route to a New SHG Material with Two Types of Parallel π-Conjugated Planar Triangular Units |
| URI | https://api.istex.fr/ark:/67375/WNG-GGSBZ6LN-7/fulltext.pdf https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fanie.201412344 https://www.ncbi.nlm.nih.gov/pubmed/25630286 https://www.proquest.com/docview/1662639195 https://www.proquest.com/docview/1701100266 |
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