Thermal- and Photo-Induced Phase-Transition Behaviors of a Tapered Dendritic Liquid Crystal with Photochromic Azobenzene Mesogens and a Bicyclic Chiral Center

A ribbon‐shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optic...

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Published inChemistry : a European journal Vol. 20; no. 19; pp. 5689 - 5695
Main Authors Kim, Dae-Yoon, Lee, Sang-A, Choi, Yu-Jin, Hwang, Seok-Ho, Kuo, Shiao-Wei, Nah, Changwoon, Lee, Myong-Hoon, Jeong, Kwang-Un
Format Journal Article
LanguageEnglish
Published Weinheim WILEY-VCH Verlag 05.05.2014
WILEY‐VCH Verlag
Wiley
Wiley Subscription Services, Inc
Subjects
Azo Compounds - chemistry
Bridged Bicyclo Compounds, Heterocyclic - chemistry
Calorimetry, Differential Scanning
Chemistry
Chemistry, Multidisciplinary
chirality
dendrimers
Dendrimers - chemistry
Differential scanning calorimetry
Helical
Isomerization
Isosorbide - chemistry
Liquid crystals
Liquid Crystals - chemistry
Models, Molecular
Phase Transition
Phase transitions
Photochemical
photochromism
Physical Sciences
Science & Technology
Solubility
Stereoisomerism
Superstructures
Tuning
phase transitions
liquid crystals
chirality
dendrimers
photochromism
UNITS
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Abstract A ribbon‐shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure‐sensitive diffraction techniques. Based on the experimental results, it was found that the AZ3DLC molecule exhibited the low‐ordered chiral smectic (Sm*) LC phase with 6.31 nm periodicity at a high‐temperature phase region. AZ3DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral‐inducing agent, it exhibited a good solubility, a high helical‐twisting power, and a large change in the helical‐twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly “remote‐control” the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures. Remote‐controlled color: A ribbon‐shaped chiral dendritic liquid crystal was newly synthesized, and its thermal and photo‐induced phase behaviors were investigated with the combined techniques of the thermal, microscopic, and scattering methods (see figure).
AbstractList A ribbon‐shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure‐sensitive diffraction techniques. Based on the experimental results, it was found that the AZ3DLC molecule exhibited the low‐ordered chiral smectic (Sm*) LC phase with 6.31 nm periodicity at a high‐temperature phase region. AZ3DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral‐inducing agent, it exhibited a good solubility, a high helical‐twisting power, and a large change in the helical‐twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly “remote‐control” the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures. Remote‐controlled color: A ribbon‐shaped chiral dendritic liquid crystal was newly synthesized, and its thermal and photo‐induced phase behaviors were investigated with the combined techniques of the thermal, microscopic, and scattering methods (see figure).
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure-sensitive diffraction techniques. Based on the experimental results, it was found that the AZ3DLC molecule exhibited the low-ordered chiral smectic (Sm*) LC phase with 6.31nm periodicity at a high-temperature phase region. AZ3DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral-inducing agent, it exhibited a good solubility, a high helical-twisting power, and a large change in the helical-twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly "remote-control" the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures. [PUBLICATION ABSTRACT]
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ(3)DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure-sensitive diffraction techniques. Based on the experimental results, it was found that the AZ(3)DLC molecule exhibited the low-ordered chiral smectic (Sm*) LC phase with 6.31nm periodicity at a high-temperature phase region. AZ(3)DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral-inducing agent, it exhibited a good solubility, a high helical-twisting power, and a large change in the helical-twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly remote-control the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures.
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ sub(3)DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure-sensitive diffraction techniques. Based on the experimental results, it was found that the AZ sub(3)DLC molecule exhibited the low-ordered chiral smectic (Sm*) LC phase with 6.31nm periodicity at a high-temperature phase region. AZ sub(3)DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral-inducing agent, it exhibited a good solubility, a high helical-twisting power, and a large change in the helical-twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly "remote-control" the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures. Remote-controlled color: A ribbon-shaped chiral dendritic liquid crystal was newly synthesized, and its thermal and photo-induced phase behaviors were investigated with the combined techniques of the thermal, microscopic, and scattering methods (see figure).
Abstract A ribbon‐shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ 3 DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure‐sensitive diffraction techniques. Based on the experimental results, it was found that the AZ 3 DLC molecule exhibited the low‐ordered chiral smectic (Sm*) LC phase with 6.31 nm periodicity at a high‐temperature phase region. AZ 3 DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral‐inducing agent, it exhibited a good solubility, a high helical‐twisting power, and a large change in the helical‐twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly “remote‐control” the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures.
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3 DLC) was successfully synthesized and its major phase transitions were studied by using differential scanning calorimetry (DSC) and linear polarized optical microscopy (POM). Its ordered structures at different temperatures were further identified through structure-sensitive diffraction techniques. Based on the experimental results, it was found that the AZ3 DLC molecule exhibited the low-ordered chiral smectic (Sm*) LC phase with 6.31 nm periodicity at a high-temperature phase region. AZ3 DLC showed the reversible photoisomerization in both organic solvents and nematic (N) LC media. As a chiral-inducing agent, it exhibited a good solubility, a high helical-twisting power, and a large change in the helical-twisting power due to its photochemical isomerization in the commercially available N LC hosts. Therefore, we were able to reversibly "remote-control" the colors in the whole visible region by finely tuning the helical pitch of the spontaneously formed helical superstructures.
Author Choi, Yu-Jin
Lee, Myong-Hoon
Kuo, Shiao-Wei
Hwang, Seok-Ho
Kim, Dae-Yoon
Nah, Changwoon
Lee, Sang-A
Jeong, Kwang-Un
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  organization: Department of Polymer Nanoscience and Technology, Department of Flexible and Printable Electronics, Chonbuk National University, Jeongju 561-756 (Korea), Fax: (+82) 63-270-2341
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  organization: Department of Materials Science and Optoelectronic Engineering, National Sun Yat-Sen University, Kaohsiung 804 (Taiwan)
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  givenname: Changwoon
  surname: Nah
  fullname: Nah, Changwoon
  organization: Department of Polymer Nanoscience and Technology, Department of Flexible and Printable Electronics, Chonbuk National University, Jeongju 561-756 (Korea), Fax: (+82) 63-270-2341
– sequence: 7
  givenname: Myong-Hoon
  surname: Lee
  fullname: Lee, Myong-Hoon
  organization: Department of Polymer Nanoscience and Technology, Department of Flexible and Printable Electronics, Chonbuk National University, Jeongju 561-756 (Korea), Fax: (+82) 63-270-2341
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  givenname: Kwang-Un
  surname: Jeong
  fullname: Jeong, Kwang-Un
  email: kujeong@jbnu.ac.kr
  organization: Department of Polymer Nanoscience and Technology, Department of Flexible and Printable Electronics, Chonbuk National University, Jeongju 561-756 (Korea), Fax: (+82) 63-270-2341
BackLink https://www.ncbi.nlm.nih.gov/pubmed/24665056$$D View this record in MEDLINE/PubMed
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Issue 19
Keywords phase transitions
liquid crystals
chirality
dendrimers
photochromism
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PublicationDateYYYYMMDD 2014-05-05
PublicationDate_xml – month: 05
  year: 2014
  text: May 5, 2014
  day: 05
PublicationDecade 2010
PublicationPlace Weinheim
PublicationPlace_xml – name: Weinheim
– name: WEINHEIM
– name: Germany
PublicationSubtitle A European Journal
PublicationTitle Chemistry : a European journal
PublicationTitleAbbrev CHEM-EUR J
PublicationTitleAlternate Chem. Eur. J
PublicationYear 2014
Publisher WILEY-VCH Verlag
WILEY‐VCH Verlag
Wiley
Wiley Subscription Services, Inc
Publisher_xml – name: WILEY-VCH Verlag
– name: WILEY‐VCH Verlag
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Snippet A ribbon‐shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3DLC) was...
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ(3)DLC) was...
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3 DLC) was...
Abstract A ribbon‐shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ 3...
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ3DLC) was...
A ribbon-shaped chiral liquid crystalline (LC) dendrimer with photochromic azobenzene mesogens and an isosorbide chiral center (abbreviated as AZ sub(3)DLC)...
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SubjectTerms Azo Compounds - chemistry
Bridged Bicyclo Compounds, Heterocyclic - chemistry
Calorimetry, Differential Scanning
Chemistry
Chemistry, Multidisciplinary
chirality
dendrimers
Dendrimers - chemistry
Differential scanning calorimetry
Helical
Isomerization
Isosorbide - chemistry
Liquid crystals
Liquid Crystals - chemistry
Models, Molecular
Phase Transition
Phase transitions
Photochemical
photochromism
Physical Sciences
Science & Technology
Solubility
Stereoisomerism
Superstructures
Tuning
Title Thermal- and Photo-Induced Phase-Transition Behaviors of a Tapered Dendritic Liquid Crystal with Photochromic Azobenzene Mesogens and a Bicyclic Chiral Center
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