Graphene-Supported Ultrafine Metal Nanoparticles Encapsulated by Mesoporous Silica: Robust Catalysts for Oxidation and Reduction Reactions
Graphene nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high‐temperature stability. The catalysts can be recycled and reused in many gas‐ and solution‐phase reactions,...
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| Published in | Angewandte Chemie International Edition Vol. 53; no. 1; pp. 250 - 254 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
03.01.2014
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Graphene nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high‐temperature stability. The catalysts can be recycled and reused in many gas‐ and solution‐phase reactions, and their high catalytic activity can be fully recovered by high‐temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions.
Layer cake: The synthesis of graphene‐nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous silica layers is reported. The resulting class of robust catalysts was shown to possess high activity, good stability under high temperature conditions, and excellent recyclability and reusability in both gas‐ and solution‐phase reactions. |
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| AbstractList | Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high-temperature stability. The catalysts can be recycled and reused in many gas- and solution-phase reactions, and their high catalytic activity can be fully recovered by high-temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions. [PUBLICATION ABSTRACT] Graphene nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high‐temperature stability. The catalysts can be recycled and reused in many gas‐ and solution‐phase reactions, and their high catalytic activity can be fully recovered by high‐temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions. Layer cake: The synthesis of graphene‐nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous silica layers is reported. The resulting class of robust catalysts was shown to possess high activity, good stability under high temperature conditions, and excellent recyclability and reusability in both gas‐ and solution‐phase reactions. Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high-temperature stability. The catalysts can be recycled and reused in many gas- and solution-phase reactions, and their high catalytic activity can be fully recovered by high-temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions. Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high-temperature stability. The catalysts can be recycled and reused in many gas- and solution-phase reactions, and their high catalytic activity can be fully recovered by high-temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions.Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high-temperature stability. The catalysts can be recycled and reused in many gas- and solution-phase reactions, and their high catalytic activity can be fully recovered by high-temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions. Graphene nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO 2 layers were prepared and used as robust catalysts with high catalytic activity and excellent high‐temperature stability. The catalysts can be recycled and reused in many gas‐ and solution‐phase reactions, and their high catalytic activity can be fully recovered by high‐temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO 2 layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions. Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO sub(2) layers were prepared and used as robust catalysts with high catalytic activity and excellent high-temperature stability. The catalysts can be recycled and reused in many gas- and solution-phase reactions, and their high catalytic activity can be fully recovered by high-temperature regeneration, should they be deactivated by feedstock poisoning. In addition to the large surface area provided by the graphene support, the enhanced catalytic performance is also attributed to the mesoporous SiO sub(2) layers, which not only stabilize the ultrafine metal nanoparticles, but also prevent the aggregation of the graphene nanosheets. The synthetic strategy can be extended to other metals, such as Pd and Ru, for preparing robust catalysts for various reactions. Layer cake: The synthesis of graphene-nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous silica layers is reported. The resulting class of robust catalysts was shown to possess high activity, good stability under high temperature conditions, and excellent recyclability and reusability in both gas- and solution-phase reactions. |
| Author | Zhang, Donghui Zhang, Tierui Yin, Yadong Shang, Lu Bian, Tong Wu, Li-Zhu Tung, Chen-Ho Zhang, Baihui |
| Author_xml | – sequence: 1 givenname: Lu surname: Shang fullname: Shang, Lu organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) – sequence: 2 givenname: Tong surname: Bian fullname: Bian, Tong organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) – sequence: 3 givenname: Baihui surname: Zhang fullname: Zhang, Baihui organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) – sequence: 4 givenname: Donghui surname: Zhang fullname: Zhang, Donghui organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) – sequence: 5 givenname: Li-Zhu surname: Wu fullname: Wu, Li-Zhu organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) – sequence: 6 givenname: Chen-Ho surname: Tung fullname: Tung, Chen-Ho organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) – sequence: 7 givenname: Yadong surname: Yin fullname: Yin, Yadong email: yadong.yin@ucr.edu organization: Department of Chemistry, University of California, Riverside, CA 92521 (USA) – sequence: 8 givenname: Tierui surname: Zhang fullname: Zhang, Tierui email: tierui@mail.ipc.ac.cn organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190 (P. R. China) |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/24288240$$D View this record in MEDLINE/PubMed |
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| CODEN | ACIEAY |
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| Keywords | heterogeneous catalysis metal nanoparticles mesoporous materials graphene stability |
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| Notes | ArticleID:ANIE201306863 istex:04C07F3E496372ADE56BB7EF01DB8ED128990A27 100 Talents Program of the Chinese Academy of Sciences We acknowledge support from the Ministry of Science and Technology of China (2014CB239402, 2013CB834505), the National Natural Science Foundation of China (51322213, 20901081, 51172245, 91127005, 21201172), the Knowledge Innovation Project of the Chinese Academy of Sciences (KGCX2-EW-311-3), and the 100 Talents Program of the Chinese Academy of Sciences. Y.Y. also thanks the U.S. Department of Energy (DE-FG02-09ER16096) for financial support. Knowledge Innovation Project of the Chinese Academy of Sciences - No. KGCX2-EW-311-3 National Natural Science Foundation of China - No. 51322213; No. 20901081; No. 51172245; No. 91127005; No. 21201172 U.S. Department of Energy - No. DE-FG02-09ER16096 ark:/67375/WNG-GJCTCQ8B-G Ministry of Science and Technology of China - No. 2014CB239402; No. 2013CB834505 We acknowledge support from the Ministry of Science and Technology of China (2014CB239402, 2013CB834505), the National Natural Science Foundation of China (51322213, 20901081, 51172245, 91127005, 21201172), the Knowledge Innovation Project of the Chinese Academy of Sciences (KGCX2‐EW‐311‐3), and the 100 Talents Program of the Chinese Academy of Sciences. Y.Y. also thanks the U.S. Department of Energy (DE‐FG02‐09ER16096) for financial support. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 content type line 23 |
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| Snippet | Graphene nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high... Graphene nanosheet‐supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO 2 layers were prepared and used as robust catalysts with high... Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO2 layers were prepared and used as robust catalysts with high... Graphene nanosheet-supported ultrafine metal nanoparticles encapsulated by thin mesoporous SiO sub(2) layers were prepared and used as robust catalysts with... |
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| SubjectTerms | Catalysis Catalysts Catalytic activity Encapsulation Gold Graphene heterogeneous catalysis High temperature mesoporous materials metal nanoparticles Metals Nanoparticles Nanostructure Oxidation Silica Silicon dioxide stability |
| Title | Graphene-Supported Ultrafine Metal Nanoparticles Encapsulated by Mesoporous Silica: Robust Catalysts for Oxidation and Reduction Reactions |
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