One-Pot Green Synthesis of Ag-Decorated SnO2 Microsphere: an Efficient and Reusable Catalyst for Reduction of 4-Nitrophenol

In this paper, hierarchical Ag-decorated SnO 2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitropheno...

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Published in	Nanoscale research letters Vol. 12; no. 1; pp. 435 - 10
Main Authors	Hu, Min, Zhang, Zhenwei, Luo, Chenkun, Qiao, Xiuqing
Format	Journal Article
Language	English
Published	New York Springer US 01.12.2017 Springer Nature B.V SpringerOpen
Subjects	4-Nitrophenol Ag-decorated SnO2 Aminophenol Catalysts Catalytic Catalytic activity Chemical synthesis Chemistry and Materials Science Decoration Hierarchical Hydrothermal Materials Science Microsphere Microspheres Molecular Medicine Nano Express Nanochemistry Nanoparticles Nanoscale Science and Technology Nanosheets Nanostructure Nanotechnology Nanotechnology and Microengineering Nitrophenol p-Aminophenol p-Nitrophenol Reduction Silver Time dependence Tin dioxide X ray photoelectron spectroscopy Ag-decorated SnO Hierarchical Catalytic 4-Nitrophenol Microsphere Hydrothermal
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Abstract	In this paper, hierarchical Ag-decorated SnO 2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH 4 ) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO 2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO 2 nanoparticles will self-assemble into SnO 2 nanosheets and Ag nanoparticles decorated SnO 2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO 2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant ( κ nor ) of 6.20 min −1 g −1 L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO 2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO 2 microsphere and discussed the possible origin of the excellent catalytic activity.
AbstractList	Abstract In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH4) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO2 nanoparticles will self-assemble into SnO2 nanosheets and Ag nanoparticles decorated SnO2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant (κ nor) of 6.20 min−1g−1L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO2 microsphere and discussed the possible origin of the excellent catalytic activity. In this paper, hierarchical Ag-decorated SnO 2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH 4 ) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO 2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO 2 nanoparticles will self-assemble into SnO 2 nanosheets and Ag nanoparticles decorated SnO 2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO 2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant ( κ nor ) of 6.20 min −1 g −1 L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO 2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO 2 microsphere and discussed the possible origin of the excellent catalytic activity. In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH4) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO2 nanoparticles will self-assemble into SnO2 nanosheets and Ag nanoparticles decorated SnO2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant (κnor) of 6.20 min−1g−1L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO2 microsphere and discussed the possible origin of the excellent catalytic activity. In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH4) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO2 nanoparticles will self-assemble into SnO2 nanosheets and Ag nanoparticles decorated SnO2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant (κ nor) of 6.20 min−1g−1L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO2 microsphere and discussed the possible origin of the excellent catalytic activity. In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH4) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO2 nanoparticles will self-assemble into SnO2 nanosheets and Ag nanoparticles decorated SnO2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant (κ nor) of 6.20 min-1g-1L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO2 microsphere and discussed the possible origin of the excellent catalytic activity.In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were characterized by XRD, SEM, TEM, XPS, BET, and FTIR analysis. The catalytic performances of the samples were evaluated with the reduction of 4-nitrophenol to 4-aminophenol by potassium borohydride (KBH4) as a model reaction. Time-dependent experiments indicated that the hierarchical microspheres assembled from SnO2 and Ag nanoparticles can be formed when the react time is less than 10 h. With the increase of hydrothermal time, SnO2 nanoparticles will self-assemble into SnO2 nanosheets and Ag nanoparticles decorated SnO2 nanosheets were obtained. When evaluated as catalyst, the obtained Ag-decorated SnO2 microsphere prepared for 36 h exhibited excellent catalytic performance with normalized rate constant (κ nor) of 6.20 min-1g-1L, which is much better than that of some previous reported catalysts. Moreover, this Ag-decorated SnO2 microsphere demonstrates good reusability after the first five cycles. In addition, we speculate the formation mechanism of the hierarchical Ag-decorated SnO2 microsphere and discussed the possible origin of the excellent catalytic activity.
ArticleNumber	435
Author	Hu, Min Qiao, Xiuqing Luo, Chenkun Zhang, Zhenwei
Author_xml	– sequence: 1 givenname: Min surname: Hu fullname: Hu, Min organization: College of Materials and Chemical Engineering, Hubei Provincial Collaborative Innovation Center for New Energy Microgrid, Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials, China Three Gorges University – sequence: 2 givenname: Zhenwei surname: Zhang fullname: Zhang, Zhenwei organization: College of Materials and Chemical Engineering, Hubei Provincial Collaborative Innovation Center for New Energy Microgrid, Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials, China Three Gorges University – sequence: 3 givenname: Chenkun surname: Luo fullname: Luo, Chenkun organization: College of Materials and Chemical Engineering, Hubei Provincial Collaborative Innovation Center for New Energy Microgrid, Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials, China Three Gorges University – sequence: 4 givenname: Xiuqing surname: Qiao fullname: Qiao, Xiuqing email: 280186517@qq.com organization: College of Materials and Chemical Engineering, Hubei Provincial Collaborative Innovation Center for New Energy Microgrid, Key Laboratory of Inorganic Nonmetallic Crystalline and Energy Conversion Materials, China Three Gorges University
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Keywords	Ag-decorated SnO Hierarchical Catalytic 4-Nitrophenol Microsphere Hydrothermal
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Snippet	In this paper, hierarchical Ag-decorated SnO 2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were... In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were... Abstract In this paper, hierarchical Ag-decorated SnO2 microspheres were synthesized by a facile one-pot hydrothermal method. The resulting composites were...
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SubjectTerms	4-Nitrophenol Ag-decorated SnO2 Aminophenol Catalysts Catalytic Catalytic activity Chemical synthesis Chemistry and Materials Science Decoration Hierarchical Hydrothermal Materials Science Microsphere Microspheres Molecular Medicine Nano Express Nanochemistry Nanoparticles Nanoscale Science and Technology Nanosheets Nanostructure Nanotechnology Nanotechnology and Microengineering Nitrophenol p-Aminophenol p-Nitrophenol Reduction Silver Time dependence Tin dioxide X ray photoelectron spectroscopy
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Title	One-Pot Green Synthesis of Ag-Decorated SnO2 Microsphere: an Efficient and Reusable Catalyst for Reduction of 4-Nitrophenol
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