Control of Metal Nanocrystal Size Reveals Metal-Support Interface Role for Ceria Catalysts
Interactions between ceria (CeO 2 ) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between structure and function in these catalysts have been difficult to extract because the samples studied either were heterogeneous or were model syste...
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| Published in | Science (American Association for the Advancement of Science) Vol. 341; no. 6147; pp. 771 - 773 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Association for the Advancement of Science
16.08.2013
The American Association for the Advancement of Science |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Interactions between ceria (CeO 2 ) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between structure and function in these catalysts have been difficult to extract because the samples studied either were heterogeneous or were model systems dissimilar to working catalysts. We report rate measurements on samples in which the length of the ceria-metal interface was tailored by the use of monodisperse nickel, palladium, and platinum nanocrystals. We found that carbon monoxide oxidation in ceria-based catalysts is greatly enhanced at the ceria-metal interface sites for a range of group VIII metal catalysts, clarifying the pivotal role played by the support. |
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| AbstractList | Interactions between ceria (CeO 2 ) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between structure and function in these catalysts have been difficult to extract because the samples studied either were heterogeneous or were model systems dissimilar to working catalysts. We report rate measurements on samples in which the length of the ceria-metal interface was tailored by the use of monodisperse nickel, palladium, and platinum nanocrystals. We found that carbon monoxide oxidation in ceria-based catalysts is greatly enhanced at the ceria-metal interface sites for a range of group VIII metal catalysts, clarifying the pivotal role played by the support. Interactions between ceria (CeO2) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between structure and function in these catalysts have been difficult to extract because the samples studied either were heterogeneous or were model systems dissimilar to working catalysts. We report rate measurements on samples in which the length of the ceria-metal interface was tailored by the use of monodisperse nickel, palladium, and platinum nanocrystals. We found that carbon monoxide oxidation in ceria-based catalysts is greatly enhanced at the ceria-metal interface sites for a range of group VIII metal catalysts, clarifying the pivotal role played by the support. The rate of a catalytic reaction can sometimes be enhanced by using a different metal oxide as the support for adsorbed metal nanoparticles. Such enhancement is often attributed to more active sites at the metal-oxide interface, but it can be difficult to quantify this effect. Cargnello et al. (p. 771 , published online 18 July) synthesized monodisperse nanoparticles of nickel, platinum, and palladium and dispersed them on high-surface-area ceria or alumina supports. High-resolution transmission electron microscopy enabled a detailed analysis of interfacial site structure, which showed that the rate of CO oxidation on ceria was indeed enhanced greatly at interface sites. Comparing nanocrystals of different sizes on different oxides shows that ceria-metal interface sites enhance carbon monoxide oxidation. Interactions between ceria (CeO 2 ) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between structure and function in these catalysts have been difficult to extract because the samples studied either were heterogeneous or were model systems dissimilar to working catalysts. We report rate measurements on samples in which the length of the ceria-metal interface was tailored by the use of monodisperse nickel, palladium, and platinum nanocrystals. We found that carbon monoxide oxidation in ceria-based catalysts is greatly enhanced at the ceria-metal interface sites for a range of group VIII metal catalysts, clarifying the pivotal role played by the support. A Measure of Metal-Oxide InterfacesThe rate of a catalytic reaction can sometimes be enhanced by using a different metal oxide as the support for adsorbed metal nanoparticles. Such enhancement is often attributed to more active sites at the metal-oxide interface, but it can be difficult to quantify this effect. Cargnello et al. (p. 771, published online 18 July) synthesized monodisperse nanoparticles of nickel, platinum, and palladium and dispersed them on high-surface-area ceria or alumina supports. High-resolution transmission electron microscopy enabled a detailed analysis of interfacial site structure, which showed that the rate of CO oxidation on ceria was indeed enhanced greatly at interface sites. The rate of a catalytic reaction can sometimes be enhanced by using a different metal oxide as the support for adsorbed metal nanoparticles. Such enhancement is often attributed to more active sites at the metal-oxide interface, but it can be difficult to quantify this effect. Cargnello et al. (p. 771, published online 18 July) synthesized monodisperse nanoparticles of nickel, platinum, and palladium and dispersed them on high-surface-area ceria or alumina supports. High-resolution transmission electron microscopy enabled a detailed analysis of interfacial site structure, which showed that the rate of CO oxidation on ceria was indeed enhanced greatly at interface sites. [PUBLICATION ABSTRACT] Interactions between ceria (CeO2) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between structure and function in these catalysts have been difficult to extract because the samples studied either were heterogeneous or were model systems dissimilar to working catalysts. We report rate measurements on samples in which the length of the ceria-metal interface was tailored by the use of monodisperse nickel, palladium, and platinum nanocrystals. We found that carbon monoxide oxidation in ceria-based catalysts is greatly enhanced at the ceria-metal interface sites for a range of group VIII metal catalysts, clarifying the pivotal role played by the support. [PUBLICATION ABSTRACT] |
| Author | Doan-Nguyen, Vicky V. T. Murray, Christopher B. Gorte, Raymond J. Fornasiero, Paolo Cargnello, Matteo Gordon, Thomas R. Diaz, Rosa E. Stach, Eric A. |
| Author_xml | – sequence: 1 givenname: Matteo surname: Cargnello fullname: Cargnello, Matteo – sequence: 2 givenname: Vicky V. T. surname: Doan-Nguyen fullname: Doan-Nguyen, Vicky V. T. – sequence: 3 givenname: Thomas R. surname: Gordon fullname: Gordon, Thomas R. – sequence: 4 givenname: Rosa E. surname: Diaz fullname: Diaz, Rosa E. – sequence: 5 givenname: Eric A. surname: Stach fullname: Stach, Eric A. – sequence: 6 givenname: Raymond J. surname: Gorte fullname: Gorte, Raymond J. – sequence: 7 givenname: Paolo surname: Fornasiero fullname: Fornasiero, Paolo – sequence: 8 givenname: Christopher B. surname: Murray fullname: Murray, Christopher B. |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=27895700$$DView record in Pascal Francis https://www.ncbi.nlm.nih.gov/pubmed/23868919$$D View this record in MEDLINE/PubMed https://www.osti.gov/biblio/1110758$$D View this record in Osti.gov |
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| ContentType | Journal Article |
| Copyright | Copyright © 2013 American Association for the Advancement of Science 2015 INIST-CNRS Copyright © 2013, American Association for the Advancement of Science |
| Copyright_xml | – notice: Copyright © 2013 American Association for the Advancement of Science – notice: 2015 INIST-CNRS – notice: Copyright © 2013, American Association for the Advancement of Science |
| CorporateAuthor | Brookhaven National Laboratory (BNL) Center for Functional Nanomaterials |
| CorporateAuthor_xml | – name: Brookhaven National Laboratory (BNL) Center for Functional Nanomaterials |
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| DOI | 10.1126/science.1240148 |
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| Keywords | Metal support interaction Particle size Group VIII metal Transition metal Palladium Cerium oxide Supported catalyst Heterogeneous catalysis Platinum Nickel Platinoid Interface Nanocrystal |
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| Snippet | Interactions between ceria (CeO 2 ) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between... Interactions between ceria (CeO2) and supported metals greatly enhance rates for a number of important reactions. However, direct relationships between... The rate of a catalytic reaction can sometimes be enhanced by using a different metal oxide as the support for adsorbed metal nanoparticles. Such enhancement... A Measure of Metal-Oxide InterfacesThe rate of a catalytic reaction can sometimes be enhanced by using a different metal oxide as the support for adsorbed... |
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| SubjectTerms | Active sites Aluminum oxide Atoms Carbon monoxide Catalysis Catalysts Cerium oxide Chemical reactions Chemistry Diameters Exact sciences and technology functional nanomaterials General and physical chemistry INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY Metal oxides Metal particles Metals Nanocrystals nanoparticle assembly Nanoparticles Oxidation Oxygen Particle size distribution Roasting Surface physical chemistry Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry transmission electron microscopy |
| Title | Control of Metal Nanocrystal Size Reveals Metal-Support Interface Role for Ceria Catalysts |
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