Manipulating the ordered oxygen complexes to achieve high strength and ductility in medium-entropy alloys

Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particula...

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Published inNature communications Vol. 14; no. 1; pp. 806 - 11
Main Authors Jiao, Meiyuan, Lei, Zhifeng, Wu, Yuan, Du, Jinlong, Zhou, Xiao-Ye, Li, Wenyue, Yuan, Xiaoyuan, Liu, Xiaochun, Zhu, Xiangyu, Wang, Shudao, Zhu, Huihui, Cao, Peipei, Liu, Xiongjun, Zhang, Xiaobin, Wang, Hui, Jiang, Suihe, Lu, Zhaoping
Format Journal Article
LanguageEnglish
Published London Nature Publishing Group UK 13.02.2023
Nature Publishing Group
Nature Portfolio
Subjects
147/135
147/137
147/143
639/301/1023/1026
639/301/1023/303
Alloy systems
Alloys
Ductility
Entropy
Grain Boundary Segregation
High entropy alloys
Humanities and Social Sciences
Interstitials
Medium entropy alloys
multidisciplinary
Niobium
Oxygen
Phase stability
Science
Science (multidisciplinary)
Strengthening
Yield strength
Zirconium
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Abstract Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particular strengthening mechanism holds in other alloys and how these OOCs are tailored remain unclear. Herein, we demonstrate that OOCs can be obtained in bcc (body-centered-cubic) Ti-Zr-Nb medium-entropy alloys via adjusting the content of Nb and oxygen. Decreasing the phase stability enhances the degree of (Ti, Zr)-rich chemical short-range orderings, and then favors formation of OOCs after doping oxygen. Moreover, the number density of OOCs increases with oxygen contents in a given alloy, but adding excessive oxygen (>3.0 at.%) causes grain boundary segregation. Consequently, the tensile yield strength is enhanced by ~75% and ductility is substantially improved by ~164% with addition of 3.0 at.% O in the Ti-30Zr-14Nb MEA. Ordered oxygen complexes (OOCs) endow a unique interstitial strengthening mechanism for simultaneously enhancing strength and ductility in HEAs. Here, the authors demonstrate whether such mechanism can be extended to other alloy systems and how the formation of OOCs is tailored.
AbstractList Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particular strengthening mechanism holds in other alloys and how these OOCs are tailored remain unclear. Herein, we demonstrate that OOCs can be obtained in bcc (body-centered-cubic) Ti-Zr-Nb medium-entropy alloys via adjusting the content of Nb and oxygen. Decreasing the phase stability enhances the degree of (Ti, Zr)-rich chemical short-range orderings, and then favors formation of OOCs after doping oxygen. Moreover, the number density of OOCs increases with oxygen contents in a given alloy, but adding excessive oxygen (>3.0 at.%) causes grain boundary segregation. Consequently, the tensile yield strength is enhanced by ~75% and ductility is substantially improved by ~164% with addition of 3.0 at.% O in the Ti-30Zr-14Nb MEA. Ordered oxygen complexes (OOCs) endow a unique interstitial strengthening mechanism for simultaneously enhancing strength and ductility in HEAs. Here, the authors demonstrate whether such mechanism can be extended to other alloy systems and how the formation of OOCs is tailored.
Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particular strengthening mechanism holds in other alloys and how these OOCs are tailored remain unclear. Herein, we demonstrate that OOCs can be obtained in bcc (body-centered-cubic) Ti-Zr-Nb medium-entropy alloys via adjusting the content of Nb and oxygen. Decreasing the phase stability enhances the degree of (Ti, Zr)-rich chemical short-range orderings, and then favors formation of OOCs after doping oxygen. Moreover, the number density of OOCs increases with oxygen contents in a given alloy, but adding excessive oxygen (>3.0 at.%) causes grain boundary segregation. Consequently, the tensile yield strength is enhanced by ~75% and ductility is substantially improved by ~164% with addition of 3.0 at.% O in the Ti-30Zr-14Nb MEA.Ordered oxygen complexes (OOCs) endow a unique interstitial strengthening mechanism for simultaneously enhancing strength and ductility in HEAs. Here, the authors demonstrate whether such mechanism can be extended to other alloy systems and how the formation of OOCs is tailored.
Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particular strengthening mechanism holds in other alloys and how these OOCs are tailored remain unclear. Herein, we demonstrate that OOCs can be obtained in bcc (body-centered-cubic) Ti-Zr-Nb medium-entropy alloys via adjusting the content of Nb and oxygen. Decreasing the phase stability enhances the degree of (Ti, Zr)-rich chemical short-range orderings, and then favors formation of OOCs after doping oxygen. Moreover, the number density of OOCs increases with oxygen contents in a given alloy, but adding excessive oxygen (>3.0 at.%) causes grain boundary segregation. Consequently, the tensile yield strength is enhanced by ~75% and ductility is substantially improved by ~164% with addition of 3.0 at.% O in the Ti-30Zr-14Nb MEA.
Ordered oxygen complexes (OOCs) endow a unique interstitial strengthening mechanism for simultaneously enhancing strength and ductility in HEAs. Here, the authors demonstrate whether such mechanism can be extended to other alloy systems and how the formation of OOCs is tailored.
Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particular strengthening mechanism holds in other alloys and how these OOCs are tailored remain unclear. Herein, we demonstrate that OOCs can be obtained in bcc (body-centered-cubic) Ti-Zr-Nb medium-entropy alloys via adjusting the content of Nb and oxygen. Decreasing the phase stability enhances the degree of (Ti, Zr)-rich chemical short-range orderings, and then favors formation of OOCs after doping oxygen. Moreover, the number density of OOCs increases with oxygen contents in a given alloy, but adding excessive oxygen (>3.0 at.%) causes grain boundary segregation. Consequently, the tensile yield strength is enhanced by ~75% and ductility is substantially improved by ~164% with addition of 3.0 at.% O in the Ti-30Zr-14Nb MEA.Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state between random interstitials and oxides, can simultaneously enhance strength and ductility in high-entropy alloys. However, whether this particular strengthening mechanism holds in other alloys and how these OOCs are tailored remain unclear. Herein, we demonstrate that OOCs can be obtained in bcc (body-centered-cubic) Ti-Zr-Nb medium-entropy alloys via adjusting the content of Nb and oxygen. Decreasing the phase stability enhances the degree of (Ti, Zr)-rich chemical short-range orderings, and then favors formation of OOCs after doping oxygen. Moreover, the number density of OOCs increases with oxygen contents in a given alloy, but adding excessive oxygen (>3.0 at.%) causes grain boundary segregation. Consequently, the tensile yield strength is enhanced by ~75% and ductility is substantially improved by ~164% with addition of 3.0 at.% O in the Ti-30Zr-14Nb MEA.
ArticleNumber 806
Author Wang, Shudao
Jiang, Suihe
Wang, Hui
Zhu, Huihui
Jiao, Meiyuan
Li, Wenyue
Yuan, Xiaoyuan
Zhou, Xiao-Ye
Liu, Xiongjun
Lei, Zhifeng
Zhang, Xiaobin
Lu, Zhaoping
Du, Jinlong
Liu, Xiaochun
Wu, Yuan
Zhu, Xiangyu
Cao, Peipei
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/36781880$$D View this record in MEDLINE/PubMed
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SSID ssj0000391844
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Snippet Oxygen solute strengthening is an effective strategy to harden alloys, yet, it often deteriorates the ductility. Ordered oxygen complexes (OOCs), a state...
Ordered oxygen complexes (OOCs) endow a unique interstitial strengthening mechanism for simultaneously enhancing strength and ductility in HEAs. Here, the...
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SubjectTerms 147/135
147/137
147/143
639/301/1023/1026
639/301/1023/303
Alloy systems
Alloys
Ductility
Entropy
Grain Boundary Segregation
High entropy alloys
Humanities and Social Sciences
Interstitials
Medium entropy alloys
multidisciplinary
Niobium
Oxygen
Phase stability
Science
Science (multidisciplinary)
Strengthening
Yield strength
Zirconium
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Title Manipulating the ordered oxygen complexes to achieve high strength and ductility in medium-entropy alloys
URI https://link.springer.com/article/10.1038/s41467-023-36319-0
https://www.ncbi.nlm.nih.gov/pubmed/36781880
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https://www.proquest.com/docview/2776517918
https://pubmed.ncbi.nlm.nih.gov/PMC9925791
https://doaj.org/article/78028a0168bb42e2addf62c3bf7ddb05
Volume 14
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