Potential of a metal-organic framework as a new material for solid-phase extraction of pesticides from lettuce (Lactuca sativa), with analysis by gas chromatography-mass spectrometry
The metal-organic framework ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α- and β-endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5...
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| Published in | Journal of separation science Vol. 33; no. 23-24; pp. 3811 - 3816 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley-VCH Verlag
01.12.2010
WILEY-VCH Verlag WILEY‐VCH Verlag Wiley |
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| Abstract | The metal-organic framework ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α- and β-endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5 mg/kg), and resulted in recoveries in the range of 78-107%, with RSD values between 1.6 and 8.0% for ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] sorbent. Detection and quantification limits ranged from 0.02 to 0.05 mg/kg and from 0.05 to 0.10 mg/kg, respectively, for the different pesticides studied. The method developed was linear over the range tested (0.05-10.0 μg/mL), with correlation coefficients ranging from 0.9990 to 0.9997. Comparison between ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] and conventional sorbent (silica gel) showed better performance of the ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] polymeric sorbent for all pesticides tested. |
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| AbstractList | The metal–organic framework ∞[(La0.9Eu0.1)2(DPA)3(H2O)3] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α‐ and β‐endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5 mg/kg), and resulted in recoveries in the range of 78–107%, with RSD values between 1.6 and 8.0% for ∞[(La0.9Eu0.1)2(DPA)3(H2O)3] sorbent. Detection and quantification limits ranged from 0.02 to 0.05 mg/kg and from 0.05 to 0.10 mg/kg, respectively, for the different pesticides studied. The method developed was linear over the range tested (0.05–10.0 μg/mL), with correlation coefficients ranging from 0.9990 to 0.9997. Comparison between ∞[(La0.9Eu0.1)2(DPA)3(H2O)3] and conventional sorbent (silica gel) showed better performance of the ∞[(La0.9Eu0.1)2(DPA)3(H2O)3] polymeric sorbent for all pesticides tested. The metal-organic framework {infinity}[(La0.9Eu0.1)2(DPA)3(H2O)3] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and - and Delta *b-endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5mg/kg), and resulted in recoveries in the range of 78-107%, with RSD values between 1.6 and 8.0% for {infinity}[(La0.9Eu0.1)2(DPA)3(H2O)3] sorbent. Detection and quantification limits ranged from 0.02 to 0.05mg/kg and from 0.05 to 0.10mg/kg, respectively, for the different pesticides studied. The method developed was linear over the range tested (0.05-10.0 Delta *mg/mL), with correlation coefficients ranging from 0.9990 to 0.9997. Comparison between {infinity}[(La0.9Eu0.1)2(DPA)3(H2O)3] and conventional sorbent (silica gel) showed better performance of the {infinity}[(La0.9Eu0.1)2(DPA)3(H2O)3] polymeric sorbent for all pesticides tested. The metal-organic framework ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α- and β-endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5 mg/kg), and resulted in recoveries in the range of 78-107%, with RSD values between 1.6 and 8.0% for ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] sorbent. Detection and quantification limits ranged from 0.02 to 0.05 mg/kg and from 0.05 to 0.10 mg/kg, respectively, for the different pesticides studied. The method developed was linear over the range tested (0.05-10.0 μg/mL), with correlation coefficients ranging from 0.9990 to 0.9997. Comparison between ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] and conventional sorbent (silica gel) showed better performance of the ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] polymeric sorbent for all pesticides tested. The metal-organic framework (∞)[(La(0.9)Eu(0.1))(2)(DPA)(3)(H(2)O)(3)] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α- and β-endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5 mg/kg), and resulted in recoveries in the range of 78-107%, with RSD values between 1.6 and 8.0% for (∞)[(La(0.9)Eu(0.1))(2)(DPA)(3)(H(2)O)(3)] sorbent. Detection and quantification limits ranged from 0.02 to 0.05 mg/kg and from 0.05 to 0.10 mg/kg, respectively, for the different pesticides studied. The method developed was linear over the range tested (0.05-10.0 μg/mL), with correlation coefficients ranging from 0.9990 to 0.9997. Comparison between (∞)[(La(0.9)Eu(0.1))(2)(DPA)(3)(H(2)O)(3)] and conventional sorbent (silica gel) showed better performance of the (∞)[(La(0.9)Eu(0.1))(2)(DPA)(3)(H(2)O)(3)] polymeric sorbent for all pesticides tested. Abstract The metal–organic framework ∞ [(La 0.9 Eu 0.1 ) 2 (DPA) 3 (H 2 O) 3 ] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α‐ and β‐endosulfan from lettuce, with analysis using GC/MS in SIM mode. Experiments were carried out in triplicate at two fortification levels (0.1 and 0.5 mg/kg), and resulted in recoveries in the range of 78–107%, with RSD values between 1.6 and 8.0% for ∞ [(La 0.9 Eu 0.1 ) 2 (DPA) 3 (H 2 O) 3 ] sorbent. Detection and quantification limits ranged from 0.02 to 0.05 mg/kg and from 0.05 to 0.10 mg/kg, respectively, for the different pesticides studied. The method developed was linear over the range tested (0.05–10.0 μg/mL), with correlation coefficients ranging from 0.9990 to 0.9997. Comparison between ∞ [(La 0.9 Eu 0.1 ) 2 (DPA) 3 (H 2 O) 3 ] and conventional sorbent (silica gel) showed better performance of the ∞ [(La 0.9 Eu 0.1 ) 2 (DPA) 3 (H 2 O) 3 ] polymeric sorbent for all pesticides tested. |
| Author | Barreto, Alysson S. da Silva, Rogério Luiz Navickiene, Sandro de Simone, Carlos A. de Mesquita, Maria Eliane Rodrigues, Marcelo O. dos Santos Silva, Silvia Caroline G. Júnior, Severino A. de Sá, Gilberto F. |
| Author_xml | – sequence: 1 fullname: Barreto, Alysson S – sequence: 2 fullname: da Silva, Rogério Luiz – sequence: 3 fullname: dos Santos Silva, Silvia Caroline G – sequence: 4 fullname: Rodrigues, Marcelo O – sequence: 5 fullname: de Simone, Carlos A – sequence: 6 fullname: de Sá, Gilberto F – sequence: 7 fullname: Júnior, Severino A – sequence: 8 fullname: Navickiene, Sandro – sequence: 9 fullname: de Mesquita, Maria Eliane |
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| Keywords | Solid phase extraction Chemical analysis Insecticide Vegetables Systemic Compositae Chemical enrichment Lettuce Sample preparation Dicotyledones Angiospermae Adsorbent Lactuca sativa Quantitative analysis Matrix Solid Phase Dispersion extraction Trace analysis Metal organic framework Coupled method Pesticides Malathion Matrix solid-phase dispersion Contamination Fungicide Gas chromatography Vegetable crop Residue Organophosphorus compounds Spermatophyta Metal-organic framework Mass spectrometry |
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| Snippet | The metal-organic framework ∞[(La₀.₉Eu₀.₁)₂(DPA)₃(H₂O)₃] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α- and... The metal–organic framework ∞[(La0.9Eu0.1)2(DPA)3(H2O)3] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α‐ and... The metal-organic framework (∞)[(La(0.9)Eu(0.1))(2)(DPA)(3)(H(2)O)(3)] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and α-... Abstract The metal–organic framework ∞ [(La 0.9 Eu 0.1 ) 2 (DPA) 3 (H 2 O) 3 ] was tested for extraction of pyrimicarb, procymidone, malathion, methyl... The metal-organic framework {infinity}[(La0.9Eu0.1)2(DPA)3(H2O)3] was tested for extraction of pyrimicarb, procymidone, malathion, methyl parathion and - and... |
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| SubjectTerms | Biological and medical sciences Extraction Food industries Fruit and vegetable industries Fundamental and applied biological sciences. Psychology Gas Chromatography-Mass Spectrometry - methods Lactuca - chemistry Lettuce Lettuces Limit of Detection Matrix solid-phase dispersion Metal-organic framework Metal-organic frameworks Pesticides Pesticides - analysis Reference Standards Reproducibility of Results Silica gel SIM Solid Phase Extraction - instrumentation Sorbents Spectrometry Spectroscopy Spectroscopy, Fourier Transform Infrared |
| Title | Potential of a metal-organic framework as a new material for solid-phase extraction of pesticides from lettuce (Lactuca sativa), with analysis by gas chromatography-mass spectrometry |
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