Low-Temperature Synthesis of Nanosized Bismuth Ferrite by Soft Chemical Route
The present research describes a simple low‐temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of Bismuth and Iron. Tartaric acid is used as a template material and nitric acid as an oxidizing agent. The synthesized powders are characteriz...
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| Published in | Journal of the American Ceramic Society Vol. 88; no. 5; pp. 1349 - 1352 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford, UK
Blackwell Science Inc
01.05.2005
Blackwell Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The present research describes a simple low‐temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of Bismuth and Iron. Tartaric acid is used as a template material and nitric acid as an oxidizing agent. The synthesized powders are characterized by X‐ray diffractometry, thermogravimetry and differential thermal analysis, infrared spectroscopy, and scanning electron microscopy. The particle size of the powder lies between 3 and 16 nm. In the process, phase pure bismuth ferrite can be obtained at a temperature as low as 400°C, in contrast to 550°C for coprecipitation route. On the other hand, we find that, like solid state reaction route, Pechini's autocombustion method of synthesis generates a lot of impurity phases along with bismuth ferrite. |
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| AbstractList | The present research describes a simple low-temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of Bismuth and Iron. Tartaric acid is used as a template material and nitric acid as an oxidizing agent. The synthesized powders are characterized by X-ray diffractometry, thermogravimetry and differential thermal analysis, infrared spectroscopy, and scanning electron microscopy. The particle size of the powder lies between 3 and 16 nm. In the process, phase pure bismuth ferrite can be obtained at a temperature as low as 400 degrees C, in contrast to 550 degrees C for coprecipitation route. On the other hand, we find that, like solid state reaction route, Pechini's autocombustion method of synthesis generates a lot of impurity phases along with bismuth ferrite.[PUBLICATION ABSTRACT] The present research describes a simple low‐temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of Bismuth and Iron. Tartaric acid is used as a template material and nitric acid as an oxidizing agent. The synthesized powders are characterized by X‐ray diffractometry, thermogravimetry and differential thermal analysis, infrared spectroscopy, and scanning electron microscopy. The particle size of the powder lies between 3 and 16 nm. In the process, phase pure bismuth ferrite can be obtained at a temperature as low as 400°C, in contrast to 550°C for coprecipitation route. On the other hand, we find that, like solid state reaction route, Pechini's autocombustion method of synthesis generates a lot of impurity phases along with bismuth ferrite. The present research describes a simple low-temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of Bismuth and Iron. Tartaric acid is used as a template material and nitric acid as an oxidizing agent. The synthesized powders are characterized by X-ray diffractometry, thermogravimetry and differential thermal analysis, infrared spectroscopy, and scanning electron microscopy. The particle size of the powder lies between 3 and 16 nm. In the process, phase pure bismuth ferrite can be obtained at a temperature as low as 400DGC, in contrast to 550DGC for coprecipitation route. On the other hand, we find that, like solid state reaction route, Pechini's autocombustion method of synthesis generates a lot of impurity phases along with bismuth ferrite. A soft chemical route using nitrates of bismuth and iron provided a simple low-temperature synthesis of bismuth ferrite nanopowders. Tartaric acid was used as a template material and nitric acid as an oxidising agent. The synthesised powders were characterised by XRD, TG/DTA, IR spectroscopy, and SEM. The particle size of the powder lay between 3 and 16 nm. In the process, phase pure bismuth ferrite could be obtained at a temperature as low as 400 C, in contrast to 550 C for the coprecipitation route. On the other hand, as with the solid state reaction route, Pechini's autocombustion method of synthesis generated a lot of impurity phases along with the bismuth ferrite. 12 refs. |
| Author | Dasgupta, Subrata Sen, Amarnath Ghosh, Sushmita Sekhar Maiti, Himadri |
| Author_xml | – sequence: 1 givenname: Sushmita surname: Ghosh fullname: Ghosh, Sushmita organization: Central Glass & Ceramic Research Institute, Kolkata 700 032, India – sequence: 2 givenname: Subrata surname: Dasgupta fullname: Dasgupta, Subrata email: sdasgupta@cgcri.res.in organization: Central Glass & Ceramic Research Institute, Kolkata 700 032, India – sequence: 3 givenname: Amarnath surname: Sen fullname: Sen, Amarnath organization: Central Glass & Ceramic Research Institute, Kolkata 700 032, India – sequence: 4 givenname: Himadri surname: Sekhar Maiti fullname: Sekhar Maiti, Himadri organization: Central Glass & Ceramic Research Institute, Kolkata 700 032, India |
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| Keywords | Scanning electron microscopy Inorganic compounds Transition element compounds Thermogravimetry Oxides Bismuth Iron Oxides Mixed Bismuth oxides Differential thermal analysis XRD Evaporation Experimental study Ultrafine powder Characterization Ferrites Ferroelectric materials Iron oxides Chemical synthesis Soft chemistry Nanostructured materials Low temperature |
| Language | English |
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| Notes | ark:/67375/WNG-71PW33JD-K istex:D963254C4B59A9FAF44D60F4861927E61CBB1850 ArticleID:JACE00306 L. C. Klein—contributing editor Supported by the CSIR Network project CMM 002. ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| PublicationDate | May 2005 |
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| PublicationTitle | Journal of the American Ceramic Society |
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| References | J. D. Bucci, B. K. Robertson, and W. J. James, "The Precision Determination of the Lattice Parameters and the Coefficients of Thermal Expansion of BiFeO3,"J. Appl. Cryst., 5, 187-91 (1972). I. Nakagawa and J. L. Walter, "Optically Active Crystal Vibrations of the Alkali-Metal Nitrates,"J. Chem. Phys., 51 [4] 1389-97 (1969). V. R. Palkar and R. Pinto, "BiFeO3 Thin Films: Novel Effects,"Pramana J. Phys., 58 [5, 6] 1003-8 (2002). S. Shetty, V. R. Palkar, and R. Pinto, "Size Effect Study in Magnetoelectric BiFeO3 System,"Pramana J. Phys., 58 [5, 6] 1027-30 (2002). F. Kubel and H. Schmid, "Structure of a Ferroelectric and Ferroelastic Monodomain Crystal of the Perovskite BiFeO3,"Acta Crystallogr., 46, 698-702 (1990). Y. P. Wang, L. Zohu, M. F. Zhang, X. Y. Chen, J. M. Liu, and Z. G. Liu, "Room-Temperature Saturated Ferroelectric Polarization in BiFeO3 Ceramics Synthesized by Rapid Liquid Phase Sintering,"Appl. Phys. Lett., 84 [10] 1731-3 (2004). M. Marezio, J. P. Remeiko, and P. D. Dernier, "The Crystal Chemistry of the Rare Earth Orthoferrites,"Acta Crystallogr., B26, 2008-22 (1970). G. D. Achenbach, W. J. James, and R. Gerson, "Preparation of Single-Phase Polycrystalline BiFeO3,"J. Am. Ceram. Soc., 8, 437 (1967). A. W. Herrmann, E. Herdtweck, K. Wolfgang, and P. Paul, "Metal Complexes in Biology and Medicine, V. New Bismuth Hydroxycarboxylate Complexes-Synthesis and Structure of Bismuth (III) Malate Monohydrate and Bismuth (III) Tartarate Trihydrate,"Chem. Ber., 126 [1] 51-6 (1993). 2000; 50 2002; 58 1967; 8 1961 2004; 84 1990; 46 1972; 5 1970; B26 1993; 126 1969; 51 e_1_2_5_13_2 e_1_2_5_8_2 e_1_2_5_7_2 e_1_2_5_10_2 e_1_2_5_6_2 e_1_2_5_5_2 e_1_2_5_12_2 e_1_2_5_11_2 e_1_2_5_3_2 e_1_2_5_2_2 Vogel A. I. (e_1_2_5_9_2) 1961 Palkar V. R. (e_1_2_5_4_2) 2002; 58 |
| References_xml | – volume: 5 start-page: 187 year: 1972 end-page: 91 article-title: The Precision Determination of the Lattice Parameters and the Coefficients of Thermal Expansion of BiFeO publication-title: J. Appl. Cryst. – volume: 8 start-page: 437 year: 1967 article-title: Preparation of Single‐Phase Polycrystalline BiFeO publication-title: J. Am. Ceram. Soc. – volume: 58 start-page: 1027 issue: [5, 6] year: 2002 end-page: 30 article-title: Size Effect Study in Magnetoelectric BiFeO System publication-title: Pramana J. Phys. – volume: 46 start-page: 698 year: 1990 end-page: 702 article-title: Structure of a Ferroelectric and Ferroelastic Monodomain Crystal of the Perovskite BiFeO publication-title: Acta Crystallogr. – volume: 50 start-page: 285 year: 2000 end-page: 357 – volume: 84 start-page: 1731 issue: [10] year: 2004 end-page: 3 article-title: Room‐Temperature Saturated Ferroelectric Polarization in BiFeO Ceramics Synthesized by Rapid Liquid Phase Sintering publication-title: Appl. Phys. Lett. – volume: B26 start-page: 2008 year: 1970 end-page: 22 article-title: The Crystal Chemistry of the Rare Earth Orthoferrites publication-title: Acta Crystallogr. – volume: 58 start-page: 1003 issue: [5, 6] year: 2002 end-page: 8 article-title: BiFeO Thin Films publication-title: Novel Effects – start-page: 442 year: 1961 – volume: 51 start-page: 1389 issue: [4] year: 1969 end-page: 97 article-title: Optically Active Crystal Vibrations of the Alkali‐Metal Nitrates publication-title: J. Chem. Phys. – volume: 126 start-page: 51 issue: [1] year: 1993 end-page: 6 article-title: Metal Complexes in Biology and Medicine, V. New Bismuth Hydroxycarboxylate Complexes‐Synthesis and Structure of Bismuth (III) Malate Monohydrate and Bismuth (III) Tartarate Trihydrate publication-title: Chem. Ber. – ident: e_1_2_5_12_2 doi: 10.1002/cber.19931260109 – ident: e_1_2_5_3_2 doi: 10.1107/S0108768190006887 – ident: e_1_2_5_7_2 doi: 10.1007/s12043-002-0211-4 – start-page: 442 volume-title: A Text Book of Inorganic Analysis year: 1961 ident: e_1_2_5_9_2 contributor: fullname: Vogel A. I. – volume: 58 start-page: 1003 issue: 5 year: 2002 ident: e_1_2_5_4_2 article-title: BiFeO3 Thin Films publication-title: Novel Effects contributor: fullname: Palkar V. R. – ident: e_1_2_5_2_2 doi: 10.1107/S0021889872009173 – ident: e_1_2_5_11_2 doi: 10.1016/S0898-8838(00)50007-5 – ident: e_1_2_5_10_2 doi: 10.1063/1.1672186 – ident: e_1_2_5_5_2 doi: 10.1063/1.1667612 – ident: e_1_2_5_6_2 doi: 10.1111/j.1151-2916.1967.tb15153.x – ident: e_1_2_5_8_2 – ident: e_1_2_5_13_2 doi: 10.1107/S0567740870005319 |
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| Snippet | The present research describes a simple low‐temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of... The present research describes a simple low-temperature synthesis route of preparing bismuth ferrite nanopowders through soft chemical route using nitrates of... A soft chemical route using nitrates of bismuth and iron provided a simple low-temperature synthesis of bismuth ferrite nanopowders. Tartaric acid was used as... |
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| SubjectTerms | Ceramics Cross-disciplinary physics: materials science; rheology Electrons Exact sciences and technology Iron Materials science Microscopy Nanopowders Nanoscale materials and structures: fabrication and characterization Physics |
| Title | Low-Temperature Synthesis of Nanosized Bismuth Ferrite by Soft Chemical Route |
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