Degradation of a commercial textile biocide with advanced oxidation processes and ozone
The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well...
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| Published in | Journal of environmental management Vol. 82; no. 2; pp. 145 - 154 |
|---|---|
| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
2007
Elsevier Academic Press Ltd |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO
2/UV-A, TiO
2/UV-A/H
2O
2) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4′-trichloro-2′-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD
5,o⩽5
mg/L; COD
o=200
mg/L; DOC
o (dissolved organic carbon)=58
mg/L; AOX
o (adsorbable organic halogens)=48
mg/L; LC
50,o (lethal concentration causing 50% death or immobilization in
Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500–900
mg/h) and initial pH (7–12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV
280 and UV
254 abatement), dechlorination (AOX removal) and detoxification (changes in LC
50). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO
2 was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H
2O
2 addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO
2/UV-A and TiO
2/UV-A/H
2O
2) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV
280 abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20
min ozonation (267
mg O
3). On the other hand, for complete detoxification, ozonation had to be continued for at least 30
min (corresponding to 400
mg O
3). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO
2/UV-A and TiO
2/UV-A/H
2O
2). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals. |
|---|---|
| AbstractList | The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO(2)/UV-A, TiO(2)/UV-A/H(2)O(2)) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4'-trichloro-2'-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD(5,o) < or =5 mg/L; COD(o)=200 mg/L; DOC(o) (dissolved organic carbon)=58 mg/L; AOX(o) (adsorbable organic halogens)=48 mg/L; LC(50,o) (lethal concentration causing 50% death or immobilization in Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500-900 mg/h) and initial pH (7-12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV(280) and UV(254) abatement), dechlorination (AOX removal) and detoxification (changes in LC(50)). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO(2) was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H(2)O(2) addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO(2)/UV-A and TiO(2)/UV-A/H(2)O(2)) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV(280) abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20 min ozonation (267 mg O(3)). On the other hand, for complete detoxification, ozonation had to be continued for at least 30 min (corresponding to 400mg O(3)). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO(2)/UV-A and TiO(2)/UV-A/H(2)O(2)). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals. The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO2/UV-A, TiO2/UV-A/H2O2) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4'- trichloro-2'-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD5,o ≤ 5 mg/L; CODo=200 mg L; DOCo (dissolved organic carbon) 58 mg L; AOXo (adsorbable organic halogens) 48 mg L; LC50,o (lethal concentration causing 5000 death or immobilization in Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500 900 mg h) and initial pH (7 12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV280 and UV254 abatement), dechlorination (AOX removal) and detoxification (changes in LC50). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO2 was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H2O2 addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO2/UV-A and TiO2/UV-A/H2O2) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV280 abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20 min ozonation (267 mg O3). On the other hand, for complete detoxification, ozonation had to be continued for at least 30 min (corresponding to 400 mg O3). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO2/UV-A and TiO2/UV-A/H2O2). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals. [PUBLICATION ABSTRACT] The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO(2)/UV-A, TiO(2)/UV-A/H(2)O(2)) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4'-trichloro-2'-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD(5,o) < or =5 mg/L; COD(o)=200 mg/L; DOC(o) (dissolved organic carbon)=58 mg/L; AOX(o) (adsorbable organic halogens)=48 mg/L; LC(50,o) (lethal concentration causing 50% death or immobilization in Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500-900 mg/h) and initial pH (7-12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV(280) and UV(254) abatement), dechlorination (AOX removal) and detoxification (changes in LC(50)). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO(2) was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H(2)O(2) addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO(2)/UV-A and TiO(2)/UV-A/H(2)O(2)) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV(280) abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20 min ozonation (267 mg O(3)). On the other hand, for complete detoxification, ozonation had to be continued for at least 30 min (corresponding to 400mg O(3)). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO(2)/UV-A and TiO(2)/UV-A/H(2)O(2)). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals.The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO(2)/UV-A, TiO(2)/UV-A/H(2)O(2)) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4'-trichloro-2'-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD(5,o) < or =5 mg/L; COD(o)=200 mg/L; DOC(o) (dissolved organic carbon)=58 mg/L; AOX(o) (adsorbable organic halogens)=48 mg/L; LC(50,o) (lethal concentration causing 50% death or immobilization in Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500-900 mg/h) and initial pH (7-12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV(280) and UV(254) abatement), dechlorination (AOX removal) and detoxification (changes in LC(50)). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO(2) was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H(2)O(2) addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO(2)/UV-A and TiO(2)/UV-A/H(2)O(2)) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV(280) abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20 min ozonation (267 mg O(3)). On the other hand, for complete detoxification, ozonation had to be continued for at least 30 min (corresponding to 400mg O(3)). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO(2)/UV-A and TiO(2)/UV-A/H(2)O(2)). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals. Degradation of commercial textile biocide with oxidation process and ozone was examined. The aqueous biocide solution was prepared to mimic effluent originating from the antimicrobial operation. Ozonation experiments were conducted at different ozone doses and pH to assess the effect of ozonation on degradation, dearomatization, dechlorination and detoxification. Fenton experiments were also carried out to find the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation. During ozonation of the textile biocide effluent, adsorbable organic halogens AOX abatement proceeded significantly faster than dearomatization and was completed after 20 min of ozonation. It was concluded that textile biocides can be effectively degraded and detoxified with partial oxidation and mineralization using advanced oxidation process and ozone. The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO 2/UV-A, TiO 2/UV-A/H 2O 2) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4′-trichloro-2′-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD 5,o⩽5 mg/L; COD o=200 mg/L; DOC o (dissolved organic carbon)=58 mg/L; AOX o (adsorbable organic halogens)=48 mg/L; LC 50,o (lethal concentration causing 50% death or immobilization in Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500–900 mg/h) and initial pH (7–12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV 280 and UV 254 abatement), dechlorination (AOX removal) and detoxification (changes in LC 50). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO 2 was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H 2O 2 addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO 2/UV-A and TiO 2/UV-A/H 2O 2) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV 280 abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20 min ozonation (267 mg O 3). On the other hand, for complete detoxification, ozonation had to be continued for at least 30 min (corresponding to 400 mg O 3). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO 2/UV-A and TiO 2/UV-A/H 2O 2). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals. The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a subject of major public health concern and scientific interest only recently. In the present study, the treatment efficiency of selected, well-known advanced oxidation processes (Fenton, Photo-Fenton, TiO sub(2)/UV-A, TiO sub(2)/UV-A/H sub(2)O sub(2)) and ozone was compared for the degradation and detoxification of a commercial textile biocide formulation containing a 2,4,4'-trichloro-2'-hydroxydiphenyl ether as the active ingredient. The aqueous biocide solution was prepared to mimic typical effluent originating from the antimicrobial finishing operation (BOD sub(5) sub(,) sub(o)=<5mg/L; COD sub(o)=200mg/L; DOC sub(o) (dissolved organic carbon)=58mg/L; AOX sub(o) (adsorbable organic halogens)=48mg/L; LC sub(5) sub(0) sub(,) sub(o) (lethal concentration causing 50% death or immobilization in Daphnia magna)=8% v/v). Ozonation experiments were conducted at different ozone doses (500-900mg/h) and initial pH (7-12) to assess the effect of ozonation on degradation (COD, DOC removal), dearomatization (UV sub(2) sub(8) sub(0) and UV sub(2) sub(5) sub(4) abatement), dechlorination (AOX removal) and detoxification (changes in LC sub(5) sub(0)). For the Fenton experiments, the effect of varying ferrous iron catalyst concentrations and UV-A light irradiation (the Photo-Fenton process) was examined. In the heterogenous photocatalytic experiments, Degussa P25-type TiO sub(2) was used as the catalyst and the effect of reaction pH (3, 7 and 12) and H sub(2)O sub(2) addition on the photocatalytic treatment efficiency was examined. Although in the photochemical (i.e. Photo-Fenton, TiO sub(2)/UV-A and TiO sub(2)/UV-A/H sub(2)O sub(2)) experiments appreciably higher COD and DOC removal efficiencies were obtained, ozonation appeared to be equally effective to achieve dearomatization (UV sub(2) sub(8) sub(0) abatement) at all studied reaction pH. During ozonation of the textile biocide effluent, AOX abatement proceeded significantly faster than dearomatization and was complete after 20min ozonation (267mg O sub(3)). On the other hand, for complete detoxification, ozonation had to be continued for at least 30min (corresponding to 400mg O sub(3)). Effective AOX and acute toxicity removal was also obtained after heterogeneous photocatalytic treatment (TiO sub(2)/UV-A and TiO sub(2)/UV-A/H sub(2)O sub(2)). The Fenton-based treatment experiments and particularly the dark Fenton reaction resulted in relatively poor degradation, dearomatization, AOX and acute toxicity removals. |
| Author | Arslan-Alaton, Idil |
| Author_xml | – sequence: 1 givenname: Idil surname: Arslan-Alaton fullname: Arslan-Alaton, Idil email: arslanid@itu.edu.tr organization: Department of Environmental Engineering, Faculty of Civil Engineering, Istanbul Technical University, 34469 Maslak, Istanbul, Turkey |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=18403247$$DView record in Pascal Francis https://www.ncbi.nlm.nih.gov/pubmed/16624477$$D View this record in MEDLINE/PubMed |
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| DOI | 10.1016/j.jenvman.2005.12.021 |
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| Keywords | Ozonation Textile finishing biocides AOX Xenobiotics Advanced Oxidation Processes (AOPS) Acute toxicity Textile Toxicity Acute Ozone Environmental management Degradation Oxidation Biocide Xenobiotic |
| Language | English |
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| Snippet | The occurrence of significant amounts of biocidal finishing agents in the environment as a consequence of intensive textile finishing activities has become a... Degradation of commercial textile biocide with oxidation process and ozone was examined. The aqueous biocide solution was prepared to mimic effluent... |
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| SubjectTerms | Acute toxicity adsorption Advanced Oxidation Processes (AOPS) Animal, plant and microbial ecology anti-infective agents antimicrobial agents AOX Applied ecology Aqueous solutions aromatic hydrocarbons biochemical oxygen demand Biodegradation Biological and medical sciences chemical degradation chemical oxygen demand chemistry Coloring Agents Coloring Agents - chemistry Conservation, protection and management of environment and wildlife Daphnia Daphnia magna dechlorination decontamination detoxification (processing) dissolved organic carbon dosage duration ecotoxicology Ecotoxicology, biological effects of pollution fabrics Fundamental and applied biological sciences. Psychology General aspects halogenated hydrocarbons Hydrogen Peroxide Industrial Waste Industrial Waste - prevention & control lethal concentration 50 methods Oxidants, Photochemical Oxidants, Photochemical - chemistry Oxidation Oxidation-Reduction Oxidation-Reduction - radiation effects Ozonation ozone Ozone - chemistry ozone treatment Photocatalysis pollutants prevention & control radiation effects textile finishes Textile finishing biocides Textile Industry textile mill effluents Textiles Toxicity ultraviolet radiation Ultraviolet Rays Waste Disposal, Fluid Waste Disposal, Fluid - methods Water Pollutants, Chemical Water Pollutants, Chemical - chemistry Water Pollution, Chemical Water Pollution, Chemical - prevention & control Xenobiotics |
| Title | Degradation of a commercial textile biocide with advanced oxidation processes and ozone |
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