General and Selective Iron-Catalyzed Aminocarbonylation of Alkynes: Synthesis of Acryl- and Cinnamides
Entering the iron age: The first general method for iron‐catalyzed monocarbonylation of alkynes has been developed. A range of structurally diverse cinnamides and acrylamides have been obtained smoothly starting from commercially available amines and alkynes in the presence of [Fe3(CO)12] and ligand...
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| Published in | Angewandte Chemie (International ed.) Vol. 50; no. 2; pp. 537 - 541 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley-VCH Verlag
10.01.2011
WILEY-VCH Verlag WILEY‐VCH Verlag Wiley Wiley Subscription Services, Inc |
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Entering the iron age: The first general method for iron‐catalyzed monocarbonylation of alkynes has been developed. A range of structurally diverse cinnamides and acrylamides have been obtained smoothly starting from commercially available amines and alkynes in the presence of [Fe3(CO)12] and ligand L (see scheme). The method is highly chemo‐ and regioselective and requires no expensive catalyst. |
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| AbstractList | Entering the iron age: The first general method for iron‐catalyzed monocarbonylation of alkynes has been developed. A range of structurally diverse cinnamides and acrylamides have been obtained smoothly starting from commercially available amines and alkynes in the presence of [Fe3(CO)12] and ligand L (see scheme). The method is highly chemo‐ and regioselective and requires no expensive catalyst. |
| Author | Beller, Matthias Jackstell, Ralf Driller, Katrin Marie Prateeptongkum, Saisuree |
| Author_xml | – sequence: 1 fullname: Driller, Katrin Marie – sequence: 2 fullname: Prateeptongkum, Saisuree – sequence: 3 fullname: Jackstell, Ralf – sequence: 4 fullname: Beller, Matthias |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/21120980$$D View this record in MEDLINE/PubMed |
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| Keywords | cinnamides P-ARYLTHIO CINNAMIDES EFFICIENT SYNTHESIS TRANSFER HYDROGENATION ALPHA,BETA-UNSATURATED AMIDES CARBONYL-COMPLEXES CROSS-COUPLING REACTIONS homogeneous catalysis acrylamides iron METAL (E)-ALPHA,BETA-UNSATURATED AMIDES carbonylation ALLYLIC SUBSTITUTION CYCLOBUTENEDIONES |
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| Notes | http://dx.doi.org/10.1002/anie.201005823 ArticleID:ANIE201005823 Deutsche Forschungsgemeinschaft This work was funded by the the Deutsche Forschungsgemeinschaft (Graduiertenkolleg 1213 and Leibniz-price). We thank Dr. C. Fischer, S. Buchholz, S. Schareina, A. Kammer, K. Fiedler, A. Lehmann, I. Stahr, A. Koch, and Dr. W. Baumann for their excellent technical and analytical support. istex:1371A2AC20D2055E00EE2531F153CE3097AD0E10 ark:/67375/WNG-8QXMWW30-X This work was funded by the the Deutsche Forschungsgemeinschaft (Graduiertenkolleg 1213 and Leibniz‐price). We thank Dr. C. Fischer, S. Buchholz, S. Schareina, A. Kammer, K. Fiedler, A. Lehmann, I. Stahr, A. Koch, and Dr. W. Baumann for their excellent technical and analytical support. ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
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| Snippet | Entering the iron age: The first general method for iron‐catalyzed monocarbonylation of alkynes has been developed. A range of structurally diverse cinnamides... |
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| SubjectTerms | acrylamides Alkynes carbonylation Chemistry Chemistry, Multidisciplinary cinnamides homogeneous catalysis iron Physical Sciences Science & Technology |
| Title | General and Selective Iron-Catalyzed Aminocarbonylation of Alkynes: Synthesis of Acryl- and Cinnamides |
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