Completely Solvent-free Protocols to Access Phase-Pure, Metastable Metal Halide Perovskites and Functional Photodetectors from the Precursor Salts
Mechanochemistry is a green, solid-state, re-emerging synthetic technique that can rapidly form complex molecules and materials without exogenous heat or solvent(s). Herein, we report the application of solvent-free mechanochemical ball milling for the synthesis of metal halide perovskites, to overc...
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| Published in | iScience Vol. 16; pp. 312 - 325 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier
28.06.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Mechanochemistry is a green, solid-state, re-emerging synthetic technique that can rapidly form complex molecules and materials without exogenous heat or solvent(s). Herein, we report the application of solvent-free mechanochemical ball milling for the synthesis of metal halide perovskites, to overcome problems with solution-based syntheses. We prepared phase-pure, air-sensitive CsSnX
(X = I, Br, Cl) and its mixed halide perovskites by mechanochemistry for the first time by reactions between cesium and tin(II) halides. Notably, we report the sole examples where metastable, high-temperature phases like cubic CsSnCl
, cubic CsPbI
, and trigonal FAPbI
were accessible at ambient temperatures and pressures without post-synthetic processing. The perovskites can be prepared up to "kilogram scales." Lead-free, all-inorganic photodetector devices were fabricated using the mechanosynthesized CsSnBr
Cl
under solvent-free conditions and showed 10-fold differences between on-off currents. We highlight an essentially solvent-free, general approach to synthesize metastable compounds and fabricate photodetectors from commercially available precursors. |
|---|---|
| AbstractList | Mechanochemistry is a green, solid-state, re-emerging synthetic technique that can rapidly form complex molecules and materials without exogenous heat or solvent(s). Herein, we report the application of solvent-free mechanochemical ball milling for the synthesis of metal halide perovskites, to overcome problems with solution-based syntheses. We prepared phase-pure, air-sensitive CsSnX
(X = I, Br, Cl) and its mixed halide perovskites by mechanochemistry for the first time by reactions between cesium and tin(II) halides. Notably, we report the sole examples where metastable, high-temperature phases like cubic CsSnCl
, cubic CsPbI
, and trigonal FAPbI
were accessible at ambient temperatures and pressures without post-synthetic processing. The perovskites can be prepared up to "kilogram scales." Lead-free, all-inorganic photodetector devices were fabricated using the mechanosynthesized CsSnBr
Cl
under solvent-free conditions and showed 10-fold differences between on-off currents. We highlight an essentially solvent-free, general approach to synthesize metastable compounds and fabricate photodetectors from commercially available precursors. Mechanochemistry is a green, solid-state, re-emerging synthetic technique that can rapidly form complex molecules and materials without exogenous heat or solvent(s). Herein, we report the application of solvent-free mechanochemical ball milling for the synthesis of metal halide perovskites, to overcome problems with solution-based syntheses. We prepared phase-pure, air-sensitive CsSnX3 (X = I, Br, Cl) and its mixed halide perovskites by mechanochemistry for the first time by reactions between cesium and tin(II) halides. Notably, we report the sole examples where metastable, high-temperature phases like cubic CsSnCl3, cubic CsPbI3, and trigonal FAPbI3 were accessible at ambient temperatures and pressures without post-synthetic processing. The perovskites can be prepared up to “kilogram scales.” Lead-free, all-inorganic photodetector devices were fabricated using the mechanosynthesized CsSnBr1.5Cl1.5 under solvent-free conditions and showed 10-fold differences between on-off currents. We highlight an essentially solvent-free, general approach to synthesize metastable compounds and fabricate photodetectors from commercially available precursors. : Devices; Energy Materials; Materials Synthesis Subject Areas: Devices, Energy Materials, Materials Synthesis Mechanochemistry is a green, solid-state, re-emerging synthetic technique that can rapidly form complex molecules and materials without exogenous heat or solvent(s). Herein, we report the application of solvent-free mechanochemical ball milling for the synthesis of metal halide perovskites, to overcome problems with solution-based syntheses. We prepared phase-pure, air-sensitive CsSnX 3 (X = I, Br, Cl) and its mixed halide perovskites by mechanochemistry for the first time by reactions between cesium and tin(II) halides. Notably, we report the sole examples where metastable, high-temperature phases like cubic CsSnCl 3 , cubic CsPbI 3 , and trigonal FAPbI 3 were accessible at ambient temperatures and pressures without post-synthetic processing. The perovskites can be prepared up to “kilogram scales.” Lead-free, all-inorganic photodetector devices were fabricated using the mechanosynthesized CsSnBr 1.5 Cl 1.5 under solvent-free conditions and showed 10-fold differences between on-off currents. We highlight an essentially solvent-free, general approach to synthesize metastable compounds and fabricate photodetectors from commercially available precursors. • Mechanochemistry provided a solvent-free perovskite and device fabrication process • Direct access to metastable phases of perovskites without post-synthetic annealing • Energy- and time-efficient synthetic protocol demonstrated up to kilogram scales • Procedures applicable for lead-based, air-sensitive tin(II), and other perovskites Devices; Energy Materials; Materials Synthesis |
| Author | Hong, Zonghan Tay, Yong Kang Eugene Ho, Yan King Terence Sum, Tze Chien García, Felipe Zhao, Xin Tan, Davin John, Rohit Abraham Soo, Han Sen Mathews, Nripan |
| AuthorAffiliation | 1 Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore 5 Solar Fuels Laboratory, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore 2 School of Materials Science and Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore 3 Division of Physics and Applied Physics, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore 4 Energy Research Institute @NTU (ERI@N), Research Techno Plaza, X-Frontier Block, Level 5, 50 Nanyang Drive, Singapore 637553, Singapore |
| AuthorAffiliation_xml | – name: 2 School of Materials Science and Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore – name: 3 Division of Physics and Applied Physics, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – name: 5 Solar Fuels Laboratory, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore – name: 1 Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – name: 4 Energy Research Institute @NTU (ERI@N), Research Techno Plaza, X-Frontier Block, Level 5, 50 Nanyang Drive, Singapore 637553, Singapore |
| Author_xml | – sequence: 1 givenname: Zonghan surname: Hong fullname: Hong, Zonghan organization: Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – sequence: 2 givenname: Davin surname: Tan fullname: Tan, Davin organization: Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – sequence: 3 givenname: Rohit Abraham surname: John fullname: John, Rohit Abraham organization: School of Materials Science and Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore – sequence: 4 givenname: Yong Kang Eugene surname: Tay fullname: Tay, Yong Kang Eugene organization: Division of Physics and Applied Physics, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – sequence: 5 givenname: Yan King Terence surname: Ho fullname: Ho, Yan King Terence organization: Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – sequence: 6 givenname: Xin surname: Zhao fullname: Zhao, Xin organization: Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – sequence: 7 givenname: Tze Chien surname: Sum fullname: Sum, Tze Chien organization: Division of Physics and Applied Physics, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore – sequence: 8 givenname: Nripan surname: Mathews fullname: Mathews, Nripan email: ERI@N, nripan@ntu.edu.sg organization: School of Materials Science and Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore; Energy Research Institute @NTU (ERI@N), Research Techno Plaza, X-Frontier Block, Level 5, 50 Nanyang Drive, Singapore 637553, Singapore. Electronic address: nripan@ntu.edu.sg – sequence: 9 givenname: Felipe surname: García fullname: García, Felipe email: fgarcia@ntu.edu.sg organization: Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore. Electronic address: fgarcia@ntu.edu.sg – sequence: 10 givenname: Han Sen surname: Soo fullname: Soo, Han Sen email: hansen@ntu.edu.sg organization: Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore; Solar Fuels Laboratory, Nanyang Technological University, 50 Nanyang Avenue, Singapore 639798, Singapore. Electronic address: hansen@ntu.edu.sg |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31203187$$D View this record in MEDLINE/PubMed |
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