Microstructure evolution and mechanical properties of rheo-squeeze casting AZ91-Ca alloy during heat treatment

The rheo-squeeze casting(RSC)process is a newly-developed casting process for high-performance components.In order to further improve the mechanical properties of magnesium alloys,AZ91-2wt.%Ca(AZX912)alloy was prepared by the RSC process and then subjected to heat treatment.The microstructure evolut...

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Published inChina foundry Vol. 14; no. 6; pp. 485 - 491
Main Authors Zhang, Yang, Li, Xiao-ping, Sun, Shun-ping, Lu, Ya-lin, Wu, Guo-hua
Format Journal Article
LanguageEnglish
Published Singapore Springer Singapore 01.11.2017
Foundry Journal Agency
School of Materials Engineering, Jiangsu University of Technology, Changzhou 213001, China%National Engineering Research Center of Light Alloy Net Forming, Shanghai Jiao Tong University, Shanghai 200240, China
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Abstract The rheo-squeeze casting(RSC)process is a newly-developed casting process for high-performance components.In order to further improve the mechanical properties of magnesium alloys,AZ91-2wt.%Ca(AZX912)alloy was prepared by the RSC process and then subjected to heat treatment.The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated.It was found that during solid solution treatment at 410°C,β-Mg_(17)Al_(12) phase with low melting point dissolves intoα-Mg matrix,while the connected network-like Al_2Ca phase with high melting point tends to separate gradually,and the tips of Al_2Ca phase is partially spheroidized.With the increase of solid solution time,the yield strength(YS)of AZX912 alloy decreases gradually while the ultimate tensile strength(UTS)and elongation to failure(E_f)increase continuously.Isothermal ageing at 225°C promotes the precipitation ofβ-Mg_(17)Al_(12) phase in the matrix of AZX912 alloy.The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%.The precipitation ofβ-Mg_(17)Al_(12) phase during ageing treatment is beneficial to YS but harmful to E_f.The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
AbstractList The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the mechanical properties of magnesium alloys, AZ91-2wt.%Ca (AZX912) alloy was prepared by the RSC process and then subjected to heat treatment. The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated. It was found that during solid solution treatment at 410 °C, β-Mg 17 Al 12 phase with low melting point dissolves into α-Mg matrix, while the connected network-like Al 2 Ca phase with high melting point tends to separate gradually, and the tips of Al 2 Ca phase is partially spheroidized. With the increase of solid solution time, the yield strength (YS) of AZX912 alloy decreases gradually while the ultimate tensile strength (UTS) and elongation to failure (E f ) increase continuously. Isothermal ageing at 225 °C promotes the precipitation of β-Mg 17 Al 12 phase in the matrix of AZX912 alloy. The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%. The precipitation of β-Mg 17 Al 12 phase during ageing treatment is beneficial to YS but harmful to E f . The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the mechanical properties of magnesium alloys, AZ91-2wt.%Ca (AZX912) alloy was prepared by the RSC process and then subjected to heat treatment. The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated. It was found that during solid solution treatment at 410 [degrees]C, [beta]-[Mg.sub.17][Al.sub.12] phase with low melting point dissolves into a-Mg matrix, while the connected network-like [Al.sub.2]Ca phase with high melting point tends to separate gradually, and the tips of [Al.sub.2]Ca phase is partially spheroidized. With the increase of solid solution time, the yield strength (YS) of AZX912 alloy decreases gradually while the ultimate tensile strength (UTS) and elongation to failure ([E.sub.f]) increase continuously. Isothermal ageing at 225 [degrees]C promotes the precipitation of [beta]-[Mg.sub.17][Al.sub.12] phase in the matrix of AZX912 alloy. The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%. The precipitation of [beta]-[Mg.sub.17][Al.sub.12] phase during ageing treatment is beneficial to YS but harmful to [E.sub.f]. The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
The rheo-squeeze casting(RSC)process is a newly-developed casting process for high-performance components.In order to further improve the mechanical properties of magnesium alloys,AZ91-2wt.%Ca(AZX912)alloy was prepared by the RSC process and then subjected to heat treatment.The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated.It was found that during solid solution treatment at 410°C,β-Mg_(17)Al_(12) phase with low melting point dissolves intoα-Mg matrix,while the connected network-like Al_2Ca phase with high melting point tends to separate gradually,and the tips of Al_2Ca phase is partially spheroidized.With the increase of solid solution time,the yield strength(YS)of AZX912 alloy decreases gradually while the ultimate tensile strength(UTS)and elongation to failure(E_f)increase continuously.Isothermal ageing at 225°C promotes the precipitation ofβ-Mg_(17)Al_(12) phase in the matrix of AZX912 alloy.The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%.The precipitation ofβ-Mg_(17)Al_(12) phase during ageing treatment is beneficial to YS but harmful to E_f.The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the mechanical properties of magnesium alloys, AZ91-2wt.%Ca (AZX912) alloy was prepared by the RSC process and then subjected to heat treatment. The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated. It was found that during solid solution treatment at 410 [degrees]C, [beta]-[Mg.sub.17][Al.sub.12] phase with low melting point dissolves into a-Mg matrix, while the connected network-like [Al.sub.2]Ca phase with high melting point tends to separate gradually, and the tips of [Al.sub.2]Ca phase is partially spheroidized. With the increase of solid solution time, the yield strength (YS) of AZX912 alloy decreases gradually while the ultimate tensile strength (UTS) and elongation to failure ([E.sub.f]) increase continuously. Isothermal ageing at 225 [degrees]C promotes the precipitation of [beta]-[Mg.sub.17][Al.sub.12] phase in the matrix of AZX912 alloy. The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%. The precipitation of [beta]-[Mg.sub.17][Al.sub.12] phase during ageing treatment is beneficial to YS but harmful to [E.sub.f]. The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed. Key words: magnesium alloys; semisolid processing; heat treatment; microstructure; mechanical properties CLC numbers: TG146.22 Document code: A Article ID: 1672-6421(2017)06-485-07
The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the mechanical properties of magnesium alloys, AZ91-2wt.%Ca (AZX912) alloy was prepared by the RSC process and then subjected to heat treatment. The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated. It was found that during solid solution treatment at 410 °C, β-Mg17Al12 phase with low melting point dissolves into α-Mg matrix, while the connected network-like Al2Ca phase with high melting point tends to separate gradually, and the tips of Al2Ca phase is partially spheroidized. With the increase of solid solution time, the yield strength (YS) of AZX912 alloy decreases gradually while the ultimate tensile strength (UTS) and elongation to failure (Ef) increase continuously. Isothermal ageing at 225 °C promotes the precipitation of β-Mg17Al12 phase in the matrix of AZX912 alloy. The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%. The precipitation of β-Mg17Al12 phase during ageing treatment is beneficial to YS but harmful to Ef. The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
TG146.22; The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the mechanical properties of magnesium alloys, AZ91-2wt.%Ca (AZX912) alloy was prepared by the RSC process and then subjected to heat treatment. The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated. It was found that during solid solution treatment at 410℃, β-Mg17Al12 phase with low melting point dissolves into α-Mg matrix, while the connected network-like Al2Ca phase with high melting point tends to separate gradually, and the tips of Al2Ca phase is partially spheroidized. With the increase of solid solution time, the yield strength (YS) of AZX912 alloy decreases gradually while the ultimate tensile strength (UTS) and elongation to failure (Ef) increase continuously. Isothermal ageing at 225 ℃ promotes the precipitation of β-Mg17Al12 phase in the matrix of AZX912 alloy. The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%. The precipitation of β-Mg17Al12 phase during ageing treatment is beneficial to YS but harmful to Ef. The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
Audience Academic
Author Yang Zhang;Xiao-ping Li;Shun-ping Sun;Ya-lin Lu;Guo-hua Wu
AuthorAffiliation ehool of Materials Engineering, Jiangsu University of Technology, Changzhou 213001, China;National Engineering Research Center of Light Alloy Net Forming, Shanghai Jiao Tong University, Shanghai 200240, China
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CitedBy_id crossref_primary_10_1007_s40962_021_00575_x
crossref_primary_10_1088_1757_899X_838_1_012012
crossref_primary_10_1016_j_matdes_2020_108990
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ClassificationCodes TG146.22
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Issue 6
Keywords A
magnesium alloys
microstructure
semisolid processing
heat treatment
mechanical properties
TG146.22
Language English
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Notes 21-1498/TG
The rheo-squeeze casting(RSC)process is a newly-developed casting process for high-performance components.In order to further improve the mechanical properties of magnesium alloys,AZ91-2wt.%Ca(AZX912)alloy was prepared by the RSC process and then subjected to heat treatment.The microstructure evolution and mechanical properties of AZX912 alloy during heat treatment were investigated.It was found that during solid solution treatment at 410°C,β-Mg_(17)Al_(12) phase with low melting point dissolves intoα-Mg matrix,while the connected network-like Al_2Ca phase with high melting point tends to separate gradually,and the tips of Al_2Ca phase is partially spheroidized.With the increase of solid solution time,the yield strength(YS)of AZX912 alloy decreases gradually while the ultimate tensile strength(UTS)and elongation to failure(E_f)increase continuously.Isothermal ageing at 225°C promotes the precipitation ofβ-Mg_(17)Al_(12) phase in the matrix of AZX912 alloy.The hardness reaches the peak after ageing for 96 h and the increase in hardness is about 24.8%.The precipitation ofβ-Mg_(17)Al_(12) phase during ageing treatment is beneficial to YS but harmful to E_f.The mechanism of microstructure evolution during heat treatment and its effect on mechanical properties are discussed.
magnesium alloys; semisolid processing; heat treatment; microstructure; mechanical properties
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Snippet The rheo-squeeze casting(RSC)process is a newly-developed casting process for high-performance components.In order to further improve the mechanical properties...
The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the mechanical...
TG146.22; The rheo-squeeze casting (RSC) process is a newly-developed casting process for high-performance components. In order to further improve the...
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SubjectTerms Alloys
Casting (Metal)
Engineering
Hardness (Materials)
heat treatment
Machines
Magnesium alloys
Manufacturing
Materials Engineering
Mechanical properties
Metallic Materials
Metals (Materials)
microstructure
Precipitation (Meteorology)
Processes
Research & Development
semisolid processing
Specialty metals industry
Title Microstructure evolution and mechanical properties of rheo-squeeze casting AZ91-Ca alloy during heat treatment
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Volume 14
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