Evaluating the Effect of Severe Plastic Deformation: High-Pressure Torsion and High-Pressure Sliding in Grade 2 Titanium

This study investigates the effects of severe plastic deformation (SPD) techniques, particularly high-pressure torsion (HPT) and high-pressure sliding (HPS), on the microstructural evolution and mechanical properties of commercially pure (Grade 2) Ti. The experiments were conducted under pressures o...

Full description

Saved in:
Bibliographic Details
Published inMATERIALS TRANSACTIONS Vol. 66; no. 5; pp. 569 - 576
Main Authors Gonzalez-Hernandez, Joaquín E., González-Jiménez, Kathy A., Takizawa, Yoichi, Yumoto, Manabu, Cubero-Sesin, Jorge M., Horita, Zenji
Format Journal Article
LanguageEnglish
Published Sendai The Japan Institute of Metals and Materials 01.05.2025
公益社団法人 日本金属学会
Japan Science and Technology Agency
Subjects
Biomedical materials
Crystallography
Deformation effects
Diamond pyramid hardness
High pressure
high-pressure sliding
High-pressure torsion
Material properties
Mechanical properties
Microstructure
omega phase transformation
Phase transitions
Plastic deformation
pure titanium
Severe plastic deformation
Sliding
Tensile tests
Online AccessGet full text
ISSN1345-9678
1347-5320
DOI10.2320/matertrans.MT-MC2024018

Cover

Abstract This study investigates the effects of severe plastic deformation (SPD) techniques, particularly high-pressure torsion (HPT) and high-pressure sliding (HPS), on the microstructural evolution and mechanical properties of commercially pure (Grade 2) Ti. The experiments were conducted under pressures of 2, 5, and 6 GPa. For the crystallographic analyses, X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used. Nanostructured Ti was obtained after processing by HPT and HPS, and the phase transformation from alpha (α) to omega (ω) phase was confirmed under pressures of 5 and 6 GPa. Vickers microhardness and tensile tests confirmed that HPT-processed samples exhibited increased strength under higher pressures, while the HPS process produced more homogenous material properties, along with a promising strength-to-ductility ratio. These findings indicate that the HPS process may offer better control over microstructure and mechanical performance, making it a promising technique to enhance the mechanical properties of pure Ti for biomedical applications.
AbstractList This study investigates the effects of severe plastic deformation (SPD) techniques, particularly high-pressure torsion (HPT) and high-pressure sliding (HPS), on the microstructural evolution and mechanical properties of commercially pure (Grade 2) Ti. The experiments were conducted under pressures of 2, 5, and 6 GPa. For the crystallographic analyses, X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used. Nanostructured Ti was obtained after processing by HPT and HPS, and the phase transformation from alpha (α) to omega (ω) phase was confirmed under pressures of 5 and 6 GPa. Vickers microhardness and tensile tests confirmed that HPT-processed samples exhibited increased strength under higher pressures, while the HPS process produced more homogenous material properties, along with a promising strength-to-ductility ratio. These findings indicate that the HPS process may offer better control over microstructure and mechanical performance, making it a promising technique to enhance the mechanical properties of pure Ti for biomedical applications.Fig. 9 Comparison of yield strength vs. elongation to failure of data obtained in this study with those reported by Valiev et al. [67]. (online color)
This study investigates the effects of severe plastic deformation (SPD) techniques, particularly high-pressure torsion (HPT) and high-pressure sliding (HPS), on the microstructural evolution and mechanical properties of commercially pure (Grade 2) Ti. The experiments were conducted under pressures of 2, 5, and 6 GPa. For the crystallographic analyses, X-ray diffraction (XRD) and transmission electron microscopy (TEM) were used. Nanostructured Ti was obtained after processing by HPT and HPS, and the phase transformation from alpha (α) to omega (ω) phase was confirmed under pressures of 5 and 6 GPa. Vickers microhardness and tensile tests confirmed that HPT-processed samples exhibited increased strength under higher pressures, while the HPS process produced more homogenous material properties, along with a promising strength-to-ductility ratio. These findings indicate that the HPS process may offer better control over microstructure and mechanical performance, making it a promising technique to enhance the mechanical properties of pure Ti for biomedical applications.
ArticleNumber MT-MC2024018
Author González-Jiménez, Kathy A.
Takizawa, Yoichi
Gonzalez-Hernandez, Joaquín E.
Cubero-Sesin, Jorge M.
Yumoto, Manabu
Horita, Zenji
Author_xml – sequence: 1
  fullname: Gonzalez-Hernandez, Joaquín E.
  organization: Centro de Investigación y Extensión en Materiales (CIEMTEC), Escuela de Ciencia e ingeniería de los Materiales, Instituto Tecnológico de Costa Rica
– sequence: 1
  fullname: González-Jiménez, Kathy A.
  organization: Centro de Investigación y Extensión en Materiales (CIEMTEC), Escuela de Ciencia e ingeniería de los Materiales, Instituto Tecnológico de Costa Rica
– sequence: 1
  fullname: Takizawa, Yoichi
  organization: Technology Department, Nagano Forging Co., Ltd
– sequence: 1
  fullname: Yumoto, Manabu
  organization: Technology Department, Nagano Forging Co., Ltd
– sequence: 1
  fullname: Cubero-Sesin, Jorge M.
  organization: Centro de Investigación y Extensión en Materiales (CIEMTEC), Escuela de Ciencia e ingeniería de los Materiales, Instituto Tecnológico de Costa Rica
– sequence: 1
  fullname: Horita, Zenji
  organization: Synchrotron Light Application Center, Saga University
BackLink https://cir.nii.ac.jp/crid/1390303233089873024$$DView record in CiNii
BookMark eNpdkN1u1DAQhS1UJPr3DFiC2xTb48QOd2hZWqSuWqnh2nKdya5XWafYTlXeHi-LloqbmdH4m3Pkc0ZOwhSQkPecXQkQ7NPOZow52pCuVl21WggmJOP6DTnlIFVVF-bkz1xXbaP0O3KW0pYxULUQp-Rl-WzH2WYf1jRvkC6HAV2m00Af8Bkj0vvRpuwd_YrDFIuXn8JneuPXm-o-YkpzQbopprKmNvT_vTyMvt8r-0Cvo-2RCtr5bIOfdxfk7WDHhJd_-zn58W3ZLW6q27vr74svt5WrgeeqFmCh4UxZjuVXjXBtX1uteK9QQtMPUssGtawF0xwG6XrpVMuklNgI_qjhnHw46D7F6eeMKZvtNMdQLA0IrlXJirNCqQPl4pRSxME8Rb-z8ZfhzOxjNv9iNqvOHGMulx8Pl8F74_y-cmgZMBAATLdaQSELtjpg25TtGo_yNpZwR3wt3zSm3pfXNkfObWw0GOA3IkCbUA
Cites_doi 10.1557/JMR.2002.0002
10.1016/j.msea.2004.01.096
10.1007/s10853-013-7988-z
10.1146/annurev-matsci-081720-123248
10.1016/j.msea.2016.05.105
10.1134/S0031918X20040055
10.1134/S1029959920030029
10.1088/1742-6596/240/1/012113
10.2320/matertrans.MT-MF2022043
10.2320/matertrans.MT-MF2022031
10.1016/j.msea.2016.05.001
10.2320/matertrans.MT-MF2022059
10.1007/s10853-017-0916-x
10.1016/j.jallcom.2014.12.159
10.1007/s11661-010-0400-6
10.1007/s11661-021-06347-w
10.2320/matertrans.MT-MF2022025
10.2320/matertrans.MT-MF2022041
10.2320/matertrans.MT-MF2022046
10.2320/matertrans.MT-LA2022032
10.1016/j.mtla.2020.100916
10.2320/matertrans.MT-MF2022045
10.1016/j.msec.2005.08.032
10.5772/intechopen.84991
10.1088/1757-899X/1213/1/012003
10.1038/nmat1292
10.1016/j.pmatsci.2008.03.002
10.2320/matertrans.MT-MF2022056
10.2320/matertrans.MT-MF2022036
10.2320/matertrans.MT-MF2022014
10.1007/s11661-009-9890-5
10.2320/matertrans.MT-MF2022004
10.1016/j.msec.2019.04.064
10.2320/matertrans.MF201923
10.2320/matertrans.MT-LA2022054
10.1504/IJNBM.2007.016517
10.2320/matertrans.MT-MF2022039
10.1557/JMR.1996.0239
10.2320/matertrans.MT-L2023022
10.2320/matertrans.MT-M2020314
10.1016/j.actamat.2014.01.037
10.2320/matertrans.MT-MF2022048
10.3390/ma16020587
10.2320/matertrans.MA201325
10.2320/matertrans.MT-MF2022040
10.2320/matertrans.MT-MF2022019
10.1016/B978-0-12-812456-7.00001-9
10.2320/matertrans.MT-MF2022047
10.2320/matertrans.M2009431
10.1103/PhysRev.48.825
10.2320/matertrans.ME201924
10.1002/adem.202400282
10.1016/j.msea.2014.07.030
10.1016/j.msea.2015.11.074
10.3139/146.101606
10.2320/matertrans.MT-M2020074
10.3139/146.110224
10.1016/j.msea.2014.04.014
10.1016/j.kijoms.2017.08.005
10.1007/978-3-030-48122-3_1
10.2320/matertrans.MRP2008445
10.1016/B978-0-12-814599-9.00001-8
10.1016/0921-5093(96)10243-4
10.1007/s11837-017-2672-4
10.3390/ma13040967
10.1016/j.msea.2020.140687
10.2320/matertrans.MT-MF2022034
10.1007/s11837-016-1820-6
10.1016/j.apsusc.2018.04.120
ContentType Journal Article
Copyright 2025 The Japan Institute of Metals and Materials
Copyright Japan Science and Technology Agency 2025
Copyright_xml – notice: 2025 The Japan Institute of Metals and Materials
– notice: Copyright Japan Science and Technology Agency 2025
DBID RYH
AAYXX
CITATION
7SR
8BQ
8FD
JG9
DOI 10.2320/matertrans.MT-MC2024018
DatabaseName CiNii Complete
CrossRef
Engineered Materials Abstracts
METADEX
Technology Research Database
Materials Research Database
DatabaseTitle CrossRef
Materials Research Database
Engineered Materials Abstracts
Technology Research Database
METADEX
DatabaseTitleList Materials Research Database
DeliveryMethod fulltext_linktorsrc
Discipline Engineering
EISSN 1347-5320
EndPage 576
ExternalDocumentID 10_2320_matertrans_MT_MC2024018
article_matertrans_66_5_66_MT_MC2024018_article_char_en
GroupedDBID -~X
.L7
.LE
5GY
93D
ABJNI
ACGFS
ACIWK
ADMLS
AENEX
ALMA_UNASSIGNED_HOLDINGS
CS3
DU5
JSI
JSP
RJT
RZJ
SJN
RYH
AAYXX
CITATION
7SR
8BQ
8FD
JG9
ID FETCH-LOGICAL-c531t-523a36107a1e01862c9d5a871d7e436df4846e84520813f4cd4c790444e621b83
ISSN 1345-9678
IngestDate Mon Jun 30 07:24:53 EDT 2025
Sun Jul 06 05:05:14 EDT 2025
Fri Jun 27 01:02:31 EDT 2025
Wed Sep 03 06:30:36 EDT 2025
IsDoiOpenAccess false
IsOpenAccess true
IsPeerReviewed true
IsScholarly true
Issue 5
Language English
LinkModel OpenURL
MergedId FETCHMERGED-LOGICAL-c531t-523a36107a1e01862c9d5a871d7e436df4846e84520813f4cd4c790444e621b83
Notes ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 14
OpenAccessLink https://doi.org/10.2320/matertrans.mt-mc2024018
PQID 3218740110
PQPubID 1976393
PageCount 8
ParticipantIDs proquest_journals_3218740110
crossref_primary_10_2320_matertrans_MT_MC2024018
nii_cinii_1390303233089873024
jstage_primary_article_matertrans_66_5_66_MT_MC2024018_article_char_en
PublicationCentury 2000
PublicationDate 2025-05-01
PublicationDateYYYYMMDD 2025-05-01
PublicationDate_xml – month: 05
  year: 2025
  text: 2025-05-01
  day: 01
PublicationDecade 2020
PublicationPlace Sendai
PublicationPlace_xml – name: Sendai
PublicationTitle MATERIALS TRANSACTIONS
PublicationTitleAlternate Mater. Trans.
PublicationTitle_FL MATERIALS TRANSACTIONS
Mater. Trans
PublicationYear 2025
Publisher The Japan Institute of Metals and Materials
公益社団法人 日本金属学会
Japan Science and Technology Agency
Publisher_xml – name: The Japan Institute of Metals and Materials
– name: 公益社団法人 日本金属学会
– name: Japan Science and Technology Agency
References 44
45
46
47
48
49
50
51
52
53
10
54
11
55
12
56
13
57
14
58
15
59
16
17
18
19
1
2
3
4
5
6
7
8
9
60
61
62
63
20
64
21
65
22
66
23
67
24
68
25
69
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
References_xml – ident: 67
  doi: 10.1557/JMR.2002.0002
– ident: 26
  doi: 10.1016/j.msea.2004.01.096
– ident: 61
  doi: 10.1007/s10853-013-7988-z
– ident: 15
  doi: 10.1146/annurev-matsci-081720-123248
– ident: 13
  doi: 10.1016/j.msea.2016.05.105
– ident: 10
  doi: 10.1134/S0031918X20040055
– ident: 16
  doi: 10.1134/S1029959920030029
– ident: 6
  doi: 10.1088/1742-6596/240/1/012113
– ident: 45
  doi: 10.2320/matertrans.MT-MF2022043
– ident: 51
  doi: 10.2320/matertrans.MT-MF2022031
– ident: 55
  doi: 10.1016/j.msea.2016.05.001
– ident: 36
  doi: 10.2320/matertrans.MT-MF2022059
– ident: 37
  doi: 10.1007/s10853-017-0916-x
– ident: 54
  doi: 10.1016/j.jallcom.2014.12.159
– ident: 66
  doi: 10.1007/s11661-010-0400-6
– ident: 27
  doi: 10.1007/s11661-021-06347-w
– ident: 31
  doi: 10.2320/matertrans.MT-MF2022025
– ident: 48
  doi: 10.2320/matertrans.MT-MF2022041
– ident: 42
  doi: 10.2320/matertrans.MT-MF2022046
– ident: 20
  doi: 10.2320/matertrans.MT-LA2022032
– ident: 28
  doi: 10.1016/j.mtla.2020.100916
– ident: 41
  doi: 10.2320/matertrans.MT-MF2022045
– ident: 1
  doi: 10.1016/j.msec.2005.08.032
– ident: 7
  doi: 10.5772/intechopen.84991
– ident: 23
  doi: 10.1088/1757-899X/1213/1/012003
– ident: 57
  doi: 10.1038/nmat1292
– ident: 21
  doi: 10.1016/j.pmatsci.2008.03.002
– ident: 43
  doi: 10.2320/matertrans.MT-MF2022056
– ident: 39
  doi: 10.2320/matertrans.MT-MF2022036
– ident: 32
  doi: 10.2320/matertrans.MT-MF2022014
– ident: 52
  doi: 10.1007/s11661-009-9890-5
– ident: 47
  doi: 10.2320/matertrans.MT-MF2022004
– ident: 4
  doi: 10.1016/j.msec.2019.04.064
– ident: 53
  doi: 10.2320/matertrans.MF201923
– ident: 69
  doi: 10.2320/matertrans.MT-LA2022054
– ident: 8
  doi: 10.1504/IJNBM.2007.016517
– ident: 46
  doi: 10.2320/matertrans.MT-MF2022039
– ident: 60
  doi: 10.1557/JMR.1996.0239
– ident: 59
  doi: 10.2320/matertrans.MT-L2023022
– ident: 22
  doi: 10.2320/matertrans.MT-M2020314
– ident: 62
  doi: 10.1016/j.actamat.2014.01.037
– ident: 40
  doi: 10.2320/matertrans.MT-MF2022048
– ident: 24
  doi: 10.3390/ma16020587
– ident: 35
  doi: 10.2320/matertrans.MA201325
– ident: 44
  doi: 10.2320/matertrans.MT-MF2022040
– ident: 50
  doi: 10.2320/matertrans.MT-MF2022019
– ident: 2
  doi: 10.1016/B978-0-12-812456-7.00001-9
– ident: 18
  doi: 10.2320/matertrans.MT-MF2022047
– ident: 65
  doi: 10.2320/matertrans.M2009431
– ident: 17
  doi: 10.1103/PhysRev.48.825
– ident: 30
  doi: 10.2320/matertrans.ME201924
– ident: 38
  doi: 10.1002/adem.202400282
– ident: 64
  doi: 10.1016/j.msea.2014.07.030
– ident: 25
  doi: 10.1016/j.msea.2015.11.074
– ident: 56
  doi: 10.3139/146.101606
– ident: 29
  doi: 10.2320/matertrans.MT-M2020074
– ident: 63
  doi: 10.3139/146.110224
– ident: 68
  doi: 10.1016/j.msea.2014.04.014
– ident: 9
  doi: 10.1016/j.kijoms.2017.08.005
– ident: 14
  doi: 10.1007/978-3-030-48122-3_1
– ident: 19
  doi: 10.2320/matertrans.MRP2008445
– ident: 33
  doi: 10.1016/B978-0-12-814599-9.00001-8
– ident: 5
  doi: 10.1016/0921-5093(96)10243-4
– ident: 58
  doi: 10.1007/s11837-017-2672-4
– ident: 3
  doi: 10.3390/ma13040967
– ident: 34
  doi: 10.1016/j.msea.2020.140687
– ident: 49
  doi: 10.2320/matertrans.MT-MF2022034
– ident: 12
  doi: 10.1007/s11837-016-1820-6
– ident: 11
  doi: 10.1016/j.apsusc.2018.04.120
SSID ssj0037522
Score 2.4357333
Snippet This study investigates the effects of severe plastic deformation (SPD) techniques, particularly high-pressure torsion (HPT) and high-pressure sliding (HPS),...
SourceID proquest
crossref
nii
jstage
SourceType Aggregation Database
Index Database
Publisher
StartPage 569
SubjectTerms Biomedical materials
Crystallography
Deformation effects
Diamond pyramid hardness
High pressure
high-pressure sliding
High-pressure torsion
Material properties
Mechanical properties
Microstructure
omega phase transformation
Phase transitions
Plastic deformation
pure titanium
Severe plastic deformation
Sliding
Tensile tests
Title Evaluating the Effect of Severe Plastic Deformation: High-Pressure Torsion and High-Pressure Sliding in Grade 2 Titanium
URI https://www.jstage.jst.go.jp/article/matertrans/66/5/66_MT-MC2024018/_article/-char/en
https://cir.nii.ac.jp/crid/1390303233089873024
https://www.proquest.com/docview/3218740110
Volume 66
hasFullText 1
inHoldings 1
isFullTextHit
isPrint
ispartofPNX MATERIALS TRANSACTIONS, 2025/05/01, Vol.66(5), pp.569-576
link http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwrV1Nb9MwGLb2wQEOiE9R2JAP3KqUxnbihFu0dSvVsgPNpHGK8uGIIJbASAX01_O-sZOmAySYuFiRY1dOnqf2Y-f9IOSVzTDCh8ctd5opS9gytTwlYc_joRr3WGFn6JwcnrvzC7G4dC53dkcDq6VVk06y9W_9Sm6DKtQBrugl-w_I9j8KFXAN-EIJCEP5VxjPTKhu4_FkIhGjG4qCZ1GYkQjDMMOk0vso4gkA2nZY2i8QGkV1e2LWfkXYvrP8VHYuL6fXSY5HtVEJYrI04Ru6RFABSOK3wdlyHL0LzpfaLKXXmKd1tYZFaG3NhyfWizr5smo_0h9X49lk2LittbHHorzS3_Er3QktP36Mg751BOp3nXxr5e_7usw-lP0ctgIG1toXqUrS1fBsgzkbS8JJ7x0HmqHatpwIVYOhpbUhSqPhHEzhXDiW7-rEQBPV1UkLU2AM532d7cXw2xlM4o5OHmP0gKPz09xcakCJom3mFQ6gaWVFGFnhEcOYcWZF2Y7jbVgSb3rErhs7WIRR3PeMu3bodQck3yX7TEq0QNgPjsOzZSczuNSh8PvH1caLOKzXfxjUlvS68xF2HxhWYrcqy1-ESKuuogfkvtkW0UCP6iHZUdUjcm8QLPMx-b5hOwW2U812WhdUs50attMB29_QLUZTw3UKoN64Y7hOy4q2XKeMdlx_Qi5OZtHR3DJ5Q6wMVpQGz1YSDtsCmdgKHttlmZ87iSftXCrB3bwQILqVJxwGepgXIstFJn0MnKhcZqcef0r2qrpSzwgVgqc89XNVJImQzEvldJoX0il8j8nUT0dk2r3S-LMODxPDthpRGAI9BHhETvSr7zvckhkjcgjQxVmJJWzkYLnmjPOp53uwbDMxIgcdqLGZtL7GnOkknPb0-f8axwtyd_PfPSB7zfVKHYJSb9KXhrM_AVm264A
linkProvider EBSCOhost
openUrl ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Evaluating+the+Effect+of+Severe+Plastic+Deformation%3A+High-Pressure+Torsion+and+High-Pressure+Sliding+in+Grade+2+Titanium&rft.jtitle=MATERIALS+TRANSACTIONS&rft.au=Gonzalez-Hernandez%2C+Joaqu%C3%ADn+E.&rft.au=Gonz%C3%A1lez-Jim%C3%A9nez%2C+Kathy+A.&rft.au=Takizawa%2C+Yoichi&rft.au=Yumoto%2C+Manabu&rft.date=2025-05-01&rft.pub=The+Japan+Institute+of+Metals+and+Materials&rft.issn=1345-9678&rft.eissn=1347-5320&rft.volume=66&rft.issue=5&rft.spage=569&rft.epage=576&rft_id=info:doi/10.2320%2Fmatertrans.MT-MC2024018&rft.externalDocID=article_matertrans_66_5_66_MT_MC2024018_article_char_en
thumbnail_l http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=1345-9678&client=summon
thumbnail_m http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=1345-9678&client=summon
thumbnail_s http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=1345-9678&client=summon