Characterization of aroma compounds in Rosa roxburghii Tratt using solvent-assisted flavor evaporation headspace-solid phase microextraction coupled with gas chromatography-mass spectrometry and gas chromatography-olfactometry
•The volatile compounds of Rosa roxburghii Tratt samples from 4 origins were extracted by SAFE, HS-SPME.•143 volatiles were identified in Rosa roxburghii Tratt.•45 odor-active compounds were determined by GC-O.•Sensory attributes, odor-active compounds and origins were correlated by PLSR. Rosa roxbu...
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Published in | Food Chemistry: X Vol. 18; p. 100632 |
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Abstract | •The volatile compounds of Rosa roxburghii Tratt samples from 4 origins were extracted by SAFE, HS-SPME.•143 volatiles were identified in Rosa roxburghii Tratt.•45 odor-active compounds were determined by GC-O.•Sensory attributes, odor-active compounds and origins were correlated by PLSR.
Rosa roxburghii Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their processed products. In this study, volatile compounds were extracted using headspace-solid phase microextraction (HS-SPME) and solvent-assisted flavor evaporation (SAFE); 143 volatile compounds were identified by gas chromatography-mass spectrometry (GC–MS), and RRT from different origins were well distinguished based on principal component analysis. 45 odor-active components were identified using gas chromatography-olfactometry (GC-O). Through quantitative descriptive analysis (QDA), there were prominent “grassy” and “tea-like” attributes in RRT. Partial least-squares regression (PLSR) revealed that Longli RRT was greatly related to “tea-like” and “woody” attributes. Among the volatiles identified, alcohols and esters were considered the dominant volatile compounds of RRT, 4-methoxy-2,5-dimethyl-3(2H)-furanone was the most prominent compound. This study enriches the flavor chemistry theory of RRT and provides a scientific basis for optimizing the aroma of RRT and its processed products. |
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AbstractList | Rosa roxburghii Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their processed products. In this study, volatile compounds were extracted using headspace-solid phase microextraction (HS-SPME) and solvent-assisted flavor evaporation (SAFE); 143 volatile compounds were identified by gas chromatography-mass spectrometry (GC–MS), and RRT from different origins were well distinguished based on principal component analysis. 45 odor-active components were identified using gas chromatography-olfactometry (GC-O). Through quantitative descriptive analysis (QDA), there were prominent “grassy” and “tea-like” attributes in RRT. Partial least-squares regression (PLSR) revealed that Longli RRT was greatly related to “tea-like” and “woody” attributes. Among the volatiles identified, alcohols and esters were considered the dominant volatile compounds of RRT, 4-methoxy-2,5-dimethyl-3(2H)-furanone was the most prominent compound. This study enriches the flavor chemistry theory of RRT and provides a scientific basis for optimizing the aroma of RRT and its processed products. •The volatile compounds of Rosa roxburghii Tratt samples from 4 origins were extracted by SAFE, HS-SPME.•143 volatiles were identified in Rosa roxburghii Tratt.•45 odor-active compounds were determined by GC-O.•Sensory attributes, odor-active compounds and origins were correlated by PLSR. Rosa roxburghii Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their processed products. In this study, volatile compounds were extracted using headspace-solid phase microextraction (HS-SPME) and solvent-assisted flavor evaporation (SAFE); 143 volatile compounds were identified by gas chromatography-mass spectrometry (GC–MS), and RRT from different origins were well distinguished based on principal component analysis. 45 odor-active components were identified using gas chromatography-olfactometry (GC-O). Through quantitative descriptive analysis (QDA), there were prominent “grassy” and “tea-like” attributes in RRT. Partial least-squares regression (PLSR) revealed that Longli RRT was greatly related to “tea-like” and “woody” attributes. Among the volatiles identified, alcohols and esters were considered the dominant volatile compounds of RRT, 4-methoxy-2,5-dimethyl-3(2H)-furanone was the most prominent compound. This study enriches the flavor chemistry theory of RRT and provides a scientific basis for optimizing the aroma of RRT and its processed products. Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their processed products. In this study, volatile compounds were extracted using headspace-solid phase microextraction (HS-SPME) and solvent-assisted flavor evaporation (SAFE); 143 volatile compounds were identified by gas chromatography-mass spectrometry (GC-MS), and RRT from different origins were well distinguished based on principal component analysis. 45 odor-active components were identified using gas chromatography-olfactometry (GC-O). Through quantitative descriptive analysis (QDA), there were prominent "grassy" and "tea-like" attributes in RRT. Partial least-squares regression (PLSR) revealed that Longli RRT was greatly related to "tea-like" and "woody" attributes. Among the volatiles identified, alcohols and esters were considered the dominant volatile compounds of RRT, 4-methoxy-2,5-dimethyl-3(2H)-furanone was the most prominent compound. This study enriches the flavor chemistry theory of RRT and provides a scientific basis for optimizing the aroma of RRT and its processed products. • The volatile compounds of Rosa roxburghii Tratt samples from 4 origins were extracted by SAFE, HS-SPME. • 143 volatiles were identified in Rosa roxburghii Tratt. • 45 odor-active compounds were determined by GC-O. • Sensory attributes, odor-active compounds and origins were correlated by PLSR. Rosa roxburghii Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their processed products. In this study, volatile compounds were extracted using headspace-solid phase microextraction (HS-SPME) and solvent-assisted flavor evaporation (SAFE); 143 volatile compounds were identified by gas chromatography-mass spectrometry (GC–MS), and RRT from different origins were well distinguished based on principal component analysis. 45 odor-active components were identified using gas chromatography-olfactometry (GC-O). Through quantitative descriptive analysis (QDA), there were prominent “grassy” and “tea-like” attributes in RRT. Partial least-squares regression (PLSR) revealed that Longli RRT was greatly related to “tea-like” and “woody” attributes. Among the volatiles identified, alcohols and esters were considered the dominant volatile compounds of RRT, 4-methoxy-2,5-dimethyl-3(2H)-furanone was the most prominent compound. This study enriches the flavor chemistry theory of RRT and provides a scientific basis for optimizing the aroma of RRT and its processed products. |
ArticleNumber | 100632 |
Author | Cen, Shunyou Li, Tingting Huang, Qun Tang, Weiyuan Huang, Mingzheng Sheng, Xiaofang Li, Xin Li, Qinyang |
Author_xml | – sequence: 1 givenname: Xiaofang orcidid: 0000-0003-2357-7577 surname: Sheng fullname: Sheng, Xiaofang organization: College of Liquor and Food Engineering, Guizhou University, Guiyang, Guizhou, China – sequence: 2 givenname: Mingzheng orcidid: 0000-0002-3009-0559 surname: Huang fullname: Huang, Mingzheng email: huangmingzheng@git.edu.cn organization: College of Food and Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang, Guizhou, China – sequence: 3 givenname: Tingting surname: Li fullname: Li, Tingting organization: College of Liquor and Food Engineering, Guizhou University, Guiyang, Guizhou, China – sequence: 4 givenname: Xin surname: Li fullname: Li, Xin organization: School of Public Health, The Key Laboratory of Environmental Pollution Monitoring and Disease Control, Ministry of Education, Guizhou Medical University, Guiyang, Guizhou, China – sequence: 5 givenname: Shunyou surname: Cen fullname: Cen, Shunyou organization: Guizhou Hongcai Junong Investment Co., Ltd., Liupanshui, Guizhou, China – sequence: 6 givenname: Qinyang surname: Li fullname: Li, Qinyang organization: College of Liquor and Food Engineering, Guizhou University, Guiyang, Guizhou, China – sequence: 7 givenname: Qun surname: Huang fullname: Huang, Qun email: huangqunlaoshi@126.com organization: School of Public Health, The Key Laboratory of Environmental Pollution Monitoring and Disease Control, Ministry of Education, Guizhou Medical University, Guiyang, Guizhou, China – sequence: 8 givenname: Weiyuan surname: Tang fullname: Tang, Weiyuan email: twygycn@126.com organization: College of Liquor and Food Engineering, Guizhou University, Guiyang, Guizhou, China |
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Keywords | Partial least squares regression (PLSR) Quantitative descriptive analysis Gas chromatography-olfactometry (GC-O) Rosa roxburghii Tratt (RRT) Volatile compounds Principal component analysis (PCA) |
Language | English |
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Snippet | •The volatile compounds of Rosa roxburghii Tratt samples from 4 origins were extracted by SAFE, HS-SPME.•143 volatiles were identified in Rosa... Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their processed... • The volatile compounds of Rosa roxburghii Tratt samples from 4 origins were extracted by SAFE, HS-SPME. • 143 volatiles were identified in Rosa roxburghii... Rosa roxburghii Tratt (RRT) has become popular owing to its high vitamin C content. Volatiles are important factors that affect the quality of RRTs and their... |
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SubjectTerms | Gas chromatography-olfactometry (GC-O) Partial least squares regression (PLSR) Principal component analysis (PCA) Quantitative descriptive analysis Rosa roxburghii Tratt (RRT) Volatile compounds |
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Title | Characterization of aroma compounds in Rosa roxburghii Tratt using solvent-assisted flavor evaporation headspace-solid phase microextraction coupled with gas chromatography-mass spectrometry and gas chromatography-olfactometry |
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