An improved approach of salting-out solvent-free microwave mediated rotary distillation for essential oil preparation from fresh leaves of magnolia (Oyama sieboldii)
•Salting-out solvent-free microwave rotary distillation to obtain essential oil.•MgCl2 was selected as a salting-out agent from a wide range of metal salts.•During the whole process, the material is in a rotating state and is heated evenly.•Essential oil was prepared from fresh leaves of Oyama siebo...
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| Published in | Food Chemistry: X Vol. 16; p. 100524 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Netherlands
Elsevier Ltd
30.12.2022
Elsevier |
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| Abstract | •Salting-out solvent-free microwave rotary distillation to obtain essential oil.•MgCl2 was selected as a salting-out agent from a wide range of metal salts.•During the whole process, the material is in a rotating state and is heated evenly.•Essential oil was prepared from fresh leaves of Oyama sieboldii.•The main component of O. sieboldii essential oil were dehydrocostuslactone.
An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia (Oyama sieboldii) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography–mass spectrometry analysis showed that the main chemical constituent of O. sieboldii essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment. |
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| AbstractList | An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia (
) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography-mass spectrometry analysis showed that the main chemical constituent of
essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment. • Salting-out solvent-free microwave rotary distillation to obtain essential oil. • MgCl 2 was selected as a salting-out agent from a wide range of metal salts. • During the whole process, the material is in a rotating state and is heated evenly. • Essential oil was prepared from fresh leaves of Oyama sieboldii. • The main component of O. sieboldii essential oil were dehydrocostuslactone. An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia ( Oyama sieboldii ) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography–mass spectrometry analysis showed that the main chemical constituent of O. sieboldii essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment. An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia (Oyama sieboldii) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography-mass spectrometry analysis showed that the main chemical constituent of O. sieboldii essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment.An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia (Oyama sieboldii) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography-mass spectrometry analysis showed that the main chemical constituent of O. sieboldii essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment. An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia (Oyama sieboldii) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography–mass spectrometry analysis showed that the main chemical constituent of O. sieboldii essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment. •Salting-out solvent-free microwave rotary distillation to obtain essential oil.•MgCl2 was selected as a salting-out agent from a wide range of metal salts.•During the whole process, the material is in a rotating state and is heated evenly.•Essential oil was prepared from fresh leaves of Oyama sieboldii.•The main component of O. sieboldii essential oil were dehydrocostuslactone. An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils from fresh magnolia (Oyama sieboldii) leaves, in which we achieved the rotation of the reaction material by means of a rotating motor to subject the material to uniform microwave irradiation. Magnesium chloride was selected as the salting-out agent through a comparative study on the salting-out effects of different anions and cations of metal salts. The variables of SOSFMRD were systematically optimized. Under the obtained optimization conditions, the essential oil yield was 21.68 ± 1.02 mL/kgDW. Gas chromatography–mass spectrometry analysis showed that the main chemical constituent of O. sieboldii essential oil was dehydrocostuslactone, the content of which reached 30.23 ± 1.27 %. Compared with the other conventional methods, this method has a high yield and low energy consumption, which can effectively reduce impact on the environment. |
| ArticleNumber | 100524 |
| Author | Gu, Huiyan Yang, Lei Liu, Tingting Yang, Xinyu Wei, Mengxia Li, Jialei Zhao, Ru |
| Author_xml | – sequence: 1 givenname: Xinyu surname: Yang fullname: Yang, Xinyu organization: Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China – sequence: 2 givenname: Ru surname: Zhao fullname: Zhao, Ru organization: Key Laboratory of Quality and Safety of Agricultural Products of Nanjing, Nanjing Xiaozhuang University, Nanjing 211171, China – sequence: 3 givenname: Mengxia surname: Wei fullname: Wei, Mengxia organization: Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China – sequence: 4 givenname: Huiyan surname: Gu fullname: Gu, Huiyan organization: School of Forestry, Northeast Forestry University, Harbin 150040, China – sequence: 5 givenname: Jialei surname: Li fullname: Li, Jialei organization: Food Processing Institute, Heilongjiang Academy of Agricultural Sciences, Harbin 150086, China – sequence: 6 givenname: Lei surname: Yang fullname: Yang, Lei email: yanglei@nefu.edu.cn organization: Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China – sequence: 7 givenname: Tingting surname: Liu fullname: Liu, Tingting email: ltting@qmu.edu.cn organization: College of Pharmacy, Qiqihar Medical University, Qiqihar 161006, China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/36519096$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1016_j_arabjc_2024_105643 crossref_primary_10_1016_j_scp_2025_101979 crossref_primary_10_1016_j_scp_2023_101259 |
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| Keywords | Magnesium chloride Fresh leaves Essential oil Salting-out solvent-free microwave mediated rotary distillation (SOSFMRD) Oyama sieboldii |
| Language | English |
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| Snippet | •Salting-out solvent-free microwave rotary distillation to obtain essential oil.•MgCl2 was selected as a salting-out agent from a wide range of metal... An improved method denoted as salting out-solvent-free microwave rotary distillation (SOSFMRD) was successfully developed for the extraction of essential oils... • Salting-out solvent-free microwave rotary distillation to obtain essential oil. • MgCl 2 was selected as a salting-out agent from a wide range of metal... |
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| SubjectTerms | Essential oil Fresh leaves Magnesium chloride Oyama sieboldii Salting-out solvent-free microwave mediated rotary distillation (SOSFMRD) |
| Title | An improved approach of salting-out solvent-free microwave mediated rotary distillation for essential oil preparation from fresh leaves of magnolia (Oyama sieboldii) |
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