Immobilization and Continuous Recycling of Photoredox Catalysts in Ionic Liquids for Applications in Batch Reactions and Flow Systems: Catalytic Alkene Isomerization by Using Visible Light
A catalytic (E)‐ to (Z)‐isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)‐alkenes can be prepared in the presence of visible light. A new reaction system allows an easy and efficient scale‐up, as well as a continuous flow process in wh...
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| Published in | Chemistry : a European journal Vol. 21; no. 14; pp. 5350 - 5354 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Weinheim
WILEY-VCH Verlag
27.03.2015
WILEY‐VCH Verlag Wiley Wiley Subscription Services, Inc |
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| Abstract | A catalytic (E)‐ to (Z)‐isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)‐alkenes can be prepared in the presence of visible light. A new reaction system allows an easy and efficient scale‐up, as well as a continuous flow process in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by simple phase separation.
Catalytic (E)‐ to (Z)‐isomerizations of olefins under mild conditions can be achieved by use of a photosensitizer and visible light. A new reaction system such as depicted allows an easy and efficient scale‐up, as well as continuous flow processes in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by phase separation. |
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| AbstractList | A catalytic (E)- to (Z)-isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)-alkenes can be prepared in the presence of visible light. A new reaction system allows an easy and efficient scale-up, as well as a continuous flow process in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by simple phase separation. A catalytic (E)‐ to (Z)‐isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)‐alkenes can be prepared in the presence of visible light. A new reaction system allows an easy and efficient scale‐up, as well as a continuous flow process in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by simple phase separation. Catalytic (E)‐ to (Z)‐isomerizations of olefins under mild conditions can be achieved by use of a photosensitizer and visible light. A new reaction system such as depicted allows an easy and efficient scale‐up, as well as continuous flow processes in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by phase separation. A catalytic (E)- to (Z)-isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)-alkenes can be prepared in the presence of visible light. A new reaction system allows an easy and efficient scale-up, as well as a continuous flow process in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by simple phase separation. Catalytic (E)- to (Z)-isomerizations of olefins under mild conditions can be achieved by use of a photosensitizer and visible light. A new reaction system such as depicted allows an easy and efficient scale-up, as well as continuous flow processes in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by phase separation. Abstract A catalytic ( E )‐ to ( Z )‐isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of ( Z )‐alkenes can be prepared in the presence of visible light. A new reaction system allows an easy and efficient scale‐up, as well as a continuous flow process in which the photocatalyst is immobilized in an ionic liquid and continuously recycled by simple phase separation. |
| Author | Fabry, David C. Rueping, Magnus Ronge, Meria A. |
| Author_xml | – sequence: 1 givenname: David C. surname: Fabry fullname: Fabry, David C. organization: Institut für Organische Chemie, RWTH Aachen, Landoltweg 1, 52074 Aachen (Germany), Fax: (+49) 241-809-2127 – sequence: 2 givenname: Meria A. surname: Ronge fullname: Ronge, Meria A. organization: Institut für Organische Chemie, RWTH Aachen, Landoltweg 1, 52074 Aachen (Germany), Fax: (+49) 241-809-2127 – sequence: 3 givenname: Magnus surname: Rueping fullname: Rueping, Magnus email: magnus.rueping@rwth-aachen.de organization: Institut für Organische Chemie, RWTH Aachen, Landoltweg 1, 52074 Aachen (Germany), Fax: (+49) 241-809-2127 |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/25694030$$D View this record in MEDLINE/PubMed |
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| Keywords | RESVERATROL immobilization isomerization COMPLEXES MECHANISMS photocatalyst EXCITED-STATES STILBENE OLEFINATION CHEMISTRY SINGLET OXYGEN PHOTOCHEMISTRY ionic liquids EFFICIENT flow chemistry |
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(e_1_2_3_40_2) 2012; 22 e_1_2_3_4_2 e_1_2_3_16_2 e_1_2_3_37_2 e_1_2_3_16_3 e_1_2_3_2_2 e_1_2_3_18_2 e_1_2_3_39_2 e_1_2_3_8_2 e_1_2_3_12_2 e_1_2_3_33_2 e_1_2_3_6_2 e_1_2_3_14_2 e_1_2_3_52_2 e_1_2_3_10_2 e_1_2_3_31_2 Shvydkiv O. (e_1_2_3_44_2) (e_1_2_3_35_2) 2013 e_1_2_3_26_2 e_1_2_3_49_2 e_1_2_3_47_3 e_1_2_3_28_2 e_1_2_3_28_3 e_1_2_3_22_2 e_1_2_3_45_2 e_1_2_3_24_2 e_1_2_3_47_2 e_1_2_3_41_2 e_1_2_3_20_2 e_1_2_3_43_2 e_1_2_3_19_2 e_1_2_3_1_2 e_1_2_3_5_2 e_1_2_3_15_2 e_1_2_3_38_2 e_1_2_3_3_2 e_1_2_3_17_2 e_1_2_3_9_2 e_1_2_3_11_2 e_1_2_3_34_2 e_1_2_3_11_3 e_1_2_3_7_2 e_1_2_3_13_2 e_1_2_3_36_2 e_1_2_3_30_2 e_1_2_3_51_2 e_1_2_3_32_2 e_1_2_3_48_3 e_1_2_3_27_2 e_1_2_3_48_2 e_1_2_3_29_2 e_1_2_3_23_2 e_1_2_3_25_2 e_1_2_3_46_2 e_1_2_3_21_2 e_1_2_3_42_2 |
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| Snippet | A catalytic (E)‐ to (Z)‐isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)‐alkenes can be... A catalytic (E)- to (Z)-isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of (Z)-alkenes can be... Abstract A catalytic ( E )‐ to ( Z )‐isomerization of olefins using a photoredox catalyst under mild reaction conditions is presented. A variety of ( Z... |
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| SubjectTerms | Catalysis Catalysts Chemistry Chemistry, Multidisciplinary Continuous flow flow chemistry immobilization Ionic liquids Ions isomerization Liquids Olefins Phase separation photocatalyst Photocatalysts Physical Sciences Recycled Science & Technology Solvents |
| Title | Immobilization and Continuous Recycling of Photoredox Catalysts in Ionic Liquids for Applications in Batch Reactions and Flow Systems: Catalytic Alkene Isomerization by Using Visible Light |
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