Aluminizing for enhanced oxidation resistance of ductile refractory high-entropy alloys
Refractory high-entropy alloys (RHEAs) emerge as promising candidate materials for ultrahigh-temperature applications. One critical issue to solve for RHEAs is their balanced oxidation resistance and mechanical properties, mainly room-temperature ductility for the latter. Recently, it was found that...
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| Published in | Intermetallics Vol. 103; pp. 40 - 51 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.12.2018
Elsevier BV |
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| Abstract | Refractory high-entropy alloys (RHEAs) emerge as promising candidate materials for ultrahigh-temperature applications. One critical issue to solve for RHEAs is their balanced oxidation resistance and mechanical properties, mainly room-temperature ductility for the latter. Recently, it was found that existing ductile RHEAs are subject to catastrophic accelerated oxidation, also known as pesting. In this work, both alloying and surface coating, are applied to enhance the oxidation resistance of ductile RHEAs, with the focus on surface coating using the pack cementation method and more specifically, aluminizing. The oxidation resistance of two RHEAs, Hf0.5Nb0.5Ta0.5Ti1.5Zr, one recently identified ductile RHEA which pests in the temperature range of 600–1000 °C, and Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, the newly designed ductile RHEA which does not pest but embrittles after oxidation, are studied after aluminizing at 900 °C using three different pack components. Aluminizing, if using the appropriate pack cementation parameters, can avoid pesting in Hf0.5Nb0.5Ta0.5Ti1.5Zr and alleviate the oxidation induced embrittlement in Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, and holds the promise for further improving the RHEAs as potential ultrahigh-temperature materials.
•Pack cementation using different pack compositions were experimented on two RHEAs.•Proper aluminizing can avoid pesting in the Hf0.5Nb0.5Ta0.5Ti1.5Zr RHEA.•Proper aluminizing can improve the embrittlement in Al0.5Cr0.25Nb0.5Ta0.5Ti1.5.•Aluminizing is promising to further improve RHEAs for high-temperature applications. |
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| AbstractList | Refractory high-entropy alloys (RHEAs) emerge as promising candidate materials for ultrahigh-temperature applications. One critical issue to solve for RHEAs is their balanced oxidation resistance and mechanical properties, mainly room-temperature ductility for the latter. Recently, it was found that existing ductile RHEAs are subject to catastrophic accelerated oxidation, also known as pesting. In this work, both alloying and surface coating, are applied to enhance the oxidation resistance of ductile RHEAs, with the focus on surface coating using the pack cementation method and more specifically, aluminizing. The oxidation resistance of two RHEAs, Hf0.5Nb0.5Ta0.5Ti1.5Zr, one recently identified ductile RHEA which pests in the temperature range of 600–1000 °C, and Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, the newly designed ductile RHEA which does not pest but embrittles after oxidation, are studied after aluminizing at 900 °C using three different pack components. Aluminizing, if using the appropriate pack cementation parameters, can avoid pesting in Hf0.5Nb0.5Ta0.5Ti1.5Zr and alleviate the oxidation induced embrittlement in Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, and holds the promise for further improving the RHEAs as potential ultrahigh-temperature materials. Refractory high-entropy alloys (RHEAs) emerge as promising candidate materials for ultrahigh-temperature applications. One critical issue to solve for RHEAs is their balanced oxidation resistance and mechanical properties, mainly room-temperature ductility for the latter. Recently, it was found that existing ductile RHEAs are subject to catastrophic accelerated oxidation, also known as pesting. In this work, both alloying and surface coating, are applied to enhance the oxidation resistance of ductile RHEAs, with the focus on surface coating using the pack cementation method and more specifically, aluminizing. The oxidation resistance of two RHEAs, Hf0.5Nb0.5Ta0.5Ti1.5Zr, one recently identified ductile RHEA which pests in the temperature range of 600–1000 °C, and Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, the newly designed ductile RHEA which does not pest but embrittles after oxidation, are studied after aluminizing at 900 °C using three different pack components. Aluminizing, if using the appropriate pack cementation parameters, can avoid pesting in Hf0.5Nb0.5Ta0.5Ti1.5Zr and alleviate the oxidation induced embrittlement in Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, and holds the promise for further improving the RHEAs as potential ultrahigh-temperature materials. •Pack cementation using different pack compositions were experimented on two RHEAs.•Proper aluminizing can avoid pesting in the Hf0.5Nb0.5Ta0.5Ti1.5Zr RHEA.•Proper aluminizing can improve the embrittlement in Al0.5Cr0.25Nb0.5Ta0.5Ti1.5.•Aluminizing is promising to further improve RHEAs for high-temperature applications. Refractory high-entropy alloys (RHEAs) emerge as promising candidate materials for ultrahigh-temperature applications. One critical issue to solve for RHEAs is their balanced oxidation resistance and mechanical properties, mainly room-temperature ductility for the latter. Recently, it was found that existing ductile RHEAs are subject to catastrophic accelerated oxidation, also known as pesting. In this work, both alloying and surface coating, are applied to enhance the oxidation resistance of ductile RHEAs, with the focus on surface coating using the pack cementation method and more specifically, aluminizing. The oxidation resistance of two RHEAs, Hf0.5Nb0.5Ta0.5Ti1.5Zr, one recently identified ductile RHEA which pests in the temperature range of 600-1000 degrees C, and Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, the newly designed ductile RHEA which does not pest but embrittles after oxidation, are studied after aluminizing at 900 degrees C using three different pack components. Aluminizing, if using the appropriate pack cementation parameters, can avoid pesting in Hf0.5Nb0.5Ta0.5Ti1.5Zr and alleviate the oxidation induced embrittlement in Al0.5Cr0.25Nb0.5Ta0.5Ti1.5, and holds the promise for further improving the RHEAs as potential ultrahigh-temperature materials. |
| Author | Murakami, Hideyuki Gan, Lu Sheikh, Saad Guo, Sheng Shafeie, Samrand Tsao, Te-Kang |
| Author_xml | – sequence: 1 givenname: Saad surname: Sheikh fullname: Sheikh, Saad organization: Industrial and Materials Science, Chalmers University of Technology, 41296, Göteborg, Sweden – sequence: 2 givenname: Lu surname: Gan fullname: Gan, Lu organization: National Institute for Materials Science, Sengen 1-2-1, Tsukuba, Ibaraki, 305-0047, Japan – sequence: 3 givenname: Te-Kang surname: Tsao fullname: Tsao, Te-Kang organization: Department of Nanoscience and Nanoengineering, Waseda University, 3-4-1 Okubo Shinjuku, Tokyo, 169-8555, Japan – sequence: 4 givenname: Hideyuki surname: Murakami fullname: Murakami, Hideyuki organization: National Institute for Materials Science, Sengen 1-2-1, Tsukuba, Ibaraki, 305-0047, Japan – sequence: 5 givenname: Samrand surname: Shafeie fullname: Shafeie, Samrand organization: Inorganic Chemistry, Department of Chemistry, Ångström Laboratory, Uppsala University, 75121, Uppsala, Sweden – sequence: 6 givenname: Sheng surname: Guo fullname: Guo, Sheng email: sheng.guo@chalmers.se organization: Industrial and Materials Science, Chalmers University of Technology, 41296, Göteborg, Sweden |
| BackLink | https://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-371037$$DView record from Swedish Publication Index https://research.chalmers.se/publication/506782$$DView record from Swedish Publication Index |
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| Snippet | Refractory high-entropy alloys (RHEAs) emerge as promising candidate materials for ultrahigh-temperature applications. One critical issue to solve for RHEAs is... |
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| SubjectTerms | Alloys Aluminizing Coating High entropy alloys Materials selection Mechanical properties Oxidation Oxidation resistance Pack cementation Pesting (intermetallics) Pests Refractory alloys Refractory high-entropy alloys |
| Title | Aluminizing for enhanced oxidation resistance of ductile refractory high-entropy alloys |
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