Enhanced photoelectrochemical activities for water oxidation and phenol degradation on WO3 nanoplates by transferring electrons and trapping holes
It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO 3 by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO 3 nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal metho...
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| Published in | Scientific reports Vol. 7; no. 1; pp. 1 - 9 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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02.05.2017
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| Abstract | It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO
3
by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO
3
nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal method, and then co-modified with RGO and phosphate acid successively by wet chemical processes. Subsequently, the as-prepared WO
3
-based nanoplates were immobilized on the conductive glasses to explore the PEC activities for both water oxidation to evolve O
2
and phenol degradation. It is clearly demonstrated that the co-modified WO
3
nanoplates exhibit significantly improved PEC activities compared with pristine WO
3
, especially for that with the amount-optimized modifiers by ca. 6-time enhancement. Mainly based on the evaluated hydroxyl radical amounts produced and the electrochemical impedance spectra, it is suggested that the improved PEC activities are attributed to the greatly enhanced photogenerated charge separation after chemically modification with RGO and phosphate groups to WO
3
, respectively by transferring electrons as the collectors and trapping holes via the formed negative field after phosphate disassociation. This work provides a feasible synthetic strategy to improve the photoactivities of nanosized WO
3
for energy production and environmental remediation. |
|---|---|
| AbstractList | It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO3 by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO3 nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal method, and then co-modified with RGO and phosphate acid successively by wet chemical processes. Subsequently, the as-prepared WO3-based nanoplates were immobilized on the conductive glasses to explore the PEC activities for both water oxidation to evolve O2 and phenol degradation. It is clearly demonstrated that the co-modified WO3 nanoplates exhibit significantly improved PEC activities compared with pristine WO3, especially for that with the amount-optimized modifiers by ca. 6-time enhancement. Mainly based on the evaluated hydroxyl radical amounts produced and the electrochemical impedance spectra, it is suggested that the improved PEC activities are attributed to the greatly enhanced photogenerated charge separation after chemically modification with RGO and phosphate groups to WO3, respectively by transferring electrons as the collectors and trapping holes via the formed negative field after phosphate disassociation. This work provides a feasible synthetic strategy to improve the photoactivities of nanosized WO3 for energy production and environmental remediation.It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO3 by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO3 nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal method, and then co-modified with RGO and phosphate acid successively by wet chemical processes. Subsequently, the as-prepared WO3-based nanoplates were immobilized on the conductive glasses to explore the PEC activities for both water oxidation to evolve O2 and phenol degradation. It is clearly demonstrated that the co-modified WO3 nanoplates exhibit significantly improved PEC activities compared with pristine WO3, especially for that with the amount-optimized modifiers by ca. 6-time enhancement. Mainly based on the evaluated hydroxyl radical amounts produced and the electrochemical impedance spectra, it is suggested that the improved PEC activities are attributed to the greatly enhanced photogenerated charge separation after chemically modification with RGO and phosphate groups to WO3, respectively by transferring electrons as the collectors and trapping holes via the formed negative field after phosphate disassociation. This work provides a feasible synthetic strategy to improve the photoactivities of nanosized WO3 for energy production and environmental remediation. It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO 3 by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO 3 nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal method, and then co-modified with RGO and phosphate acid successively by wet chemical processes. Subsequently, the as-prepared WO 3 -based nanoplates were immobilized on the conductive glasses to explore the PEC activities for both water oxidation to evolve O 2 and phenol degradation. It is clearly demonstrated that the co-modified WO 3 nanoplates exhibit significantly improved PEC activities compared with pristine WO 3 , especially for that with the amount-optimized modifiers by ca. 6-time enhancement. Mainly based on the evaluated hydroxyl radical amounts produced and the electrochemical impedance spectra, it is suggested that the improved PEC activities are attributed to the greatly enhanced photogenerated charge separation after chemically modification with RGO and phosphate groups to WO 3 , respectively by transferring electrons as the collectors and trapping holes via the formed negative field after phosphate disassociation. This work provides a feasible synthetic strategy to improve the photoactivities of nanosized WO 3 for energy production and environmental remediation. Abstract It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO3 by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO3 nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal method, and then co-modified with RGO and phosphate acid successively by wet chemical processes. Subsequently, the as-prepared WO3-based nanoplates were immobilized on the conductive glasses to explore the PEC activities for both water oxidation to evolve O2 and phenol degradation. It is clearly demonstrated that the co-modified WO3 nanoplates exhibit significantly improved PEC activities compared with pristine WO3, especially for that with the amount-optimized modifiers by ca. 6-time enhancement. Mainly based on the evaluated hydroxyl radical amounts produced and the electrochemical impedance spectra, it is suggested that the improved PEC activities are attributed to the greatly enhanced photogenerated charge separation after chemically modification with RGO and phosphate groups to WO3, respectively by transferring electrons as the collectors and trapping holes via the formed negative field after phosphate disassociation. This work provides a feasible synthetic strategy to improve the photoactivities of nanosized WO3 for energy production and environmental remediation. It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO3 by artificially modulating the photogenerated electrons and holes simultaneously. Herein, WO3 nanoplates have been successfully prepared by a simple one-pot two-phase separated hydrolysis-solvothermal method, and then co-modified with RGO and phosphate acid successively by wet chemical processes. Subsequently, the as-prepared WO3-based nanoplates were immobilized on the conductive glasses to explore the PEC activities for both water oxidation to evolve O2 and phenol degradation. It is clearly demonstrated that the co-modified WO3 nanoplates exhibit significantly improved PEC activities compared with pristine WO3, especially for that with the amount-optimized modifiers by ca. 6-time enhancement. Mainly based on the evaluated hydroxyl radical amounts produced and the electrochemical impedance spectra, it is suggested that the improved PEC activities are attributed to the greatly enhanced photogenerated charge separation after chemically modification with RGO and phosphate groups to WO3, respectively by transferring electrons as the collectors and trapping holes via the formed negative field after phosphate disassociation. This work provides a feasible synthetic strategy to improve the photoactivities of nanosized WO3 for energy production and environmental remediation. |
| ArticleNumber | 1303 |
| Author | Sun, Liqun Raziq, Fazal Bai, Linlu Qu, Yang Wang, Yuying Jing, Liqiang |
| Author_xml | – sequence: 1 givenname: Liqun surname: Sun fullname: Sun, Liqun organization: Key Laboratory of Functional Inorganic Materials Chemistry (Heilongjiang University), Ministry of Education, International Joint Research Center for Catalytic Technology, School of Chemistry and Materials Science, College of Chemical Engineering, Daqing Normal University, Key Laboratory of Oilfield Applied chemistry, College of Heilongjiang Province – sequence: 2 givenname: Yuying surname: Wang fullname: Wang, Yuying organization: Key Laboratory of Functional Inorganic Materials Chemistry (Heilongjiang University), Ministry of Education, International Joint Research Center for Catalytic Technology, School of Chemistry and Materials Science – sequence: 3 givenname: Fazal surname: Raziq fullname: Raziq, Fazal organization: Key Laboratory of Functional Inorganic Materials Chemistry (Heilongjiang University), Ministry of Education, International Joint Research Center for Catalytic Technology, School of Chemistry and Materials Science – sequence: 4 givenname: Yang surname: Qu fullname: Qu, Yang organization: Key Laboratory of Functional Inorganic Materials Chemistry (Heilongjiang University), Ministry of Education, International Joint Research Center for Catalytic Technology, School of Chemistry and Materials Science – sequence: 5 givenname: Linlu surname: Bai fullname: Bai, Linlu email: lbai2@e.ntu.edu.sg organization: Key Laboratory of Functional Inorganic Materials Chemistry (Heilongjiang University), Ministry of Education, International Joint Research Center for Catalytic Technology, School of Chemistry and Materials Science, College of Chemical and Environmental Engineering, Harbin University of Science and Technology – sequence: 6 givenname: Liqiang orcidid: 0000-0002-3189-492X surname: Jing fullname: Jing, Liqiang email: jinglq@hlju.edu.cn organization: Key Laboratory of Functional Inorganic Materials Chemistry (Heilongjiang University), Ministry of Education, International Joint Research Center for Catalytic Technology, School of Chemistry and Materials Science |
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| Snippet | It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO
3
by artificially modulating the photogenerated electrons and holes... It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO3 by artificially modulating the photogenerated electrons and holes... Abstract It is highly desired to improve the photoelectrochemical (PEC) performance of nanosized WO3 by artificially modulating the photogenerated electrons... |
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| SubjectTerms | 140/133 140/146 639/638/77/890 704/172/169 Electrochemistry Environmental cleanup Humanities and Social Sciences Hydroxyl radicals multidisciplinary Oxidation Phenols Science Science (multidisciplinary) Trapping |
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| Title | Enhanced photoelectrochemical activities for water oxidation and phenol degradation on WO3 nanoplates by transferring electrons and trapping holes |
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