Electropolymerization of robust conjugated microporous polymer membranes for rapid solvent transport and narrow molecular sieving
Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes...
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| Published in | Nature communications Vol. 11; no. 1; pp. 5323 - 9 |
|---|---|
| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
21.10.2020
Nature Publishing Group Nature Portfolio |
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| Online Access | Get full text |
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| Abstract | Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes. Inspired by the skin-core architecture of spider silk that offers both high strength and high ductility, herein we report an electropolymerization process to prepare a CMP membrane from a rigid carbazole monomer, 2,2’,7,7’-tetra(carbazol-9-yl)-9,9’-spirobifluorene, inside a robust carbon nanotube scaffold. The obtained membranes showed superior mechanical strength and ductility, high surface area, and uniform pore size of approximately 1 nm. The superfast solvent transport and excellent molecular sieving well surpass the performance of most reported polymer membranes. Our method makes it possible to use rigid CMPs membranes in pressure-driven membrane processes, providing potential applications for this important category of polymer materials.
Conjugated microporous polymers (CMPs) have great potential in membrane applications but are often brittle. Here, the authors develop an electropolymerization process to form a skin-core architecture which allows them to overcome mechanical limitations while keeping the excellent separation performance of CMP membranes. |
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| AbstractList | Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes. Inspired by the skin-core architecture of spider silk that offers both high strength and high ductility, herein we report an electropolymerization process to prepare a CMP membrane from a rigid carbazole monomer, 2,2',7,7'-tetra(carbazol-9-yl)-9,9'-spirobifluorene, inside a robust carbon nanotube scaffold. The obtained membranes showed superior mechanical strength and ductility, high surface area, and uniform pore size of approximately 1 nm. The superfast solvent transport and excellent molecular sieving well surpass the performance of most reported polymer membranes. Our method makes it possible to use rigid CMPs membranes in pressure-driven membrane processes, providing potential applications for this important category of polymer materials.Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes. Inspired by the skin-core architecture of spider silk that offers both high strength and high ductility, herein we report an electropolymerization process to prepare a CMP membrane from a rigid carbazole monomer, 2,2',7,7'-tetra(carbazol-9-yl)-9,9'-spirobifluorene, inside a robust carbon nanotube scaffold. The obtained membranes showed superior mechanical strength and ductility, high surface area, and uniform pore size of approximately 1 nm. The superfast solvent transport and excellent molecular sieving well surpass the performance of most reported polymer membranes. Our method makes it possible to use rigid CMPs membranes in pressure-driven membrane processes, providing potential applications for this important category of polymer materials. Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes. Inspired by the skin-core architecture of spider silk that offers both high strength and high ductility, herein we report an electropolymerization process to prepare a CMP membrane from a rigid carbazole monomer, 2,2’,7,7’-tetra(carbazol-9-yl)-9,9’-spirobifluorene, inside a robust carbon nanotube scaffold. The obtained membranes showed superior mechanical strength and ductility, high surface area, and uniform pore size of approximately 1 nm. The superfast solvent transport and excellent molecular sieving well surpass the performance of most reported polymer membranes. Our method makes it possible to use rigid CMPs membranes in pressure-driven membrane processes, providing potential applications for this important category of polymer materials. Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes. Inspired by the skin-core architecture of spider silk that offers both high strength and high ductility, herein we report an electropolymerization process to prepare a CMP membrane from a rigid carbazole monomer, 2,2’,7,7’-tetra(carbazol-9-yl)-9,9’-spirobifluorene, inside a robust carbon nanotube scaffold. The obtained membranes showed superior mechanical strength and ductility, high surface area, and uniform pore size of approximately 1 nm. The superfast solvent transport and excellent molecular sieving well surpass the performance of most reported polymer membranes. Our method makes it possible to use rigid CMPs membranes in pressure-driven membrane processes, providing potential applications for this important category of polymer materials.Conjugated microporous polymers (CMPs) have great potential in membrane applications but are often brittle. Here, the authors develop an electropolymerization process to form a skin-core architecture which allows them to overcome mechanical limitations while keeping the excellent separation performance of CMP membranes. Conjugated microporous polymers (CMPs) have great potential in membrane applications but are often brittle. Here, the authors develop an electropolymerization process to form a skin-core architecture which allows them to overcome mechanical limitations while keeping the excellent separation performance of CMP membranes. Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous polymers (CMPs) has shown uniform pore size and high porosity. However, their brittle nature has prevented them from preparing robust membranes. Inspired by the skin-core architecture of spider silk that offers both high strength and high ductility, herein we report an electropolymerization process to prepare a CMP membrane from a rigid carbazole monomer, 2,2’,7,7’-tetra(carbazol-9-yl)-9,9’-spirobifluorene, inside a robust carbon nanotube scaffold. The obtained membranes showed superior mechanical strength and ductility, high surface area, and uniform pore size of approximately 1 nm. The superfast solvent transport and excellent molecular sieving well surpass the performance of most reported polymer membranes. Our method makes it possible to use rigid CMPs membranes in pressure-driven membrane processes, providing potential applications for this important category of polymer materials. Conjugated microporous polymers (CMPs) have great potential in membrane applications but are often brittle. Here, the authors develop an electropolymerization process to form a skin-core architecture which allows them to overcome mechanical limitations while keeping the excellent separation performance of CMP membranes. |
| ArticleNumber | 5323 |
| Author | Liu, Xiaowei Hu, Yunxia Lu, Dongwei Lai, Zhiping Zhou, Zongyao Chen, Long Guo, Dong Shinde, Digambar B. Li, Xiang Cao, Li Aboalsaud, Ammar M. |
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| Snippet | Pore size uniformity is one of the most critical parameters in determining membrane separation performance. Recently, a novel type of conjugated microporous... Conjugated microporous polymers (CMPs) have great potential in membrane applications but are often brittle. Here, the authors develop an electropolymerization... |
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| SubjectTerms | 639/166/898 639/301/923/1028 Brittleness Carbazole Carbazoles Carbon nanotubes Ductility Humanities and Social Sciences Mechanical properties Membrane processes Membrane separation Membranes multidisciplinary Polymerization Polymers Pore size Porosity Robustness Science Science (multidisciplinary) Separation Silk Solvents |
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| Title | Electropolymerization of robust conjugated microporous polymer membranes for rapid solvent transport and narrow molecular sieving |
| URI | https://link.springer.com/article/10.1038/s41467-020-19182-1 https://www.proquest.com/docview/2471491294 https://www.proquest.com/docview/2453691828 https://pubmed.ncbi.nlm.nih.gov/PMC7578036 https://doaj.org/article/3282d7a3f7564f13827bc660ad7206ab |
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