Synthesis of granular activated carbon/zero valent iron composites for simultaneous adsorption/dechlorination of trichloroethylene

► The synthesis of new materials, GAC–ZVI composites, which combine the advantages of a sorption material (granular activated carbon) and a reduction material (zerovalent iron) is developed. ► The kinetics of the sorption/dechlorination of TCE in short- and long-term experiments is studied. ► Mass b...

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Published in	Journal of hazardous materials Vol. 192; no. 2; pp. 500 - 506
Main Authors	Tseng, Hui-Hsin, Su, Jhih-Gang, Liang, Chenju
Format	Journal Article
Language	English
Published	Kidlington Elsevier B.V 30.08.2011 Elsevier
Subjects	Activated carbon Adsorption Applied sciences Biological and physicochemical phenomena Carbon - chemistry Chemical engineering Chlorinated solvent Chlorine - chemistry Dechlorination Degradation desorption Exact sciences and technology Groundwater remediation Groundwaters Iron Iron - chemistry Kinetics Natural water pollution nitrogen Pollution Rate constants Reactive activated carbon Reactors Reduction Streams Trichloroethylene Trichloroethylene - chemistry Waste water treatment Water treatment and pollution Groundwater remediation Reactive activated carbon Reduction Waste water treatment Chlorinated solvent Dehalogenation Dispersant Zerovalent metal Composite material Chemical reduction Dechlorination Activated carbon Chlorine Organic compounds Rate constant Organic compounds Ground water Ethylene(trichloro) Desorption Impregnation Organic solvent Adsorption First order Water pollution Kinetics Waste water purification
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Abstract	► The synthesis of new materials, GAC–ZVI composites, which combine the advantages of a sorption material (granular activated carbon) and a reduction material (zerovalent iron) is developed. ► The kinetics of the sorption/dechlorination of TCE in short- and long-term experiments is studied. ► Mass balance during treatment is performed. ► Characterization before and after reaction using BET, XRD, SEM/EDS, and TEM is conducted. The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC–ZVI) composites was studied. The GAC–ZVI composites were prepared from aqueous Fe 2+ solutions by impregnation with and without the use of a PEG dispersant and then heated at 105 °C or 700 °C under a stream of N 2. Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC–ZVI composites. However, the usage of GAC–ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC–ZVI700P composite (synthesized using PEG under 700 °C). A modified Langmuir–Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC–ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately.
AbstractList	The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC–ZVI) composites was studied. The GAC–ZVI composites were prepared from aqueous Fe²⁺ solutions by impregnation with and without the use of a PEG dispersant and then heated at 105°C or 700°C under a stream of N₂. Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC–ZVI composites. However, the usage of GAC–ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC–ZVI700P composite (synthesized using PEG under 700°C). A modified Langmuir–Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC–ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately. The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC-ZVI) composites was studied. The GAC-ZVI composites were prepared from aqueous Fe(2+) solutions by impregnation with and without the use of a PEG dispersant and then heated at 105°C or 700°C under a stream of N(2). Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC-ZVI composites. However, the usage of GAC-ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC-ZVI700P composite (synthesized using PEG under 700°C). A modified Langmuir-Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC-ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately. The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC-ZVI) composites was studied. The GAC-ZVI composites were prepared from aqueous Fe2+ solutions by impregnation with and without the use of a PEG dispersant and then heated at 105 degree C or 700 degree C under a stream of N2. Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC-ZVI composites. However, the usage of GAC-ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC-ZVI700P composite (synthesized using PEG under 700 degree C). A modified Langmuir-Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC-ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately. ► The synthesis of new materials, GAC–ZVI composites, which combine the advantages of a sorption material (granular activated carbon) and a reduction material (zerovalent iron) is developed. ► The kinetics of the sorption/dechlorination of TCE in short- and long-term experiments is studied. ► Mass balance during treatment is performed. ► Characterization before and after reaction using BET, XRD, SEM/EDS, and TEM is conducted. The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC–ZVI) composites was studied. The GAC–ZVI composites were prepared from aqueous Fe 2+ solutions by impregnation with and without the use of a PEG dispersant and then heated at 105 °C or 700 °C under a stream of N 2. Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC–ZVI composites. However, the usage of GAC–ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC–ZVI700P composite (synthesized using PEG under 700 °C). A modified Langmuir–Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC–ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately. The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC-ZVI) composites was studied. The GAC-ZVI composites were prepared from aqueous Fe(2+) solutions by impregnation with and without the use of a PEG dispersant and then heated at 105°C or 700°C under a stream of N(2). Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC-ZVI composites. However, the usage of GAC-ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC-ZVI700P composite (synthesized using PEG under 700°C). A modified Langmuir-Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC-ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately.The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron (GAC-ZVI) composites was studied. The GAC-ZVI composites were prepared from aqueous Fe(2+) solutions by impregnation with and without the use of a PEG dispersant and then heated at 105°C or 700°C under a stream of N(2). Pseudo-first-order rate constant data on the removal of TCE demonstrates that the adsorption kinetics of GAC is similar to those of GAC-ZVI composites. However, the usage of GAC-ZVI composites liberated a greater amount of Cl than when ZVI was used alone. The highest degree of reductive dechlorination of TCE was achieved using a GAC-ZVI700P composite (synthesized using PEG under 700°C). A modified Langmuir-Hinshelwood rate law was employed to depict the behavior of Cl liberation. As a result, a zero-order Cl liberation reaction was observed and the desorption limited TCE degradation rate constant decreased as the composite dosage was increased. The GAC-ZVI composites can be employed as a reactive GAC that is not subject to the limitations of using GAC and ZVI separately.
Author	Su, Jhih-Gang Liang, Chenju Tseng, Hui-Hsin
Author_xml	– sequence: 1 givenname: Hui-Hsin surname: Tseng fullname: Tseng, Hui-Hsin organization: School of Occupational Safety and Health, Chung Shan Medical University, Taichung 402, Taiwan – sequence: 2 givenname: Jhih-Gang surname: Su fullname: Su, Jhih-Gang organization: Department of Environmental Engineering, National Chung Hsing University, 250 Kuo-Kuang Rd., Taichung City 402, Taiwan – sequence: 3 givenname: Chenju surname: Liang fullname: Liang, Chenju email: cliang@dragon.nchu.edu.tw organization: Department of Environmental Engineering, National Chung Hsing University, 250 Kuo-Kuang Rd., Taichung City 402, Taiwan
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Keywords	Groundwater remediation Reactive activated carbon Reduction Waste water treatment Chlorinated solvent Dehalogenation Dispersant Zerovalent metal Composite material Chemical reduction Dechlorination Activated carbon Chlorine Organic compounds Rate constant Organic compounds Ground water Ethylene(trichloro) Desorption Impregnation Organic solvent Adsorption First order Water pollution Kinetics Waste water purification
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Technol. doi: 10.1021/es950053u
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Snippet	► The synthesis of new materials, GAC–ZVI composites, which combine the advantages of a sorption material (granular activated carbon) and a reduction material... The coupling adsorption and degradation of trichloroethylene (TCE) through dechlorination using synthetic granular activated carbon and zerovalent iron...
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SubjectTerms	Activated carbon Adsorption Applied sciences Biological and physicochemical phenomena Carbon - chemistry Chemical engineering Chlorinated solvent Chlorine - chemistry Dechlorination Degradation desorption Exact sciences and technology Groundwater remediation Groundwaters Iron Iron - chemistry Kinetics Natural water pollution nitrogen Pollution Rate constants Reactive activated carbon Reactors Reduction Streams Trichloroethylene Trichloroethylene - chemistry Waste water treatment Water treatment and pollution
Title	Synthesis of granular activated carbon/zero valent iron composites for simultaneous adsorption/dechlorination of trichloroethylene
URI	https://dx.doi.org/10.1016/j.jhazmat.2011.05.047 https://www.ncbi.nlm.nih.gov/pubmed/21676545 https://www.proquest.com/docview/1671347912 https://www.proquest.com/docview/1694505412 https://www.proquest.com/docview/878030885 https://www.proquest.com/docview/883033945
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