Influence of Non-Thermal Atmospheric Pressure Plasma Treatment on Shear Bond Strength between Y-TZP and Self-Adhesive Resin Cement

• Published in: Materials Vol. 12; no. 20; p. 3321
• Main Authors: Kim, Dae-Sung, Ahn, Jong-Ju, Bae, Eun-Bin, Kim, Gyoo-Cheon, Jeong, Chang-Mo, Huh, Jung-Bo, Lee, So-Hyoun
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 12.10.2019; MDPI
• Subjects: Adhesive strength; Adhesives; Atmospheric pressure; Bond strength; Bonding strength; Cement; Cements; Chemical bonds; Contact angle; Emission analysis; Failure; Failure modes; Field emission microscopy; Heat treatment; Optical microscopes; Organic chemistry; Plasma; plasma treatment; Prostheses; Resins; Sandblasting; Scanning electron microscopy; self-adhesive resin cement; shear bond strength; Surface treatment; Tetragonal zirconia polycrystals; Variance analysis; yttria-stabilized tetragonal zirconia polycrystal (y-tzp); Yttria-stabilized zirconia; Yttrium; Zirconium dioxide; United States > US; Japan; Germany
• ISSN: 1996-1944; 1996-1944
• DOI: 10.3390/ma12203321

The purpose of this study was to evaluate the effect of non-thermal atmospheric pressure plasma (NTP) on shear bond strength (SBS) between yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) and self-adhesive resin cement. For this study, surface energy (SE) was calculated with cube-shaped Y-TZP specimens, and SBS was measured on disc-shaped Y-TZP specimens bonded with G-CEM LinkAce or RelyX U200 resin cylinder. The Y-TZP specimens were classified into four groups according to the surface treatment as follows: Control (no surface treatment), NTP, Sb (Sandblasting), and Sb + NTP. The results showed that the SE was significantly higher in the NTP group than in the Control group (p < 0.05). For the SBS test, in non-thermocycling, the NTP group of both self-adhesive resin cements showed significantly higher SBS than the Control group (p < 0.05). However, regardless of the cement type in thermocycling, there was no significant increase in the SBS between the Control and NTP groups. Comparing the two cements, regardless of thermocycling, the NTP group of G-CEM LinkAce showed significantly higher SBS than that of RelyX U200 (p < 0.05). Our study suggests that NTP increases the SE. Furthermore, NTP increases the initial SBS, which is higher when using G-CEM LinkAce than when using RelyX U200.