Microstructure and Room Temperature Mechanical Properties of Different 3 and 4 Element Medium Entropy Alloys from HfNbTaTiZr System

Refractory high entropy alloys (HEA) are promising materials for high temperature applications. This work presents investigations of the room temperature tensile mechanical properties of selected 3 and 4 elements medium entropy alloys (MEA) derived from the HfNbTaTiZr system. Tensile testing was com...

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Published inEntropy (Basel, Switzerland) Vol. 21; no. 2; p. 114
Main Authors Zýka, Jiří, Málek, Jaroslav, Veselý, Jaroslav, Lukáč, František, Čížek, Jakub, Kuriplach, Jan, Melikhova, Oksana
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 26.01.2019
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Abstract Refractory high entropy alloys (HEA) are promising materials for high temperature applications. This work presents investigations of the room temperature tensile mechanical properties of selected 3 and 4 elements medium entropy alloys (MEA) derived from the HfNbTaTiZr system. Tensile testing was combined with fractographic and microstructure analysis, using scanning electron microscope (SEM), wavelength dispersive spectroscope (WDS) and X-Ray powder diffraction (XRD). The 5 element HEA alloy HfNbTaTiZr exhibits the best combination of strength and elongation while 4 and 3 element MEAs have lower strength. Some of them are ductile, some of them brittle, depending on microstructure. Simultaneous presence of Ta and Zr in the alloy resulted in a significant reduction of ductility caused by reduction of the BCC phase content. Precipitation of Ta rich particles on grain boundaries reduces further the maximum elongation to failure down to zero values.
AbstractList Refractory high entropy alloys (HEA) are promising materials for high temperature applications. This work presents investigations of the room temperature tensile mechanical properties of selected 3 and 4 elements medium entropy alloys (MEA) derived from the HfNbTaTiZr system. Tensile testing was combined with fractographic and microstructure analysis, using scanning electron microscope (SEM), wavelength dispersive spectroscope (WDS) and X-Ray powder diffraction (XRD). The 5 element HEA alloy HfNbTaTiZr exhibits the best combination of strength and elongation while 4 and 3 element MEAs have lower strength. Some of them are ductile, some of them brittle, depending on microstructure. Simultaneous presence of Ta and Zr in the alloy resulted in a significant reduction of ductility caused by reduction of the BCC phase content. Precipitation of Ta rich particles on grain boundaries reduces further the maximum elongation to failure down to zero values.
Refractory high entropy alloys (HEA) are promising materials for high temperature applications. This work presents investigations of the room temperature tensile mechanical properties of selected 3 and 4 elements medium entropy alloys (MEA) derived from the HfNbTaTiZr system. Tensile testing was combined with fractographic and microstructure analysis, using scanning electron microscope (SEM), wavelength dispersive spectroscope (WDS) and X-Ray powder diffraction (XRD). The 5 element HEA alloy HfNbTaTiZr exhibits the best combination of strength and elongation while 4 and 3 element MEAs have lower strength. Some of them are ductile, some of them brittle, depending on microstructure. Simultaneous presence of Ta and Zr in the alloy resulted in a significant reduction of ductility caused by reduction of the BCC phase content. Precipitation of Ta rich particles on grain boundaries reduces further the maximum elongation to failure down to zero values.Refractory high entropy alloys (HEA) are promising materials for high temperature applications. This work presents investigations of the room temperature tensile mechanical properties of selected 3 and 4 elements medium entropy alloys (MEA) derived from the HfNbTaTiZr system. Tensile testing was combined with fractographic and microstructure analysis, using scanning electron microscope (SEM), wavelength dispersive spectroscope (WDS) and X-Ray powder diffraction (XRD). The 5 element HEA alloy HfNbTaTiZr exhibits the best combination of strength and elongation while 4 and 3 element MEAs have lower strength. Some of them are ductile, some of them brittle, depending on microstructure. Simultaneous presence of Ta and Zr in the alloy resulted in a significant reduction of ductility caused by reduction of the BCC phase content. Precipitation of Ta rich particles on grain boundaries reduces further the maximum elongation to failure down to zero values.
Author Málek, Jaroslav
Zýka, Jiří
Lukáč, František
Kuriplach, Jan
Melikhova, Oksana
Veselý, Jaroslav
Čížek, Jakub
AuthorAffiliation 3 Faculty of Mathematics and Physics, Charles University, V Holešovičkách 2, 18000 Praha 8, Czech Republic
2 Department of Materials Engineering, Institute of Plasma Physics CAS, Za Slovankou 1782, 1820 Praha 8, Czech Republic
1 UJP PRAHA a.s., Nad Kamínkou 1345, 156 10 Praha 5—Zbraslav, Czech Republic
AuthorAffiliation_xml – name: 2 Department of Materials Engineering, Institute of Plasma Physics CAS, Za Slovankou 1782, 1820 Praha 8, Czech Republic
– name: 3 Faculty of Mathematics and Physics, Charles University, V Holešovičkách 2, 18000 Praha 8, Czech Republic
– name: 1 UJP PRAHA a.s., Nad Kamínkou 1345, 156 10 Praha 5—Zbraslav, Czech Republic
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Snippet Refractory high entropy alloys (HEA) are promising materials for high temperature applications. This work presents investigations of the room temperature...
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SubjectTerms Alloying elements
Alloys
Ductile-brittle transition
Ductility
Elongation
Grain boundaries
High entropy alloys
High temperature
Mechanical properties
Medium entropy alloys
medium entropy alloys, mechanical properties
Microstructure
Reduction
refractory high entropy alloys
Room temperature
Solid solutions
Tensile tests
X ray powder diffraction
Zirconium
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Title Microstructure and Room Temperature Mechanical Properties of Different 3 and 4 Element Medium Entropy Alloys from HfNbTaTiZr System
URI https://www.proquest.com/docview/2548380352
https://www.proquest.com/docview/2466768303
https://pubmed.ncbi.nlm.nih.gov/PMC7514597
https://doaj.org/article/6e03dd68be0641ae80297a79e024277f
Volume 21
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