Accurate Nanoscale Crystallography in Real-Space Using Scanning Transmission Electron Microscopy
Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made possible by removing drift and residual scan distortion. We demonstrate real-space lattice parameter measurements with <0.1% error for complex-layered...
Saved in:
Published in | Microscopy and microanalysis Vol. 21; no. 4; pp. 946 - 952 |
---|---|
Main Authors | , , , , , , , , , , , |
Format | Journal Article |
Language | English |
Published |
New York, USA
Cambridge University Press
01.08.2015
Oxford University Press Microscopy Society of America (MSA) |
Subjects | |
Online Access | Get full text |
Cover
Loading…
Abstract | Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made possible by removing drift and residual scan distortion. We demonstrate real-space lattice parameter measurements with <0.1% error for complex-layered chalcogenides Bi2Te3, Bi2Se3, and a Bi2Te2.7Se0.3 nanostructured alloy. Pairing the technique with atomic resolution spectroscopy, we connect local structure with chemistry and bonding. Combining these results with density functional theory, we show that the incorporation of Se into Bi2Te3 causes charge redistribution that anomalously increases the van der Waals gap between building blocks of the layered structure. The results show that atomic resolution imaging with electrons can accurately and robustly quantify crystallography at the nanoscale. |
---|---|
AbstractList | Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made possible by removing drift and residual scan distortion. We demonstrate real-space lattice parameter measurements with <0.1% error for complex-layered chalcogenides Bi2Te3, Bi2Se3, and a Bi2Te2.7Se0.3 nanostructured alloy. Pairing the technique with atomic resolution spectroscopy, we connect local structure with chemistry and bonding. Combining these results with density functional theory, we show that the incorporation of Se into Bi2Te3 causes charge redistribution that anomalously increases the van der Waals gap between building blocks of the layered structure. The results show that atomic resolution imaging with electrons can accurately and robustly quantify crystallography at the nanoscale. Abstract Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made possible by removing drift and residual scan distortion. We demonstrate real-space lattice parameter measurements with <0.1% error for complex-layered chalcogenides Bi 2 Te 3 , Bi 2 Se 3 , and a Bi 2 Te 2.7 Se 0.3 nanostructured alloy. Pairing the technique with atomic resolution spectroscopy, we connect local structure with chemistry and bonding. Combining these results with density functional theory, we show that the incorporation of Se into Bi 2 Te 3 causes charge redistribution that anomalously increases the van der Waals gap between building blocks of the layered structure. The results show that atomic resolution imaging with electrons can accurately and robustly quantify crystallography at the nanoscale. Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made possible by removing drift and residual scan distortion. We demonstrate real-space lattice parameter measurements with <0.1% error for complex-layered chalcogenides Bi2Te3, Bi2Se3, and a Bi2Te2.7Se0.3 nanostructured alloy. Pairing the technique with atomic resolution spectroscopy, we connect local structure with chemistry and bonding. Combining these results with density functional theory, we show that the incorporation of Se into Bi2Te3 causes charge redistribution that anomalously increases the van der Waals gap between building blocks of the layered structure. The results show that atomic resolution imaging with electrons can accurately and robustly quantify crystallography at the nanoscale. |
Author | Dycus, J. Houston Sang, Xiahan Findlay, Scott D. Oni, Adedapo A. Chan, Tsung-ta E. Harris, Joshua S. Fancher, Chris M. Irving, Douglas L. LeBeau, James M. Allen, Leslie J. Jones, Jacob L. Koch, Carl C. |
Author_xml | – sequence: 1 givenname: J. Houston surname: Dycus fullname: Dycus, J. Houston organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 2 givenname: Joshua S. surname: Harris fullname: Harris, Joshua S. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 3 givenname: Xiahan surname: Sang fullname: Sang, Xiahan organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 4 givenname: Chris M. surname: Fancher fullname: Fancher, Chris M. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 5 givenname: Scott D. orcidid: 0000-0003-4862-4827 surname: Findlay fullname: Findlay, Scott D. organization: School of Physics and Astronomy, Monash University, Clayton, VIC 3800, Australia – sequence: 6 givenname: Adedapo A. surname: Oni fullname: Oni, Adedapo A. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 7 givenname: Tsung-ta E. surname: Chan fullname: Chan, Tsung-ta E. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 8 givenname: Carl C. surname: Koch fullname: Koch, Carl C. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 9 givenname: Jacob L. surname: Jones fullname: Jones, Jacob L. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 10 givenname: Leslie J. surname: Allen fullname: Allen, Leslie J. organization: School of Physics, University of Melbourne, Parkville, VIC 3010, Australia – sequence: 11 givenname: Douglas L. surname: Irving fullname: Irving, Douglas L. organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA – sequence: 12 givenname: James M. surname: LeBeau fullname: LeBeau, James M. email: jmlebeau@ncsu.edu organization: Department of Materials Science and Engineering, North Carolina State University, Raleigh, NC 27695, USA |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/26169835$$D View this record in MEDLINE/PubMed https://www.osti.gov/biblio/1225090$$D View this record in Osti.gov |
BookMark | eNp1kU1v1DAQhi1URD_gB3BBEb30Euqx4zg5Vqt-SQWkbnsOk4l36yprBzs57L-v96OoAnHyK88z78zoPWYHzjvD2Gfg34CDPp9DIaEWugTFQWop3rGj9KXyCkAdbDXkm_ohO47xmXMuuS4_sENRQllXUh2xXxdEU8DRZD_Q-UjYm2wW1nHEvvfLgMPTOrMuuzfY5_MByWSP0bplNid0biMeArq4sjFa77LL3tAYkvhuKSQ3P6w_svcL7KP5tH9P2OPV5cPsJr_7eX07u7jLSfF6zAtUXVdsT-laEhWR0JpqRClaAVIZLGqkTshKaa0FVVSVSi1a3imOEgt5wr7ufH0cbRPJjoaeyDuXNmpAiDSFJ-hsBw3B_55MHJu0OZm-R2f8FBvQknPBq6pM6Olf6LOfgksnJGoLlRISBTtqc24MZtEMwa4wrBvgzSaj5p-MUs-XvfPUrkz3p-M1lATIvSmu2mC7pXkz-7-2L2Q0nBc |
CitedBy_id | crossref_primary_10_1007_s10853_024_09686_2 crossref_primary_10_1017_S1431927621013908 crossref_primary_10_1039_D2TC02312A crossref_primary_10_1017_S1431927616007844 crossref_primary_10_1002_adfm_202107017 crossref_primary_10_1126_science_aaw2781 crossref_primary_10_1016_j_matchar_2016_02_009 crossref_primary_10_1007_s10853_020_05417_5 crossref_primary_10_1111_jace_18242 crossref_primary_10_1021_acs_nanolett_7b02947 crossref_primary_10_1038_s41563_020_0794_5 crossref_primary_10_1116_1_4976622 crossref_primary_10_1038_srep43585 crossref_primary_10_1063_1_5063933 crossref_primary_10_1017_S1431927616005390 crossref_primary_10_1017_S1431927616009132 crossref_primary_10_1186_s40543_018_0142_4 crossref_primary_10_1017_S1431927617007887 crossref_primary_10_1021_acsami_8b00845 crossref_primary_10_1016_j_ultramic_2016_08_013 crossref_primary_10_1016_j_polymer_2018_01_011 crossref_primary_10_1039_D2TC01300B crossref_primary_10_1063_1_4974271 crossref_primary_10_1111_jmi_12601 crossref_primary_10_1016_j_trac_2017_02_010 crossref_primary_10_1002_admi_201701258 crossref_primary_10_1038_s43586_022_00095_w crossref_primary_10_1063_1_4963202 crossref_primary_10_1017_S1431927617008856 crossref_primary_10_1016_j_intermet_2016_03_006 |
Cites_doi | 10.1017/S1431927614013506 10.1126/science.1156446 10.1016/j.ultramic.2013.12.004 10.1016/j.commatsci.2005.04.010 10.1016/0022-3697(58)90139-2 10.1016/0022-3697(60)90094-9 10.1038/ncomms5155 10.1103/PhysRevA.43.3161 10.1016/j.ultramic.2014.10.011 10.1002/jcc.20575 10.1038/nmat3393 10.1063/1.4823801 10.1021/nl401186d 10.1007/978-1-4419-7200-2 10.1103/PhysRevB.77.045136 10.1016/0927-0256(96)00008-0 10.1093/jmicro/dfs045 10.1103/PhysRevB.54.11169 10.1103/PhysRevLett.77.3865 10.1016/0022-3697(63)90207-5 10.1103/PhysRevB.81.115126 10.1126/science.1135080 10.1107/S0021889801002242 10.1088/0953-8984/24/42/424218 10.1021/nl803235n 10.1103/PhysRevB.88.224108 10.1103/PhysRevLett.103.056401 10.1063/1.4793518 10.1016/j.ultramic.2009.11.014 10.1103/PhysRevB.50.17953 10.1038/491186a 10.1021/cm100440p 10.1103/PhysRevB.49.14251 10.1103/PhysRevB.47.558 10.1103/PhysRevB.79.115311 10.1088/0953-8984/21/8/084204 10.1103/PhysRevB.59.1758 10.1103/PhysRevLett.78.1396 |
ContentType | Journal Article |
Copyright | Microscopy Society of America 2015 |
Copyright_xml | – notice: Microscopy Society of America 2015 |
CorporateAuthor | Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS) |
CorporateAuthor_xml | – name: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS) |
DBID | NPM AAYXX CITATION 3V. 7QO 7RV 7TK 7X7 7XB 88E 8FD 8FE 8FG 8FH 8FI 8FJ 8FK ABUWG AFKRA ARAPS AZQEC BBNVY BENPR BGLVJ BHPHI CCPQU DWQXO FR3 FYUFA GHDGH GNUQQ HCIFZ K9. KB0 LK8 M0S M1P M7P NAPCQ P5Z P62 P64 PQEST PQQKQ PQUKI 7X8 OTOTI |
DOI | 10.1017/S1431927615013732 |
DatabaseName | PubMed CrossRef ProQuest Central (Corporate) Biotechnology Research Abstracts Nursing & Allied Health Database Neurosciences Abstracts Health & Medical Collection ProQuest Central (purchase pre-March 2016) Medical Database (Alumni Edition) Technology Research Database ProQuest SciTech Collection ProQuest Technology Collection ProQuest Natural Science Collection Hospital Premium Collection Hospital Premium Collection (Alumni Edition) ProQuest Central (Alumni) (purchase pre-March 2016) ProQuest Central (Alumni) ProQuest Central Advanced Technologies & Aerospace Collection ProQuest Central Essentials Biological Science Collection AUTh Library subscriptions: ProQuest Central Technology Collection ProQuest Natural Science Collection ProQuest One Community College ProQuest Central Korea Engineering Research Database Health Research Premium Collection Health Research Premium Collection (Alumni) ProQuest Central Student SciTech Premium Collection ProQuest Health & Medical Complete (Alumni) Nursing & Allied Health Database (Alumni Edition) Biological Sciences Health & Medical Collection (Alumni Edition) PML(ProQuest Medical Library) Biological Science Database Nursing & Allied Health Premium Advanced Technologies & Aerospace Database ProQuest Advanced Technologies & Aerospace Collection Biotechnology and BioEngineering Abstracts ProQuest One Academic Eastern Edition (DO NOT USE) ProQuest One Academic ProQuest One Academic UKI Edition MEDLINE - Academic OSTI.GOV |
DatabaseTitle | PubMed CrossRef ProQuest Central Student Technology Collection Technology Research Database ProQuest Advanced Technologies & Aerospace Collection ProQuest Central Essentials ProQuest Health & Medical Complete (Alumni) ProQuest Central (Alumni Edition) SciTech Premium Collection ProQuest One Community College ProQuest Natural Science Collection ProQuest Central Health Research Premium Collection Biotechnology Research Abstracts Health and Medicine Complete (Alumni Edition) Natural Science Collection ProQuest Central Korea Biological Science Collection ProQuest Medical Library (Alumni) Advanced Technologies & Aerospace Collection ProQuest Biological Science Collection ProQuest One Academic Eastern Edition ProQuest Nursing & Allied Health Source ProQuest Hospital Collection ProQuest Technology Collection Health Research Premium Collection (Alumni) Biological Science Database ProQuest SciTech Collection Neurosciences Abstracts ProQuest Hospital Collection (Alumni) Biotechnology and BioEngineering Abstracts Advanced Technologies & Aerospace Database Nursing & Allied Health Premium ProQuest Health & Medical Complete ProQuest Medical Library ProQuest One Academic UKI Edition ProQuest Nursing & Allied Health Source (Alumni) Engineering Research Database ProQuest One Academic ProQuest Central (Alumni) MEDLINE - Academic |
DatabaseTitleList | PubMed CrossRef ProQuest Central Student MEDLINE - Academic |
Database_xml | – sequence: 1 dbid: NPM name: PubMed url: https://proxy.k.utb.cz/login?url=http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed sourceTypes: Index Database – sequence: 2 dbid: 8FG name: ProQuest Technology Collection url: https://search.proquest.com/technologycollection1 sourceTypes: Aggregation Database |
DeliveryMethod | fulltext_linktorsrc |
Discipline | Biology |
DocumentTitleAlternate | Joseph H. Dycus et al. Accurate Nanoscale Crystallography in Real-Space |
EISSN | 1435-8115 |
EndPage | 952 |
ExternalDocumentID | 1225090 3763580721 10_1017_S1431927615013732 26169835 |
Genre | Journal Article Feature |
GroupedDBID | --- -E. .FH 09C 0E1 0R~ 123 29M 3V. 4.4 53G 5VS 5WD 74X 74Y 7RV 7X7 7~V 88E 8FE 8FG 8FH 8FI 8FJ 8R4 8R5 9M5 AAAZR AABES AABWE AACJH AAEED AAGFV AAKTX AARAB AASVR AATID AAUKB ABBXD ABEFU ABITZ ABJNI ABKKG ABMWE ABPTD ABQTM ABQWD ABROB ABTCQ ABUWG ABWCF ABWST ABZCX ACBEK ACBMC ACCHT ACFRR ACGFS ACIMK ACIPB ACIWK ACPRK ACQFJ ACQPF ACREK ACUFI ACUIJ ACUYZ ACWGA ACYZP ACZBM ACZUX ACZWT ADAZD ADBBV ADCGK ADFEC ADGEJ ADIPN ADIYS ADKIL ADOCW ADOVH ADQBN ADRDM ADVEK AEBAK AEHGV AEMTW AENEX AENGE AEYYC AFFUJ AFGWE AFKQG AFKRA AFKSM AFLOS AFLVW AFRAH AFUTZ AGABE AGBYD AGJUD AGOOT AHIPN AHLTW AHMBA AHQXX AIGNW AIHIV AIOIP AISIE AJ7 AJCYY AJPFC AJQAS ALMA_UNASSIGNED_HOLDINGS ALVPG ALWZO ANFBD ANPSP AQJOH ARABE ARAPS ATUCA AUXHV AZGZS BBLKV BBNVY BENPR BGHMG BGLVJ BGNMA BHPHI BKEYQ BLZWO BMAJL BPHCQ BRIRG BVXVI C0O CAG CBIIA CCPQU CCQAD CFAFE CJCSC COF CS3 DC4 DOHLZ DU5 EBS EJD EX3 F5P FYUFA HCIFZ HG- HMCUK HST HZ~ I.6 IH6 IOEEP IS6 I~P J36 J38 J3A JHPGK JKPOH JQKCU JVRFK KCGVB KFECR KOP L98 LAS LK8 LW7 M-V M1P M4Y M7P NAPCQ NIKVX NU0 O9- OBOKY OJZSN OVD OWPYF OYBOY P62 PQQKQ PROAC PSQYO PYCCK Q2X RAMDC RCA RIG RNS ROL RR0 S6- S6U SAAAG SDH SY4 T9M TEORI UKHRP UT1 UU6 VUG WFFJZ WOW WQ3 WXU WXY WYP ZYDXJ AAUAY ATGXG CTKSN H13 NPM AAYXX CITATION 7QO 7TK 7XB 8FD 8FK AZQEC DWQXO FR3 GNUQQ K9. P64 PQEST PQUKI 7X8 09E AAPXW AIAFM CHEAL OTOTI |
ID | FETCH-LOGICAL-c509t-4a5dd427615dbc28cc277c9aa32b2135ea49acd23857772c8c8655fb0d50a3a43 |
IEDL.DBID | BENPR |
ISSN | 1431-9276 |
IngestDate | Thu May 18 18:29:20 EDT 2023 Fri Oct 25 03:27:41 EDT 2024 Thu Oct 10 21:01:59 EDT 2024 Thu Sep 26 16:56:18 EDT 2024 Sat Sep 28 08:07:47 EDT 2024 Thu Mar 28 08:08:12 EDT 2024 |
IsDoiOpenAccess | false |
IsOpenAccess | true |
IsPeerReviewed | true |
IsScholarly | true |
Issue | 4 |
Keywords | Bi2Te3 scanning transmission electron microscopy atomic resolution spectroscopy nanoscale metrology |
Language | English |
LinkModel | DirectLink |
MergedId | FETCHMERGED-LOGICAL-c509t-4a5dd427615dbc28cc277c9aa32b2135ea49acd23857772c8c8655fb0d50a3a43 |
Notes | ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 USDOE Office of Science (SC) |
ORCID | 0000-0003-4862-4827 |
OpenAccessLink | https://research.monash.edu/files/252076909/3574711_oa.pdf |
PMID | 26169835 |
PQID | 1700208631 |
PQPubID | 33692 |
PageCount | 7 |
ParticipantIDs | osti_scitechconnect_1225090 proquest_miscellaneous_1730020886 proquest_journals_1700208631 crossref_primary_10_1017_S1431927615013732 pubmed_primary_26169835 cambridge_journals_10_1017_S1431927615013732 |
PublicationCentury | 2000 |
PublicationDate | 2015-08-01 |
PublicationDateYYYYMMDD | 2015-08-01 |
PublicationDate_xml | – month: 08 year: 2015 text: 2015-08-01 day: 01 |
PublicationDecade | 2010 |
PublicationPlace | New York, USA |
PublicationPlace_xml | – name: New York, USA – name: United States – name: Oxford |
PublicationTitle | Microscopy and microanalysis |
PublicationTitleAlternate | Microsc Microanal |
PublicationYear | 2015 |
Publisher | Cambridge University Press Oxford University Press Microscopy Society of America (MSA) |
Publisher_xml | – name: Cambridge University Press – name: Oxford University Press – name: Microscopy Society of America (MSA) |
References | Blöchl 1994; 50 Harl, Kresse 2008; 77 Kresse, Hafner 1994; 49 Nakajima 1963; 24 Kimoto, Asaka, Yu, Nagai, Matsui, Ishizuka 2010; 110 Kresse, Joubert 1999; 59 Lan, Poudel, Ma, Wang, Dresselhaus, Chen, Ren 2009; 9 Poudel, Hao, Ma, Lan, Minnich, Yu, Yan, Wang, Muto, Vashaee, Chen, Liu, Dresselhaus, Chen, Ren 2008; 320 Perdew, Burke, Ernzerhof 1996; 77 Kresse, Furthmüller 1996; 54 Chan, LeBeau, Venkatasubramanian, Thomas, Stuart, Koch 2013; 103 Harl, Schimka, Kresse 2010; 81 Henkelman, Arnaldsson, Jónsson 2006; 36 Martin, Wang, Chen, Nolas 2009; 79 Kresse, Furthmüller 1996; 6 Thomas 2012; 491 Denton, Ashcroft 1991; 43 Sang, Oni, LeBeau 2014; 20 Drabble, Goodman 1958; 5 Toby 2001; 34 Tang, Sanville, Henkelman 2009; 21 Dycus, White, Pierce, Venkatasubramanian, LeBeau 2013; 102 Björkman, Gulans, Krasheninnikov, Nieminen 2012; 24 Kim, He, Biegalski, Ambaye, Lauter, Christen, Pantelides, Pennycook, Kalinin, Borisevich 2012; 11 Wiese, Muldawer 1960; 15 Allen, D’Alfonso, Findlay 2015; 151 Billinge, Levin 2007; 316 Yankovich, Berkels, Dahmen, Binev, Sanchez, Bradley, Li, Szlufarska, Voyles 2014; 5 Sang, LeBeau 2014; 138 Jiang, Wang, Sagendorf, West, Kou, Wei, He, Wang, Zhang, Zhang 2013; 13 Page, Proffen, Niederberger, Seshadri 2010; 22 Park, Nomura, Arita, Llobet, Louca 2013; 88 Esteves, Fancher, Jones 2014 Sanville, Kenny, Smith, Henkelman 2007; 28 Kresse, Hafner 1993; 47 So, Kimoto 2012; 61 Perdew, Burke, Ernzerhof 1997; 78 Harl, Kresse 2009; 103 S1431927615013732_ref40 S1431927615013732_ref21 S1431927615013732_ref20 S1431927615013732_ref27 S1431927615013732_ref26 S1431927615013732_ref29 S1431927615013732_ref28 S1431927615013732_ref23 S1431927615013732_ref22 S1431927615013732_ref25 S1431927615013732_ref24 S1431927615013732_ref2 S1431927615013732_ref30 S1431927615013732_ref3 S1431927615013732_ref32 S1431927615013732_ref10 S1431927615013732_ref1 S1431927615013732_ref31 S1431927615013732_ref6 S1431927615013732_ref7 S1431927615013732_ref4 S1431927615013732_ref5 S1431927615013732_ref16 S1431927615013732_ref38 S1431927615013732_ref15 S1431927615013732_ref37 Esteves (S1431927615013732_ref9) 2014 S1431927615013732_ref18 S1431927615013732_ref17 S1431927615013732_ref39 S1431927615013732_ref12 S1431927615013732_ref34 S1431927615013732_ref33 S1431927615013732_ref11 S1431927615013732_ref14 S1431927615013732_ref36 S1431927615013732_ref35 S1431927615013732_ref13 S1431927615013732_ref19 S1431927615013732_ref8 |
References_xml | – volume: 36 start-page: 354 year: 2006 end-page: 360 article-title: A fast and robust algorithm for bader decomposition of charge density publication-title: Comput Mater Sci contributor: fullname: Jónsson – volume: 34 start-page: 210 year: 2001 end-page: 213 article-title: Expgui, a graphical user interface for GSAS publication-title: J Appl Crystallogr contributor: fullname: Toby – volume: 15 start-page: 13 year: 1960 end-page: 16 article-title: Lattice constants of Bi2Te3-Bi2Se3 solid solution alloys publication-title: J Phys Chem Solids contributor: fullname: Muldawer – year: 2014 article-title: In situ characterization of polycrystalline ferroelectrics using x-ray and neutron diffraction publication-title: J Mater Res contributor: fullname: Jones – volume: 22 start-page: 4386 year: 2010 end-page: 4391 article-title: Probing local dipoles and ligand structure in BaTiO 3 nanoparticles publication-title: Chem Mater contributor: fullname: Seshadri – volume: 11 start-page: 888 year: 2012 end-page: 894 article-title: Probing oxygen vacancy concentration and homogeneity in solid-oxide fuel-cell cathode materials on the subunit-cell level publication-title: Nat Mater contributor: fullname: Borisevich – volume: 59 start-page: 1758 year: 1999 article-title: From ultrasoft pseudopotentials to the projector augmented-wave method publication-title: Phys Rev B contributor: fullname: Joubert – volume: 9 start-page: 1419 year: 2009 end-page: 1422 article-title: Structure study of bulk nanograined thermoelectric bismuth antimony telluride publication-title: Nano Lett contributor: fullname: Ren – volume: 78 start-page: 1396 year: 1997 end-page: 1396 article-title: Generalized gradient approximation made simple publication-title: Phys Rev Lett contributor: fullname: Ernzerhof – volume: 81 start-page: 115126 year: 2010 article-title: Assessing the quality of the random phase approximation for lattice constants and atomization energies of solids publication-title: Phys Rev B contributor: fullname: Kresse – volume: 13 start-page: 2851 year: 2013 end-page: 2856 article-title: Direct atom-by-atom chemical identification of nanostructures and defects of topological insulators publication-title: Nano Lett contributor: fullname: Zhang – volume: 21 start-page: 084204 year: 2009 article-title: A grid-based bader analysis algorithm without lattice bias publication-title: J Phys Condens Matt contributor: fullname: Henkelman – volume: 43 start-page: 3161 year: 1991 end-page: 3164 article-title: Vegard’s law publication-title: Phys Rev A contributor: fullname: Ashcroft – volume: 138 start-page: 28 year: 2014 end-page: 35 article-title: Revolving scanning transmission electron microscopy: Correcting sample drift distortion without prior knowledge publication-title: Ultramicroscopy contributor: fullname: LeBeau – volume: 61 start-page: 207 year: 2012 end-page: 215 article-title: Effect of specimen misalignment on local structure analysis using annular dark-field imaging publication-title: J Electron Microsc (Tokyo) contributor: fullname: Kimoto – volume: 79 start-page: 115311 year: 2009 article-title: Enhanced See-beck coefficient through energy-barrier scattering in PbTe nanocomposites publication-title: Phys Rev B contributor: fullname: Nolas – volume: 103 start-page: 144106 year: 2013 article-title: Carrier concentration modulation by hot pressing pressure in n-type nanostructured Bi(Se)Te alloy publication-title: Appl Phys Lett contributor: fullname: Koch – volume: 110 start-page: 778 year: 2010 end-page: 782 article-title: Local crystal structure analysis with several picometer precision using scanning transmission electron microscopy publication-title: Ultramicroscopy contributor: fullname: Ishizuka – volume: 54 start-page: 11169 year: 1996 article-title: Efficient iterative schemes for ab initio total-energy calculations using a plane-wave basis set publication-title: Phys Rev B contributor: fullname: Furthmüller – volume: 77 start-page: 045136 year: 2008 article-title: Cohesive energy curves for noble gas solids calculated by adiabatic connection fluctuation-dissipation theory publication-title: Phys Rev B contributor: fullname: Kresse – volume: 47 start-page: 558 year: 1993 end-page: 561 article-title: Ab initio molecular dynamics for liquid metals publication-title: Phys Rev B contributor: fullname: Hafner – volume: 102 start-page: 081601 year: 2013 end-page: 081601-4 article-title: Atomic scale structure and chemistry of Bi2Te3/GaAs interfaces grown by metallorganic van der Waals epitaxy publication-title: Appl Phys Lett contributor: fullname: LeBeau – volume: 24 start-page: 479 year: 1963 end-page: 485 article-title: The crystal structure of Bi2Te3−x Se x publication-title: J Phys Chem Solids contributor: fullname: Nakajima – volume: 24 start-page: 424218 year: 2012 article-title: Are we van der Waals ready? publication-title: J Phys Condens Matter contributor: fullname: Nieminen – volume: 5 start-page: 142 year: 1958 end-page: 144 article-title: Chemical bonding in bismuth telluride publication-title: J Phys Chem Solids contributor: fullname: Goodman – volume: 88 start-page: 224108 year: 2013 article-title: Local strain and anharmonicity in the bonding of Bi2Se3Gx Te x topological insulators publication-title: Phys Rev B contributor: fullname: Louca – volume: 6 start-page: 15 year: 1996 end-page: 50 article-title: ). Efficiency of ab-initio total energy calculations for metals and semiconductors using a plane-wave basis set publication-title: Comput Mater Sci contributor: fullname: Furthmüller – volume: 320 start-page: 634 year: 2008 end-page: 638 article-title: High-thermoelectric performance of nanostructured bismuth antimony telluride bulk alloys publication-title: Science contributor: fullname: Ren – volume: 491 start-page: 186 year: 2012 end-page: 187 article-title: Centenary: The birth of X-ray crystallography publication-title: Nature contributor: fullname: Thomas – volume: 28 start-page: 899 year: 2007 end-page: 908 article-title: Improved grid-based algorithm for bader charge allocation publication-title: J Comput Chem contributor: fullname: Henkelman – volume: 316 start-page: 561 year: 2007 end-page: 565 article-title: The problem with determining atomic structure at the nanoscale publication-title: Science contributor: fullname: Levin – volume: 5 start-page: 4155 year: 2014 article-title: Picometre-precision analysis of scanning transmission electron microscopy images of platinum nanocatalysts publication-title: Nat Commun contributor: fullname: Voyles – volume: 151 start-page: 11 year: 2015 end-page: 22 article-title: Modelling the inelastic scattering of fast electrons publication-title: Ultramicroscopy contributor: fullname: Findlay – volume: 77 start-page: 3865 year: 1996 article-title: Generalized gradient approximation made simple publication-title: Phys Rev Lett contributor: fullname: Ernzerhof – volume: 49 start-page: 14251 year: 1994 article-title: Ab initio molecular-dynamics simulation of the liquid-metal-amorphous-semiconductor transition in germanium publication-title: Phys Rev B contributor: fullname: Hafner – volume: 50 start-page: 17953 year: 1994 article-title: Projector augmented-wave method publication-title: Phys Rev B contributor: fullname: Blöchl – volume: 20 start-page: 1764 year: 2014 end-page: 1771 article-title: Atom column indexing: Atomic resolution image analysis through a matrix representation publication-title: Microsc Microanal contributor: fullname: LeBeau – volume: 103 start-page: 056401 year: 2009 article-title: Accurate bulk properties from approximate many-body techniques publication-title: Phys Rev Lett contributor: fullname: Kresse – ident: S1431927615013732_ref33 doi: 10.1017/S1431927614013506 – ident: S1431927615013732_ref31 doi: 10.1126/science.1156446 – ident: S1431927615013732_ref32 doi: 10.1016/j.ultramic.2013.12.004 – ident: S1431927615013732_ref13 doi: 10.1016/j.commatsci.2005.04.010 – ident: S1431927615013732_ref7 doi: 10.1016/0022-3697(58)90139-2 – year: 2014 ident: S1431927615013732_ref9 article-title: In situ characterization of polycrystalline ferroelectrics using x-ray and neutron diffraction publication-title: J Mater Res contributor: fullname: Esteves – ident: S1431927615013732_ref39 doi: 10.1016/0022-3697(60)90094-9 – ident: S1431927615013732_ref40 doi: 10.1038/ncomms5155 – ident: S1431927615013732_ref6 doi: 10.1103/PhysRevA.43.3161 – ident: S1431927615013732_ref1 doi: 10.1016/j.ultramic.2014.10.011 – ident: S1431927615013732_ref34 doi: 10.1002/jcc.20575 – ident: S1431927615013732_ref16 doi: 10.1038/nmat3393 – ident: S1431927615013732_ref5 doi: 10.1063/1.4823801 – ident: S1431927615013732_ref14 doi: 10.1021/nl401186d – ident: S1431927615013732_ref28 doi: 10.1007/978-1-4419-7200-2 – ident: S1431927615013732_ref10 doi: 10.1103/PhysRevB.77.045136 – ident: S1431927615013732_ref17 doi: 10.1016/0927-0256(96)00008-0 – ident: S1431927615013732_ref35 doi: 10.1093/jmicro/dfs045 – ident: S1431927615013732_ref18 doi: 10.1103/PhysRevB.54.11169 – ident: S1431927615013732_ref29 doi: 10.1103/PhysRevLett.77.3865 – ident: S1431927615013732_ref25 doi: 10.1016/0022-3697(63)90207-5 – ident: S1431927615013732_ref12 doi: 10.1103/PhysRevB.81.115126 – ident: S1431927615013732_ref2 doi: 10.1126/science.1135080 – ident: S1431927615013732_ref38 doi: 10.1107/S0021889801002242 – ident: S1431927615013732_ref3 doi: 10.1088/0953-8984/24/42/424218 – ident: S1431927615013732_ref22 doi: 10.1021/nl803235n – ident: S1431927615013732_ref27 doi: 10.1103/PhysRevB.88.224108 – ident: S1431927615013732_ref11 doi: 10.1103/PhysRevLett.103.056401 – ident: S1431927615013732_ref8 doi: 10.1063/1.4793518 – ident: S1431927615013732_ref15 doi: 10.1016/j.ultramic.2009.11.014 – ident: S1431927615013732_ref4 doi: 10.1103/PhysRevB.50.17953 – ident: S1431927615013732_ref23 – ident: S1431927615013732_ref37 doi: 10.1038/491186a – ident: S1431927615013732_ref26 doi: 10.1021/cm100440p – ident: S1431927615013732_ref20 doi: 10.1103/PhysRevB.49.14251 – ident: S1431927615013732_ref19 doi: 10.1103/PhysRevB.47.558 – ident: S1431927615013732_ref24 doi: 10.1103/PhysRevB.79.115311 – ident: S1431927615013732_ref36 doi: 10.1088/0953-8984/21/8/084204 – ident: S1431927615013732_ref21 doi: 10.1103/PhysRevB.59.1758 – ident: S1431927615013732_ref30 doi: 10.1103/PhysRevLett.78.1396 |
SSID | ssj0003076 |
Score | 2.2940283 |
Snippet | Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made possible by... Abstract Here, we report reproducible and accurate measurement of crystallographic parameters using scanning transmission electron microscopy. This is made... |
SourceID | osti proquest crossref pubmed cambridge |
SourceType | Open Access Repository Aggregation Database Index Database Publisher |
StartPage | 946 |
SubjectTerms | Accuracy Alloys Calibration Crystal structure Crystallography Materials Applications and Techniques Software Transmission electron microscopy X-rays |
Title | Accurate Nanoscale Crystallography in Real-Space Using Scanning Transmission Electron Microscopy |
URI | https://www.cambridge.org/core/product/identifier/S1431927615013732/type/journal_article https://www.ncbi.nlm.nih.gov/pubmed/26169835 https://www.proquest.com/docview/1700208631 https://search.proquest.com/docview/1730020886 https://www.osti.gov/biblio/1225090 |
Volume | 21 |
hasFullText | 1 |
inHoldings | 1 |
isFullTextHit | |
isPrint | |
link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV1Li9swEB66CYW9lD63brZBhZ7KisaybNmnsg1JQyGhJBvIzZUlGRaKneZxyL_vjF-7pTQXH2Thx4xm5htpHgAfYx2b0EQ-j4UWXFoUqVj6ktvISStznVtFicLzRTRby--bcNNsuO2bsMpWJ1aK2paG9sg_Ux05gfg78L9sf3PqGkWnq00LjQvoC_QURA_6XyeLH8tOF-MKrvOLAp8nQkXtuSYVjaZBGkNI5AeK-o88VFf4y0r1SpS2_yPQyhJNn8OzBkKy25rnL-CJK17C07qp5OkV_Lw15kgFIBhqznKPPHBsvDshCvzV1qdm9wVbIkLkK_SYHavCBtjK1O2LWGW-kP20j8YmTZscNqfIPcphOb2G9XRyN57xpo8CNwgHDlzq0FpZ_anNjIiNEUqZROtAZMIPQqdloo1F4x0qBNsmNpStmmcjG450oGXwBnpFWbi3wNCbzvLEWWFRjlHasxzdKY0QC2GiROfJg5uOhmkjDfu0jiRT6T8k9-BTS-Z0W1fXODd5QIxIERpQfVtDgUDmkPqokUbJyIPrlj-PXtwtGg8-dLeRgnQqogtXHmlOUE2KIw-uar5234LuZZQgRn13_uEDuEQcFdZxgdfQO-yO7j1ilUM2hAu1UXiNp9-GzeL8A5kl5Bk |
link.rule.ids | 230,315,783,787,888,12070,12779,21402,27938,27939,31733,31734,33387,33388,33758,33759,43324,43614,43819 |
linkProvider | ProQuest |
linkToHtml | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV1ZS8QwEB50RfRFvK1nBJ_E4DZNrycRUdZjffCAfatpkoIg7eruPuy_d6aXiuhrG3rMZCbfJDPfABxFKtK-DlweCSW4NGhSkXQlN4GVRmYqMyEVCvfvg96zvBn4g3rDbVSnVTY-sXTUptC0R35KPHIC8bfnng3fOXWNotPVuoXGLMwRDxdx54eDNuCi-VtVF3kuj0UYNKeaRBlNF-kaAiLXC6n7yBe3wo81qlOgrf2NP8t16GoZlmoAyc4rja_AjM1XYb5qKTldg5dzrSdE_8DQbxYj1IBlFx9TxIBvDTs1e83ZA-JD_ojxsmVl0gB71FXzIlYuXqh82kVjl3WTHNanvD2qYJmuw_PV5dNFj9ddFLhGMDDmUvnGyPJPTapFpLUIQx0r5YlUuJ5vlYyVNrh0-yFCbR1pqlXN0q7xu8pT0tuATl7kdgsYxtJpFlsjDFox2nqaYTClEGAhSJQYOjlw0sowqW1hlFR5ZGHyS-QOHDdiToYVt8Z_g3dIEQkCA2K31ZQGpMeJi_6oG3cd2G308-3F7ZRx4LC9jRKkMxGV22JCY7xyUBQ4sFnptf0WDC6DGBHq9v8PP4CF3lP_Lrm7vr_dgUVEVH6VIbgLnfHHxO4hahmn--XU_ATd8ePX |
openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Accurate+Nanoscale+Crystallography+in+Real-Space+Using+Scanning+Transmission+Electron+Microscopy&rft.jtitle=Microscopy+and+microanalysis&rft.au=Dycus%2C+J+Houston&rft.au=Harris%2C+Joshua+S&rft.au=Sang%2C+Xiahan&rft.au=Fancher%2C+Chris+M&rft.date=2015-08-01&rft.pub=Oxford+University+Press&rft.issn=1431-9276&rft.eissn=1435-8115&rft.volume=21&rft.issue=4&rft.spage=946&rft_id=info:doi/10.1017%2FS1431927615013732&rft.externalDocID=3763580721 |
thumbnail_l | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=1431-9276&client=summon |
thumbnail_m | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=1431-9276&client=summon |
thumbnail_s | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=1431-9276&client=summon |