Adsorption of divalent metal ions from aqueous solutions using graphene oxide
The adsorptive properties of graphene oxide (GO) towards divalent metal ions (copper, zinc, cadmium and lead) were investigated. GO prepared through the oxidation of graphite using potassium dichromate was characterized by scanning electron microscopy (SEM), powder X-ray diffraction (XRD), X-ray pho...
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| Published in | Dalton transactions : an international journal of inorganic chemistry Vol. 42; no. 16; pp. 5682 - 5689 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
28.04.2013
|
| Subjects | |
| Online Access | Get full text |
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| Abstract | The adsorptive properties of graphene oxide (GO) towards divalent metal ions (copper, zinc, cadmium and lead) were investigated. GO prepared through the oxidation of graphite using potassium dichromate was characterized by scanning electron microscopy (SEM), powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and infrared spectroscopy (FT-IR). The results of batch experiments and measurements by flame atomic absorption spectrometry (F-AAS) indicate that maximum adsorption can be achieved in broad pH ranges: 3-7 for Cu(
ii
), 5-8 for Zn(
ii
), 4-8 for Cd(
ii
), 3-7 for Pb(
ii
). The maximum adsorption capacities of Cu(
ii
), Zn(
ii
), Cd(
ii
) and Pb(
ii
) on GO at pH = 5 are 294, 345, 530, 1119 mg g
−1
, respectively. The competitive adsorption experiments showed the affinity in the order of Pb(
ii
) > Cu(
ii
) > Cd(
ii
) > Zn(
ii
). Adsorption isotherms and kinetic studies suggest that sorption of metal ions on GO nanosheets is monolayer coverage and adsorption is controlled by chemical adsorption involving the strong surface complexation of metal ions with the oxygen-containing groups on the surface of GO. Chemisorption was confirmed by XPS (binding energy and shape of O1s and C1s peaks) of GO with adsorbed metal ions. The adsorption experiments show that the dispersibility of GO in water changes remarkably after complexation of metal ions. After adsorption, the tendency to agglomerate and precipitate is observed. Excellent dispersibility of GO and strong tendency of GO-Me(
ii
) to precipitate open the path to removal of heavy metals from water solution. Potential application of GO in analytical chemistry as a solid sorbent for preconcentration of trace elements and in heavy metal ion pollution cleanup results from its maximum adsorption capacities that are much higher than those of any of the currently reported sorbents.
The adsorptive properties of graphene oxide towards divalent metal ions (copper, zinc, cadmium and lead) have been investigated. |
|---|---|
| AbstractList | The adsorptive properties of graphene oxide (GO) towards divalent metal ions (copper, zinc, cadmium and lead) were investigated. GO prepared through the oxidation of graphite using potassium dichromate was characterized by scanning electron microscopy (SEM), powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and infrared spectroscopy (FT-IR). The results of batch experiments and measurements by flame atomic absorption spectrometry (F-AAS) indicate that maximum adsorption can be achieved in broad pH ranges: 3-7 for Cu(ii), 5-8 for Zn(ii), 4-8 for Cd(ii), 3-7 for Pb(ii). The maximum adsorption capacities of Cu(ii), Zn(ii), Cd(ii) and Pb(ii) on GO at pH = 5 are 294, 345, 530, 1119 mg g super(-1), respectively. The competitive adsorption experiments showed the affinity in the order of Pb(ii) > Cu(ii) >> Cd(ii) > Zn(ii). Adsorption isotherms and kinetic studies suggest that sorption of metal ions on GO nanosheets is monolayer coverage and adsorption is controlled by chemical adsorption involving the strong surface complexation of metal ions with the oxygen-containing groups on the surface of GO. Chemisorption was confirmed by XPS (binding energy and shape of O1s and C1s peaks) of GO with adsorbed metal ions. The adsorption experiments show that the dispersibility of GO in water changes remarkably after complexation of metal ions. After adsorption, the tendency to agglomerate and precipitate is observed. Excellent dispersibility of GO and strong tendency of GO-Me(ii) to precipitate open the path to removal of heavy metals from water solution. Potential application of GO in analytical chemistry as a solid sorbent for preconcentration of trace elements and in heavy metal ion pollution cleanup results from its maximum adsorption capacities that are much higher than those of any of the currently reported sorbents. The adsorptive properties of graphene oxide (GO) towards divalent metal ions (copper, zinc, cadmium and lead) were investigated. GO prepared through the oxidation of graphite using potassium dichromate was characterized by scanning electron microscopy (SEM), powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and infrared spectroscopy (FT-IR). The results of batch experiments and measurements by flame atomic absorption spectrometry (F-AAS) indicate that maximum adsorption can be achieved in broad pH ranges: 3-7 for Cu(II), 5-8 for Zn(II), 4-8 for Cd(II), 3-7 for Pb(II). The maximum adsorption capacities of Cu(II), Zn(II), Cd(II) and Pb(II) on GO at pH = 5 are 294, 345, 530, 1119 mg g(-1), respectively. The competitive adsorption experiments showed the affinity in the order of Pb(II) > Cu(II) ≫ Cd(II) > Zn(II). Adsorption isotherms and kinetic studies suggest that sorption of metal ions on GO nanosheets is monolayer coverage and adsorption is controlled by chemical adsorption involving the strong surface complexation of metal ions with the oxygen-containing groups on the surface of GO. Chemisorption was confirmed by XPS (binding energy and shape of O1s and C1s peaks) of GO with adsorbed metal ions. The adsorption experiments show that the dispersibility of GO in water changes remarkably after complexation of metal ions. After adsorption, the tendency to agglomerate and precipitate is observed. Excellent dispersibility of GO and strong tendency of GO-Me(II) to precipitate open the path to removal of heavy metals from water solution. Potential application of GO in analytical chemistry as a solid sorbent for preconcentration of trace elements and in heavy metal ion pollution cleanup results from its maximum adsorption capacities that are much higher than those of any of the currently reported sorbents. The adsorptive properties of graphene oxide (GO) towards divalent metal ions (copper, zinc, cadmium and lead) were investigated. GO prepared through the oxidation of graphite using potassium dichromate was characterized by scanning electron microscopy (SEM), powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and infrared spectroscopy (FT-IR). The results of batch experiments and measurements by flame atomic absorption spectrometry (F-AAS) indicate that maximum adsorption can be achieved in broad pH ranges: 3-7 for Cu( ii ), 5-8 for Zn( ii ), 4-8 for Cd( ii ), 3-7 for Pb( ii ). The maximum adsorption capacities of Cu( ii ), Zn( ii ), Cd( ii ) and Pb( ii ) on GO at pH = 5 are 294, 345, 530, 1119 mg g −1 , respectively. The competitive adsorption experiments showed the affinity in the order of Pb( ii ) > Cu( ii ) > Cd( ii ) > Zn( ii ). Adsorption isotherms and kinetic studies suggest that sorption of metal ions on GO nanosheets is monolayer coverage and adsorption is controlled by chemical adsorption involving the strong surface complexation of metal ions with the oxygen-containing groups on the surface of GO. Chemisorption was confirmed by XPS (binding energy and shape of O1s and C1s peaks) of GO with adsorbed metal ions. The adsorption experiments show that the dispersibility of GO in water changes remarkably after complexation of metal ions. After adsorption, the tendency to agglomerate and precipitate is observed. Excellent dispersibility of GO and strong tendency of GO-Me( ii ) to precipitate open the path to removal of heavy metals from water solution. Potential application of GO in analytical chemistry as a solid sorbent for preconcentration of trace elements and in heavy metal ion pollution cleanup results from its maximum adsorption capacities that are much higher than those of any of the currently reported sorbents. The adsorptive properties of graphene oxide towards divalent metal ions (copper, zinc, cadmium and lead) have been investigated. The adsorptive properties of graphene oxide (GO) towards divalent metal ions (copper, zinc, cadmium and lead) were investigated. GO prepared through the oxidation of graphite using potassium dichromate was characterized by scanning electron microscopy (SEM), powder X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and infrared spectroscopy (FT-IR). The results of batch experiments and measurements by flame atomic absorption spectrometry (F-AAS) indicate that maximum adsorption can be achieved in broad pH ranges: 3-7 for Cu(II), 5-8 for Zn(II), 4-8 for Cd(II), 3-7 for Pb(II). The maximum adsorption capacities of Cu(II), Zn(II), Cd(II) and Pb(II) on GO at pH = 5 are 294, 345, 530, 1119 mg g(-1), respectively. The competitive adsorption experiments showed the affinity in the order of Pb(II) > Cu(II) ≫ Cd(II) > Zn(II). Adsorption isotherms and kinetic studies suggest that sorption of metal ions on GO nanosheets is monolayer coverage and adsorption is controlled by chemical adsorption involving the strong surface complexation of metal ions with the oxygen-containing groups on the surface of GO. Chemisorption was confirmed by XPS (binding energy and shape of O1s and C1s peaks) of GO with adsorbed metal ions. The adsorption experiments show that the dispersibility of GO in water changes remarkably after complexation of metal ions. After adsorption, the tendency to agglomerate and precipitate is observed. Excellent dispersibility of GO and strong tendency of GO-Me(II) to precipitate open the path to removal of heavy metals from water solution. Potential application of GO in analytical chemistry as a solid sorbent for preconcentration of trace elements and in heavy metal ion pollution cleanup results from its maximum adsorption capacities that are much higher than those of any of the currently reported sorbents. |
| Author | Heimann, Jan Sitko, Rafal Wrzalik, Roman Turek, Edyta Malicka, Ewa Feist, Barbara Talik, Ewa Zawisza, Beata Gagor, Anna |
| AuthorAffiliation | Institute of Physics Institute of Chemistry University of Silesia Polish Academy of Sciences Institute of Low Temperature and Structure Research |
| AuthorAffiliation_xml | – name: Institute of Low Temperature and Structure Research – name: Institute of Chemistry – name: Institute of Physics – name: Polish Academy of Sciences – name: University of Silesia |
| Author_xml | – sequence: 1 givenname: Rafal surname: Sitko fullname: Sitko, Rafal – sequence: 2 givenname: Edyta surname: Turek fullname: Turek, Edyta – sequence: 3 givenname: Beata surname: Zawisza fullname: Zawisza, Beata – sequence: 4 givenname: Ewa surname: Malicka fullname: Malicka, Ewa – sequence: 5 givenname: Ewa surname: Talik fullname: Talik, Ewa – sequence: 6 givenname: Jan surname: Heimann fullname: Heimann, Jan – sequence: 7 givenname: Anna surname: Gagor fullname: Gagor, Anna – sequence: 8 givenname: Barbara surname: Feist fullname: Feist, Barbara – sequence: 9 givenname: Roman surname: Wrzalik fullname: Wrzalik, Roman |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/23443993$$D View this record in MEDLINE/PubMed |
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