High-performance polyamide thin-film-nanocomposite reverse osmosis membranes containing hydrophobic zeolitic imidazolate framework-8
A hydrophobic, hydrothermally stable metal-organic framework (MOF) - zeolitic imidazolate framework-8 (ZIF-8) was successfully incorporated into the selective polyamide (PA) layer of thin-film nanocomposite (TFN) membranes for water desalination. The potential advantages of ZIF-8 over classic hydrop...
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| Published in | Journal of membrane science Vol. 476; pp. 303 - 310 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.02.2015
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| Subjects | |
| Online Access | Get full text |
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| Abstract | A hydrophobic, hydrothermally stable metal-organic framework (MOF) - zeolitic imidazolate framework-8 (ZIF-8) was successfully incorporated into the selective polyamide (PA) layer of thin-film nanocomposite (TFN) membranes for water desalination. The potential advantages of ZIF-8 over classic hydrophilic zeolite used in TFNs include: i) theoretically faster water transport within the framework and ii) better compatibility with the PA matrix. The TFN membranes were characterized with SEM, TEM, AFM, XPS, water contact angle measurements and reverse osmosis tests under 15.5bar hydraulic pressure with 2000ppm NaCl solution. Lab-made, nano-sized (~200nm) ZIF-8 increased water permeance to 3.35±0.08L/m2·h·bar at 0.4% (w/v) loading, 162% higher than the pristine PA membranes; meanwhile, high NaCl rejection was maintained. The TFN surface was less crosslinked and more hydrophilic than that of the pristine PA. A filler encapsulation mechanism was proposed for the effects of filler on TFN membrane surface morphology and properties. This study experimentally verified the potential use of ZIF-8 in advanced TFN RO membranes.
[Display omitted]
•ZIF-8-based TFN membranes were successfully prepared.•Lab-made, nano-sized ZIF-8 increased water flux up to 162%.•ZIF-8 exhibited no adverse effect on NaCl rejection. |
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| AbstractList | A hydrophobic, hydrothermally stable metal-organic framework (MOF) - zeolitic imidazolate framework-8 (ZIF-8) was successfully incorporated into the selective polyamide (PA) layer of thin-film nanocomposite (TFN) membranes for water desalination. The potential advantages of ZIF-8 over classic hydrophilic zeolite used in TFNs include: i) theoretically faster water transport within the framework and ii) better compatibility with the PA matrix. The TFN membranes were characterized with SEM, TEM, AFM, XPS, water contact angle measurements and reverse osmosis tests under 15.5 bar hydraulic pressure with 2000 ppm NaCl solution. Lab-made, nano-sized (~200 nm) ZIF-8 increased water permeance to 3.35 plus or minus 0.08 L/m super(2).h.bar at 0.4% (w/v) loading, 162% higher than the pristine PA membranes; meanwhile, high NaCl rejection was maintained. The TFN surface was less crosslinked and more hydrophilic than that of the pristine PA. A filler encapsulation mechanism was proposed for the effects of filler on TFN membrane surface morphology and properties. This study experimentally verified the potential use of ZIF-8 in advanced TFN RO membranes. A hydrophobic, hydrothermally stable metal-organic framework (MOF) - zeolitic imidazolate framework-8 (ZIF-8) was successfully incorporated into the selective polyamide (PA) layer of thin-film nanocomposite (TFN) membranes for water desalination. The potential advantages of ZIF-8 over classic hydrophilic zeolite used in TFNs include: i) theoretically faster water transport within the framework and ii) better compatibility with the PA matrix. The TFN membranes were characterized with SEM, TEM, AFM, XPS, water contact angle measurements and reverse osmosis tests under 15.5bar hydraulic pressure with 2000ppm NaCl solution. Lab-made, nano-sized (~200nm) ZIF-8 increased water permeance to 3.35±0.08L/m2·h·bar at 0.4% (w/v) loading, 162% higher than the pristine PA membranes; meanwhile, high NaCl rejection was maintained. The TFN surface was less crosslinked and more hydrophilic than that of the pristine PA. A filler encapsulation mechanism was proposed for the effects of filler on TFN membrane surface morphology and properties. This study experimentally verified the potential use of ZIF-8 in advanced TFN RO membranes. [Display omitted] •ZIF-8-based TFN membranes were successfully prepared.•Lab-made, nano-sized ZIF-8 increased water flux up to 162%.•ZIF-8 exhibited no adverse effect on NaCl rejection. A hydrophobic, hydrothermally stable metal-organic framework (MOF) - zeolitic imidazolate framework-8 (ZIF-8) was successfully incorporated into the selective polyamide (PA) layer of thin-film nanocomposite (TFN) membranes for water desalination. The potential advantages of ZIF-8 over classic hydrophilic zeolite used in TFNs include: i) theoretically faster water transport within the framework and ii) better compatibility with the PA matrix. The TFN membranes were characterized with SEM, TEM, AFM, XPS, water contact angle measurements and reverse osmosis tests under 15.5bar hydraulic pressure with 2000ppm NaCl solution. Lab-made, nano-sized (~200nm) ZIF-8 increased water permeance to 3.35±0.08L/m²·h·bar at 0.4% (w/v) loading, 162% higher than the pristine PA membranes; meanwhile, high NaCl rejection was maintained. The TFN surface was less crosslinked and more hydrophilic than that of the pristine PA. A filler encapsulation mechanism was proposed for the effects of filler on TFN membrane surface morphology and properties. This study experimentally verified the potential use of ZIF-8 in advanced TFN RO membranes. |
| Author | Duan, Jintang Pacheco, Federico Pan, Yichang Pinnau, Ingo Lai, Zhiping Litwiller, Eric |
| Author_xml | – sequence: 1 givenname: Jintang surname: Duan fullname: Duan, Jintang – sequence: 2 givenname: Yichang surname: Pan fullname: Pan, Yichang – sequence: 3 givenname: Federico surname: Pacheco fullname: Pacheco, Federico – sequence: 4 givenname: Eric surname: Litwiller fullname: Litwiller, Eric – sequence: 5 givenname: Zhiping surname: Lai fullname: Lai, Zhiping – sequence: 6 givenname: Ingo surname: Pinnau fullname: Pinnau, Ingo email: ingo.pinnau@kaust.edu.sa |
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| SubjectTerms | artificial membranes atomic force microscopy Contact angle coordination polymers crosslinking desalination encapsulation Fillers hydrophilicity hydrophobicity Interfacial polymerization Membranes nanocomposites Nanostructure Nanotechnology Polyamide resins polyamides Reluctance Reverse osmosis scanning electron microscopy sodium chloride Thin films Thin-film-nanocomposite transmission electron microscopy X-ray photoelectron spectroscopy zeolites ZIF-8 |
| Title | High-performance polyamide thin-film-nanocomposite reverse osmosis membranes containing hydrophobic zeolitic imidazolate framework-8 |
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