A cyclic bis[2]catenane metallacage
Catenated cages represent chemistry’s challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic bis[2]catenane is constructed through the coordination-driven self-assembly of the interlocked bis-metallacage, by the 90° Pt(II) heteroligation...
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| Published in | Nature communications Vol. 11; no. 1; pp. 2727 - 7 |
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| Main Authors | , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
01.06.2020
Nature Publishing Group Nature Portfolio |
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| Online Access | Get full text |
| ISSN | 2041-1723 2041-1723 |
| DOI | 10.1038/s41467-020-16556-3 |
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| Abstract | Catenated cages represent chemistry’s challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic bis[2]catenane is constructed through the coordination-driven self-assembly of the interlocked bis-metallacage, by the 90° Pt(II) heteroligation of the endo-functionalized double-bridged tweezer bearing pyridyl moieties and the tetra-carboxylated linker. NMR spectrometry, X-ray crystallography and mass spectrometry confirm the formation of a cyclic bis[2]catenane with “∞”-shaped topology via a 14-component self-assembly. Particularly, reversibly responsive transformation between the bis[2]catenane and the bis-metallacage can be realized by guest exchange, concentration effect and solvent effect. This work represents a novel example of a cyclic cage-based [2]catenane oligomer.
Catenated cages are challenging synthetic targets in chemistry. Here, the authors employ a multi-component coordination strategy using a Pt(II) heteroligation to construct a cyclic bis[2]catenane metallacage, which could be reversibly transformed between the catenated structure and the bis-metallacage. |
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| AbstractList | Catenated cages represent chemistry’s challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic bis[2]catenane is constructed through the coordination-driven self-assembly of the interlocked bis-metallacage, by the 90° Pt(II) heteroligation of the endo-functionalized double-bridged tweezer bearing pyridyl moieties and the tetra-carboxylated linker. NMR spectrometry, X-ray crystallography and mass spectrometry confirm the formation of a cyclic bis[2]catenane with “∞”-shaped topology via a 14-component self-assembly. Particularly, reversibly responsive transformation between the bis[2]catenane and the bis-metallacage can be realized by guest exchange, concentration effect and solvent effect. This work represents a novel example of a cyclic cage-based [2]catenane oligomer.
Catenated cages are challenging synthetic targets in chemistry. Here, the authors employ a multi-component coordination strategy using a Pt(II) heteroligation to construct a cyclic bis[2]catenane metallacage, which could be reversibly transformed between the catenated structure and the bis-metallacage. Catenated cages are challenging synthetic targets in chemistry. Here, the authors employ a multi-component coordination strategy using a Pt(II) heteroligation to construct a cyclic bis[2]catenane metallacage, which could be reversibly transformed between the catenated structure and the bis-metallacage. Catenated cages represent chemistry’s challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic bis[2]catenane is constructed through the coordination-driven self-assembly of the interlocked bis-metallacage, by the 90° Pt(II) heteroligation of the endo-functionalized double-bridged tweezer bearing pyridyl moieties and the tetra-carboxylated linker. NMR spectrometry, X-ray crystallography and mass spectrometry confirm the formation of a cyclic bis[2]catenane with “∞”-shaped topology via a 14-component self-assembly. Particularly, reversibly responsive transformation between the bis[2]catenane and the bis-metallacage can be realized by guest exchange, concentration effect and solvent effect. This work represents a novel example of a cyclic cage-based [2]catenane oligomer.Catenated cages are challenging synthetic targets in chemistry. Here, the authors employ a multi-component coordination strategy using a Pt(II) heteroligation to construct a cyclic bis[2]catenane metallacage, which could be reversibly transformed between the catenated structure and the bis-metallacage. Catenated cages represent chemistry's challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic bis[2]catenane is constructed through the coordination-driven self-assembly of the interlocked bis-metallacage, by the 90° Pt(II) heteroligation of the endo-functionalized double-bridged tweezer bearing pyridyl moieties and the tetra-carboxylated linker. NMR spectrometry, X-ray crystallography and mass spectrometry confirm the formation of a cyclic bis[2]catenane with "∞"-shaped topology via a 14-component self-assembly. Particularly, reversibly responsive transformation between the bis[2]catenane and the bis-metallacage can be realized by guest exchange, concentration effect and solvent effect. This work represents a novel example of a cyclic cage-based [2]catenane oligomer. |
| ArticleNumber | 2727 |
| Author | Li, Chunju Vanderlinden, Ryan T. Fang, Jianhui Zhang, Yicheng Stang, Peter J. Li, Bin Jia, Xueshun Cui, Lei Zhou, Zhixuan Li, Xiaopeng Song, Bo Wang, Yiliang Li, Jian |
| Author_xml | – sequence: 1 givenname: Yiliang surname: Wang fullname: Wang, Yiliang organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 2 givenname: Yicheng surname: Zhang fullname: Zhang, Yicheng organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 3 givenname: Zhixuan orcidid: 0000-0001-8295-5860 surname: Zhou fullname: Zhou, Zhixuan organization: Department of Chemistry, University of Utah – sequence: 4 givenname: Ryan T. surname: Vanderlinden fullname: Vanderlinden, Ryan T. organization: Department of Chemistry, University of Utah – sequence: 5 givenname: Bin surname: Li fullname: Li, Bin organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 6 givenname: Bo orcidid: 0000-0002-4337-848X surname: Song fullname: Song, Bo organization: Department of Chemistry, University of South Florida – sequence: 7 givenname: Xiaopeng orcidid: 0000-0001-9655-9551 surname: Li fullname: Li, Xiaopeng organization: Department of Chemistry, University of South Florida – sequence: 8 givenname: Lei surname: Cui fullname: Cui, Lei organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 9 givenname: Jian surname: Li fullname: Li, Jian organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 10 givenname: Xueshun surname: Jia fullname: Jia, Xueshun organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 11 givenname: Jianhui surname: Fang fullname: Fang, Jianhui organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University – sequence: 12 givenname: Chunju orcidid: 0000-0001-7450-4867 surname: Li fullname: Li, Chunju email: cjli@shu.edu.cn organization: School of Materials Science and Engineering, Center for Supramolecular Chemistry and Catalysis and Department of Chemistry, Shanghai University, Key Laboratory of Inorganic-Organic Hybrid Functional Material Chemistry, Ministry of Education, Tianjin Key Laboratory of Structure and Performance for Functional Molecules, College of Chemistry, Tianjin Normal University – sequence: 13 givenname: Peter J. surname: Stang fullname: Stang, Peter J. email: stang@chem.utah.edu organization: Department of Chemistry, University of Utah |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/32483119$$D View this record in MEDLINE/PubMed |
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| Snippet | Catenated cages represent chemistry’s challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic... Catenated cages represent chemistry's challenging synthetic targets because a three-dimensional assembly is necessary for their formation. Herein, a cyclic... Catenated cages are challenging synthetic targets in chemistry. Here, the authors employ a multi-component coordination strategy using a Pt(II) heteroligation... |
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| SubjectTerms | 140/131 140/58 639/638/541 639/638/911 Cages Coordination Crystallography Humanities and Social Sciences Magnetic resonance spectroscopy Mass spectrometry Mass spectroscopy multidisciplinary NMR Nuclear magnetic resonance Science Science (multidisciplinary) Scientific imaging Self-assembly Solvent effect Spectroscopy Topology X-ray crystallography |
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| Title | A cyclic bis[2]catenane metallacage |
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