Electrochemical characterization of a PEM water electrolyzer based on a sulfonated polysulfone membrane

A polymer electrolyte membrane (PEM) based on a non-perfluorinated polymer as an alternative to Nafion was investigated for application in a water electrolyzer. The sulfonated polysulfone (SPSf) was synthesized using trimethyl silyl chlorosulfonate as the sulfonating agent. The SPSf polymer was used...

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Published inJournal of membrane science Vol. 448; pp. 209 - 214
Main Authors Siracusano, S., Baglio, V., Lufrano, F., Staiti, P., Aricò, A.S.
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 01.12.2013
Elsevier
Subjects
Applied sciences
Cathodic polarization
Chemistry
Colloidal state and disperse state
Crossovers
Current density
Electrochemistry
Electrolytes
Electrolytic cells
Exact sciences and technology
Exchange resins and membranes
Forms of application and semi-finished materials
General and physical chemistry
Membranes
Non-perfluorinated polymers
PEM electrolyzer
Polarization
Polymer industry, paints, wood
Polysulfone resins
Sulfonated polysulfone membrane
Technology of polymers
Water electrolysis
Water electrolysis
Sulfonated polysulfone membrane
PEM electrolyzer
Non-perfluorinated polymers
Characterization
Water
Polymeric membrane
Electrolysis
Electrochemistry
Polymer
Electrolyzer
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Abstract A polymer electrolyte membrane (PEM) based on a non-perfluorinated polymer as an alternative to Nafion was investigated for application in a water electrolyzer. The sulfonated polysulfone (SPSf) was synthesized using trimethyl silyl chlorosulfonate as the sulfonating agent. The SPSf polymer was used for the preparation of a proton conducting membrane. A single cell (5cm2 geometrical area) PEM electrolyzer based on SPSf membrane, IrO2 anode and Pt/C cathode electrocatalysts was investigated by polarization, impedance spectroscopy, chrono-amperometry and gas crossover measurements. The performance was compared to that of an electrolyzer based on a standard Nafion 115 membrane. The electrolyzer based on SPSf showed polarization and hydrogen permeation characteristics similar to those of Nafion. After 35h potentiostatic operation at 1.8V, the sulfonated polysulfone MEA reached a current density of 1.35Acm−2. The results indicate promising performance of the sulfonated polysulfone polymer electrolyte membrane for application in a PEM electrolyzer. •A membrane based on a non-perfluorinated polymer was investigated in a PEM-WE.•The performance was compared to that of an electrolyzer based on a Nafion 115.•The results indicate promising performance of the SPSf membrane in a PEM electrolyzer.
AbstractList A polymer electrolyte membrane (PEM) based on a non-perfluorinated polymer as an alternative to Nafion was investigated for application in a water electrolyzer. The sulfonated polysulfone (SPSf) was synthesized using trimethyl silyl chlorosulfonate as the sulfonating agent. The SPSf polymer was used for the preparation of a proton conducting membrane. A single cell (5cm2 geometrical area) PEM electrolyzer based on SPSf membrane, IrO2 anode and Pt/C cathode electrocatalysts was investigated by polarization, impedance spectroscopy, chrono-amperometry and gas crossover measurements. The performance was compared to that of an electrolyzer based on a standard Nafion 115 membrane. The electrolyzer based on SPSf showed polarization and hydrogen permeation characteristics similar to those of Nafion. After 35h potentiostatic operation at 1.8V, the sulfonated polysulfone MEA reached a current density of 1.35Acm−2. The results indicate promising performance of the sulfonated polysulfone polymer electrolyte membrane for application in a PEM electrolyzer. •A membrane based on a non-perfluorinated polymer was investigated in a PEM-WE.•The performance was compared to that of an electrolyzer based on a Nafion 115.•The results indicate promising performance of the SPSf membrane in a PEM electrolyzer.
A polymer electrolyte membrane (PEM) based on a non-perfluorinated polymer as an alternative to Nafion was investigated for application in a water electrolyzer. The sulfonated polysulfone (SPSf) was synthesized using trimethyl silyl chlorosulfonate as the sulfonating agent. The SPSf polymer was used for the preparation of a proton conducting membrane. A single cell (5 cm2 geometrical area) PEM electrolyzer based on SPSf membrane, IrO2 anode and Pt/C cathode electrocatalysts was investigated by polarization, impedance spectroscopy, chrono-amperometry and gas crossover measurements. The performance was compared to that of an electrolyzer based on a standard Nafion 115 membrane. The electrolyzer based on SPSf showed polarization and hydrogen permeation characteristics similar to those of Nafion. After 35 h potentiostatic operation at 1.8 V, the sulfonated polysulfone MEA reached a current density of 1.35 A cm-2. The results indicate promising performance of the sulfonated polysulfone polymer electrolyte membrane for application in a PEM electrolyzer.
Author Staiti, P.
Baglio, V.
Lufrano, F.
Siracusano, S.
Aricò, A.S.
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  surname: Lufrano
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  surname: Staiti
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  surname: Aricò
  fullname: Aricò, A.S.
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Keywords Water electrolysis
Sulfonated polysulfone membrane
PEM electrolyzer
Non-perfluorinated polymers
Characterization
Water
Polymeric membrane
Electrolysis
Electrochemistry
Polymer
Electrolyzer
Language English
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Snippet A polymer electrolyte membrane (PEM) based on a non-perfluorinated polymer as an alternative to Nafion was investigated for application in a water...
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SubjectTerms Applied sciences
Cathodic polarization
Chemistry
Colloidal state and disperse state
Crossovers
Current density
Electrochemistry
Electrolytes
Electrolytic cells
Exact sciences and technology
Exchange resins and membranes
Forms of application and semi-finished materials
General and physical chemistry
Membranes
Non-perfluorinated polymers
PEM electrolyzer
Polarization
Polymer industry, paints, wood
Polysulfone resins
Sulfonated polysulfone membrane
Technology of polymers
Water electrolysis
Title Electrochemical characterization of a PEM water electrolyzer based on a sulfonated polysulfone membrane
URI https://dx.doi.org/10.1016/j.memsci.2013.07.058
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