Microwave-assisted synthesis of NiS2 nanostructures for supercapacitors and cocatalytic enhancing photocatalytic H2 production
Uniform NiS 2 nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS 2 nanocubes, nanospheres and nanoparticles are obtained by controlling microwave reaction time. NiS 2 nanomaterials are primarily applied to supercapacitors and cocatalytic enhancing photocataly...
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| Published in | Scientific reports Vol. 4; no. 1; p. 3577 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
06.01.2014
Nature Publishing Group |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Uniform NiS
2
nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS
2
nanocubes, nanospheres and nanoparticles are obtained by controlling microwave reaction time. NiS
2
nanomaterials are primarily applied to supercapacitors and cocatalytic enhancing photocatalytic H
2
production. Different morphologies of NiS
2
nanostructures show different electrochemical and cocatalytic enhancing H
2
production activities. Benefited novel nanostructures, NiS
2
nanocube electrodes show a large specific capacitance (695 F g
−1
at 1.25 A g
−1
) and excellent cycling performance (the retention 93.4% of initial specific capacitance after 3000 cycles). More importantly, NiS
2
nanospheres show highly cocatalytic enhancing photocatalytic for H
2
evolution, in which the photocatalytic H
2
production is up to 3400 μmol during 12 hours under irradiation of visible light (λ>420 nm) with an average H
2
production rate of 283 μmol h
−1
. |
|---|---|
| AbstractList | Uniform NiS2 nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS2 nanocubes, nanospheres and nanoparticles are obtained by controlling microwave reaction time. NiS2 nanomaterials are primarily applied to supercapacitors and cocatalytic enhancing photocatalytic H2 production. Different morphologies of NiS2 nanostructures show different electrochemical and cocatalytic enhancing H2 production activities. Benefited novel nanostructures, NiS2 nanocube electrodes show a large specific capacitance (695 F g(-1) at 1.25 A g(-1)) and excellent cycling performance (the retention 93.4% of initial specific capacitance after 3000 cycles). More importantly, NiS2 nanospheres show highly cocatalytic enhancing photocatalytic for H2 evolution, in which the photocatalytic H2 production is up to 3400 μmol during 12 hours under irradiation of visible light (λ>420 nm) with an average H2 production rate of 283 μmol h(-1). Uniform NiS2 nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS2 nanocubes, nanospheres and nanoparticles are obtained by controlling microwave reaction time. NiS2 nanomaterials are primarily applied to supercapacitors and cocatalytic enhancing photocatalytic H2 production. Different morphologies of NiS2 nanostructures show different electrochemical and cocatalytic enhancing H2 production activities. Benefited novel nanostructures, NiS2 nanocube electrodes show a large specific capacitance (695 F g(-1) at 1.25 A g(-1)) and excellent cycling performance (the retention 93.4% of initial specific capacitance after 3000 cycles). More importantly, NiS2 nanospheres show highly cocatalytic enhancing photocatalytic for H2 evolution, in which the photocatalytic H2 production is up to 3400 μmol during 12 hours under irradiation of visible light (λ>420 nm) with an average H2 production rate of 283 μmol h(-1).Uniform NiS2 nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS2 nanocubes, nanospheres and nanoparticles are obtained by controlling microwave reaction time. NiS2 nanomaterials are primarily applied to supercapacitors and cocatalytic enhancing photocatalytic H2 production. Different morphologies of NiS2 nanostructures show different electrochemical and cocatalytic enhancing H2 production activities. Benefited novel nanostructures, NiS2 nanocube electrodes show a large specific capacitance (695 F g(-1) at 1.25 A g(-1)) and excellent cycling performance (the retention 93.4% of initial specific capacitance after 3000 cycles). More importantly, NiS2 nanospheres show highly cocatalytic enhancing photocatalytic for H2 evolution, in which the photocatalytic H2 production is up to 3400 μmol during 12 hours under irradiation of visible light (λ>420 nm) with an average H2 production rate of 283 μmol h(-1). Uniform NiS 2 nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS 2 nanocubes, nanospheres and nanoparticles are obtained by controlling microwave reaction time. NiS 2 nanomaterials are primarily applied to supercapacitors and cocatalytic enhancing photocatalytic H 2 production. Different morphologies of NiS 2 nanostructures show different electrochemical and cocatalytic enhancing H 2 production activities. Benefited novel nanostructures, NiS 2 nanocube electrodes show a large specific capacitance (695 F g −1 at 1.25 A g −1 ) and excellent cycling performance (the retention 93.4% of initial specific capacitance after 3000 cycles). More importantly, NiS 2 nanospheres show highly cocatalytic enhancing photocatalytic for H 2 evolution, in which the photocatalytic H 2 production is up to 3400 μmol during 12 hours under irradiation of visible light (λ>420 nm) with an average H 2 production rate of 283 μmol h −1 . |
| ArticleNumber | 3577 |
| Author | Zhang, Jiangshan Li, Xuexue Ma, Yahui Li, Sujuan Pang, Huan Li, Guochang Wei, Chengzhen Chen, Jing |
| Author_xml | – sequence: 1 givenname: Huan surname: Pang fullname: Pang, Huan organization: College of Chemistry and Chemical Engineering, Anyang Normal University, State Key Laboratory of Coordination Chemistry, Nanjing University – sequence: 2 givenname: Chengzhen surname: Wei fullname: Wei, Chengzhen organization: College of Chemistry and Chemical Engineering, Anyang Normal University – sequence: 3 givenname: Xuexue surname: Li fullname: Li, Xuexue organization: College of Chemistry and Chemical Engineering, Anyang Normal University – sequence: 4 givenname: Guochang surname: Li fullname: Li, Guochang organization: College of Chemistry and Chemical Engineering, Anyang Normal University – sequence: 5 givenname: Yahui surname: Ma fullname: Ma, Yahui organization: College of Chemistry and Chemical Engineering, Anyang Normal University – sequence: 6 givenname: Sujuan surname: Li fullname: Li, Sujuan organization: College of Chemistry and Chemical Engineering, Anyang Normal University – sequence: 7 givenname: Jing surname: Chen fullname: Chen, Jing organization: College of Chemistry and Chemical Engineering, Anyang Normal University – sequence: 8 givenname: Jiangshan surname: Zhang fullname: Zhang, Jiangshan organization: College of Chemistry and Chemical Engineering, Anyang Normal University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/24389929$$D View this record in MEDLINE/PubMed |
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| Snippet | Uniform NiS
2
nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS
2
nanocubes, nanospheres and nanoparticles are... Uniform NiS2 nanocubes are successfully synthesized with a microwave-assisted method. Interestingly, NiS2 nanocubes, nanospheres and nanoparticles are obtained... |
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| Title | Microwave-assisted synthesis of NiS2 nanostructures for supercapacitors and cocatalytic enhancing photocatalytic H2 production |
| URI | https://link.springer.com/article/10.1038/srep03577 https://www.ncbi.nlm.nih.gov/pubmed/24389929 https://www.proquest.com/docview/1897793699 https://www.proquest.com/docview/1490706820 https://pubmed.ncbi.nlm.nih.gov/PMC3880961 |
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