Use of Chènevotte, a Valuable Co-Product of Industrial Hemp Fiber, as Adsorbent for Pollutant Removal. Part I: Chemical, Microscopic, Spectroscopic and Thermogravimetric Characterization of Raw and Modified Samples

FINEAU (2021–2024) is a trans-disciplinary research project involving French, Serbian, Italian, Portuguese and Romanian colleagues, a French agricultural cooperative and two surface-treatment industries, intending to propose chènevotte, a co-product of the hemp industry, as an adsorbent for the remo...

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Published inMolecules (Basel, Switzerland) Vol. 26; no. 15; p. 4574
Main Authors Mongioví, Chiara, Lacalamita, Dario, Morin-Crini, Nadia, Gabrion, Xavier, Ivanovska, Aleksandra, Sala, Federico, Placet, Vincent, Rizzi, Vito, Gubitosa, Jennifer, Mesto, Ernesto, Ribeiro, Ana Rita Lado, Fini, Paola, Vietro, Nicoletta De, Schingaro, Emanuela, Kostić, Mirjana, Cosentino, Cesare, Cosma, Pinalysa, Bradu, Corina, Chanet, Gilles, Crini, Grégorio
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 28.07.2021
MDPI
Subjects
Adsorbents
Agricultural cooperatives
Cellulose
characterization
Chemical analysis
Chemical composition
Chemical treatment
chènevotte
Computed tomography
Fourier analysis
Fourier transforms
Hemp
hemp shives
Hydrogen bonds
Impurities
Industrial pollution
Infrared analysis
Infrared spectroscopy
Insulation
Lignin
Magnetic resonance spectroscopy
Mechanics
Morphology
NMR
NMR spectroscopy
Nuclear magnetic resonance
Physics
Pollutant removal
Pollutants
Research projects
Scanning electron microscopy
Spectroscopy
Spectrum analysis
surface analysis
Textiles
Thermogravimetric analysis
Wastewater
Wastewater pollution
Water treatment
X-ray diffraction
France
Europe
surface analysis
hemp shives
chènevotte
characterization
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Abstract FINEAU (2021–2024) is a trans-disciplinary research project involving French, Serbian, Italian, Portuguese and Romanian colleagues, a French agricultural cooperative and two surface-treatment industries, intending to propose chènevotte, a co-product of the hemp industry, as an adsorbent for the removal of pollutants from polycontaminated wastewater. The first objective of FINEAU was to prepare and characterize chènevotte-based materials. In this study, the impact of water washing and treatments (KOH, Na2CO3 and H3PO4) on the composition and structure of chènevotte (also called hemp shives) was evaluated using chemical analysis, X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), energy-dispersive X-ray (EDX) spectroscopy, X-ray computed nanotomography (nano-CT), attenuated total reflectance–Fourier transform infrared (ATR-FTIR) spectroscopy, solid state NMR spectroscopy and thermogravimetric analysis. The results showed that all these techniques are complementary and useful to characterize the structure and morphology of the samples. Before any chemical treatment, the presence of impurities with a compact unfibrillated structure on the surfaces of chènevotte samples was found. Data indicated an increase in the crystallinity index and significant changes in the chemical composition of each sample after treatment as well as in surface morphology and roughness. The most significant changes were observed in alkaline-treated samples, especially those treated with KOH.
AbstractList FINEAU (2021–2024) is a trans-disciplinary research project involving French, Serbian, Italian, Portuguese and Romanian colleagues, a French agricultural cooperative and two surface-treatment industries, intending to propose chènevotte, a co-product of the hemp industry, as an adsorbent for the removal of pollutants from polycontaminated wastewater. The first objective of FINEAU was to prepare and characterize chènevotte-based materials. In this study, the impact of water washing and treatments (KOH, Na2CO3 and H3PO4) on the composition and structure of chènevotte (also called hemp shives) was evaluated using chemical analysis, X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), energy-dispersive X-ray (EDX) spectroscopy, X-ray computed nanotomography (nano-CT), attenuated total reflectance–Fourier transform infrared (ATR-FTIR) spectroscopy, solid state NMR spectroscopy and thermogravimetric analysis. The results showed that all these techniques are complementary and useful to characterize the structure and morphology of the samples. Before any chemical treatment, the presence of impurities with a compact unfibrillated structure on the surfaces of chènevotte samples was found. Data indicated an increase in the crystallinity index and significant changes in the chemical composition of each sample after treatment as well as in surface morphology and roughness. The most significant changes were observed in alkaline-treated samples, especially those treated with KOH.
FINEAU (2021–2024) is a trans-disciplinary research project involving French, Serbian, Italian, Portuguese and Romanian colleagues, a French agricultural cooperative and two surface-treatment industries, intending to propose chènevotte, a co-product of the hemp industry, as an adsorbent for the removal of pollutants from polycontaminated wastewater. The first objective of FINEAU was to prepare and characterize chènevotte-based materials. In this study, the impact of water washing and treatments (KOH, Na 2 CO 3 and H 3 PO 4 ) on the composition and structure of chènevotte (also called hemp shives) was evaluated using chemical analysis, X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), energy-dispersive X-ray (EDX) spectroscopy, X-ray computed nanotomography (nano-CT), attenuated total reflectance–Fourier transform infrared (ATR-FTIR) spectroscopy, solid state NMR spectroscopy and thermogravimetric analysis. The results showed that all these techniques are complementary and useful to characterize the structure and morphology of the samples. Before any chemical treatment, the presence of impurities with a compact unfibrillated structure on the surfaces of chènevotte samples was found. Data indicated an increase in the crystallinity index and significant changes in the chemical composition of each sample after treatment as well as in surface morphology and roughness. The most significant changes were observed in alkaline-treated samples, especially those treated with KOH.
Author Cosma, Pinalysa
Mongioví, Chiara
Placet, Vincent
Vietro, Nicoletta De
Rizzi, Vito
Mesto, Ernesto
Crini, Grégorio
Fini, Paola
Ribeiro, Ana Rita Lado
Lacalamita, Dario
Bradu, Corina
Chanet, Gilles
Kostić, Mirjana
Gabrion, Xavier
Cosentino, Cesare
Morin-Crini, Nadia
Gubitosa, Jennifer
Ivanovska, Aleksandra
Sala, Federico
Schingaro, Emanuela
AuthorAffiliation 9 Department of Textile Engineering, Faculty of Technology and Metallurgy, University of Belgrade, Karnegijeva 4, 11000 Belgrade, Serbia; kostic@tmf.bg.ac.rs
8 Consiglio Nazionale delle Ricerche CNR-IPCF, UOS Bari, via Orabona 4, 70126 Bari, Italy; p.fini@ba.ipcf.cnr.it
10 PROTMED Research Centre, Department of Systems Ecology and Sustainability, University of Bucharest, Spl. Independentei 91-95, 050095 Bucharest, Romania; corina.bradu@g.unibuc.ro
1 Laboratoire Chrono-Environnement, UMR 6249, UFR Sciences et Techniques, Université Bourgogne Franche-Comté, 16 Route de Gray, 25000 Besançon, France; chiara.mongiovi@univ-fcomte.fr (C.M.); dario.lacalamita@univ-fcomte.fr (D.L.); nadia.crini@univ-fcomte.fr (N.M.-C.)
2 FEMTO-ST, CNRS/UFC/ENSMM/UTBM, Department of Applied Mechanics, Université Bourgogne Franche-Comté, 16 Route de Gray, 25000 Besançon, France; xavier.gabrion@univ-fcomte.fr (X.G.); vincent.placet@univ-fcomte.fr (V.P.)
4 Istituto di Chimica e Biochimica G. Ronzoni, via G. Colombo 81,
AuthorAffiliation_xml – name: 7 Laboratory of Separation and Reaction Engineering-Laboratory of Catalysis and Materials (LSRE-LCM), Faculdade de Engenharia, Universidade do Porto, Rua Dr. Roberto Frias s/n, 4200-465 Porto, Portugal; ritalado@fe.up.pt
– name: 9 Department of Textile Engineering, Faculty of Technology and Metallurgy, University of Belgrade, Karnegijeva 4, 11000 Belgrade, Serbia; kostic@tmf.bg.ac.rs
– name: 2 FEMTO-ST, CNRS/UFC/ENSMM/UTBM, Department of Applied Mechanics, Université Bourgogne Franche-Comté, 16 Route de Gray, 25000 Besançon, France; xavier.gabrion@univ-fcomte.fr (X.G.); vincent.placet@univ-fcomte.fr (V.P.)
– name: 6 Dipartimento di Scienze della Terra e Geoambientali, Università degli Studi di Bari “Aldo Moro”, via E. Orabona 4, 70125 Bari, Italy; ernesto.mesto@uniba.it (E.M.); emanuela.schingaro@uniba.it (E.S.)
– name: 10 PROTMED Research Centre, Department of Systems Ecology and Sustainability, University of Bucharest, Spl. Independentei 91-95, 050095 Bucharest, Romania; corina.bradu@g.unibuc.ro
– name: 11 Eurochanvre, 7 Route de Dijon, 70100 Arc-les-Gray, France; gilles.chanet@interval.coop
– name: 3 Innovation Center, Department of Textile Engineering, Faculty of Technology and Metallurgy, University of Belgrade, Karnegijeva 4, 11000 Belgrade, Serbia; aivanovska@tmf.bg.ac.rs
– name: 8 Consiglio Nazionale delle Ricerche CNR-IPCF, UOS Bari, via Orabona 4, 70126 Bari, Italy; p.fini@ba.ipcf.cnr.it
– name: 4 Istituto di Chimica e Biochimica G. Ronzoni, via G. Colombo 81, 20133 Milan, Italy; sala@ronzoni.it (F.S.); cosentino@ronzoni.it (C.C.)
– name: 1 Laboratoire Chrono-Environnement, UMR 6249, UFR Sciences et Techniques, Université Bourgogne Franche-Comté, 16 Route de Gray, 25000 Besançon, France; chiara.mongiovi@univ-fcomte.fr (C.M.); dario.lacalamita@univ-fcomte.fr (D.L.); nadia.crini@univ-fcomte.fr (N.M.-C.)
– name: 5 Dipartimento di Chimica, Università degli Studi “Aldo Moro” di Bari, via Orabona 4, 70126 Bari, Italy; vito.rizzi@uniba.it (V.R.); jennifer.gubitosa@uniba.it (J.G.); nicoletta.devietro@uniba.it (N.D.V.); pinalysa.cosma@uniba.it (P.C.)
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Issue 15
Keywords surface analysis
hemp shives
chènevotte
characterization
Language English
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Snippet FINEAU (2021–2024) is a trans-disciplinary research project involving French, Serbian, Italian, Portuguese and Romanian colleagues, a French agricultural...
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StartPage 4574
SubjectTerms Adsorbents
Agricultural cooperatives
Cellulose
characterization
Chemical analysis
Chemical composition
Chemical treatment
chènevotte
Computed tomography
Fourier analysis
Fourier transforms
Hemp
hemp shives
Hydrogen bonds
Impurities
Industrial pollution
Infrared analysis
Infrared spectroscopy
Insulation
Lignin
Magnetic resonance spectroscopy
Mechanics
Morphology
NMR
NMR spectroscopy
Nuclear magnetic resonance
Physics
Pollutant removal
Pollutants
Research projects
Scanning electron microscopy
Spectroscopy
Spectrum analysis
surface analysis
Textiles
Thermogravimetric analysis
Wastewater
Wastewater pollution
Water treatment
X-ray diffraction
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Title Use of Chènevotte, a Valuable Co-Product of Industrial Hemp Fiber, as Adsorbent for Pollutant Removal. Part I: Chemical, Microscopic, Spectroscopic and Thermogravimetric Characterization of Raw and Modified Samples
URI https://www.proquest.com/docview/2558867624
https://search.proquest.com/docview/2559437879
https://hal.science/hal-03427028
https://pubmed.ncbi.nlm.nih.gov/PMC8348367
https://doaj.org/article/8fcdb882678f4cff95ea0ed789e3a87c
Volume 26
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