Temperature gradients in the channels of a single-screw extruder
We used a temperature‐sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved doping polycarbonate with perylene and detecting fluorescence with an optical sensor that accesses a standard instrumentation port on a barrel...
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| Published in | Polymer engineering and science Vol. 44; no. 11; pp. 2148 - 2157 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Society of Plastics Engineers, Inc
01.11.2004
Wiley Subscription Services Blackwell Publishing Ltd |
| Subjects | |
| Online Access | Get full text |
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| Abstract | We used a temperature‐sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved doping polycarbonate with perylene and detecting fluorescence with an optical sensor that accesses a standard instrumentation port on a barrel of a single‐screw extruder. The sensor's confocal optics design permits fluorescence intensity measurements as a function of position. Using a previously established calibration function, temperature and temperature gradients were obtained from the measured fluorescence. Because the origin of the measurement is the fluorescent dye molecule that is soluble in the resin, this method allows temperature measurement of the polymer without interference from the surrounding metal parts. With the sensor looking over the screw, temperature profiles from the barrel wall to the core of the screw were obtained as a function of screw speed, screw design and resin melt flow rate. Polym. Eng. Sci. 44:2148–2157, 2004. © 2004 Society of Plastics Engineers.
This paper is a contribution from the National Institute of Standards and Technology, and, thus, is not subject to copyright in the United States. |
|---|---|
| AbstractList | We used a temperature-sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved doping polycarbonate with perylene and detecting fluorescence with an optical sensor that accesses a standard instrumentation port on a barrel of a single-screw extruder. The sensor's confocal optics design permits fluorescence intensity measurements as a function of position. Using a previously established calibration function, temperature and temperature gradients were obtained from the measured fluorescence. Because the origin of the measurement is the fluorescent dye molecule that is soluble in the resin, this method allows temperature measurement of the polymer without interference from the surrounding metal parts. With the sensor looking over the screw, temperature profiles from the barrel wall to the core of the screw were obtained as a function of screw speed, screw design and resin melt flow rate. [PUBLICATION ABSTRACT] We used a temperature‐sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved doping polycarbonate with perylene and detecting fluorescence with an optical sensor that accesses a standard instrumentation port on a barrel of a single‐screw extruder. The sensor's confocal optics design permits fluorescence intensity measurements as a function of position. Using a previously established calibration function, temperature and temperature gradients were obtained from the measured fluorescence. Because the origin of the measurement is the fluorescent dye molecule that is soluble in the resin, this method allows temperature measurement of the polymer without interference from the surrounding metal parts. With the sensor looking over the screw, temperature profiles from the barrel wall to the core of the screw were obtained as a function of screw speed, screw design and resin melt flow rate. Polym. Eng. Sci. 44:2148–2157, 2004. © 2004 Society of Plastics Engineers. This paper is a contribution from the National Institute of Standards and Technology, and, thus, is not subject to copyright in the United States. We used a temperature-sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved doping polycarbonate with perylene and detecting fluorescence with an optical sensor that accesses a standard instrumentation port on a barrel of a single-screw extruder. The sensor's confocal optics design permits fluorescence intensity measurements as a function of position. Using a previously established calibration function, temperature and temperature gradients were obtained from the measured fluorescence. Because the origin of the measurement is the fluorescent dye molecule that is soluble in the resin, this method allows temperature measurement of the polymer without interference from the surrounding metal parts. With the sensor looking over the screw, temperature profiles from the barrel wall to the core of the screw were obtained as a function of screw speed, screw design and resin melt flow rate. Polym. Eng. Sci. 44:2148-2157, 2004. © 2004 Society of Plastics Engineers. (†) The temperature of a molten polymer stream is a key processing prameters for many processes. We used a temperature-sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved doping polycarbonate with perylene and detecting fluorescence with an optical sensor that accesses a standard instrumentation port on a barrel of a single-screw extruder. The sensor's confocal optics design permits fluorescence intensity measurements as a function of position. Using a previously established calibration function, temperature and temperature gradients were obtained from the measured fluorescence. Because the origin of the measurement is the fluorescent dye molecule that is soluble in the resin, this method allows temperature measurement of the polymer without interference from the surrounding metal parts. With the sensor looting over the screw, temperature profiles from the barrel wall to the core of the screw were obtained as a function of screw speed, screw design and resin melt flow rate. |
| Audience | Academic |
| Author | Buzanowski, Walter C. Baugh, Daniel W. Bur, Anthony J. Spalding, Mark A. Koppi, Kurt A. Roth, Steven C. |
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| Cites_doi | 10.1002/pen.760070208 10.1002/pen.10838 10.1177/073168449701601708 10.1002/1439-2054(20020301)287:3<203::AID-MAME203>3.0.CO;2-8 10.1366/0003702021954638 10.1002/pen.10545 10.1002/pen.760110203 10.1002/adv.1994.060130204 10.1002/pen.10182 |
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| Keywords | Fluorescent tracer Process control Optical sensor Temperature control Measurement method Single screw extruder Perylene Experimental study Polycarbonate Extrusion molding |
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| References | A. J. Bur, M. G. Vangel, and S. C. Roth, Polym. Eng. Sci., 41, 1380 (2001). Z. Tadmor and I. Klein, in Engineering Principles of Plasticating Extrusion, Van Nostrand Reinhold Co., New York (1970). A. L. Kelly, E. C. Brown, and P. D. Coates, SPE ANTEC Tech. Papers, 49, 82 (2003). T. A. Hogan, M. A. Spalding, K. S. Cho, and C. I. Chung, SPE ANTEC Tech. Papers, 48, 384 (2002). E. C. Brown, A. L. Kelly, and P. D. Coates, SPE ANTEC Tech. Papers, 49, 77 (2003). T. W. McCullough and M. A. Spalding, J. Reinforced Plastics and Composites, 16, 1622 (1997). J. vanLeeuwen, Polym. Eng. Sci., 7, 98 (1967). T. W. McCullough and B. Hilton, SPE ANTEC Tech. Papers, 38, 927 (1992). K. B. Migler and A. J. Bur, Polym. Eng. Sci., 38, 213 (1998). A. J. Bur, M. G. Vangel, and S. Roth, Applied Spectroscopy, 56, 174 (2002). S. A. Somers, M. A. Spalding, J. Dooley, and K. S. Hyun, SPE ANTEC Tech. Papers, 48, 307 (2002). M. A. Spalding and K. S. Hyun, SPE ANTEC Tech. Papers, 49, 229 (2003). E. Haberstroh, L. Jakisch, E. Henssge, and P. Schwarz, Macromolecular Materials and Engineering, 287, 203 (2002). C. Maier, Polym. Eng. Sci., 36, 1502 (1996). H. Kim and E. Collins, Polym. Eng. Sci., 11, 83 (1971). M. Esseghir and V. Sernas, Adv. Polym. Technol., 13, 133 (1994). J. A. Myers and R. A. Barr, SPE ANTEC Tech. Papers, 48, 154 (2002). M. A. Spalding, J. Dooley, K. S. Hyun, and S. R. Strand, SPE ANTEC Tech. Papers, 39, 1533 (1993). 1998; 38 1967; 7 1971; 11 2002; 48 1993; 39 2001 2002; 56 2002; 287 2003; 49 1997; 16 1994; 13 1983 1970 1992; 38 1996; 36 2001; 41 Brown E. C. (e_1_2_1_3_2) 2003; 49 McCullough T. W. (e_1_2_1_7_2) 1997; 16 Myers J. A. (e_1_2_1_20_2) 2002; 48 Tadmor Z. (e_1_2_1_22_2) 1970 Hogan T. A. (e_1_2_1_17_2) 2002; 48 Kelly A. L. (e_1_2_1_4_2) 2003; 49 Spalding M. A. (e_1_2_1_18_2) 1993; 39 e_1_2_1_5_2 e_1_2_1_11_2 e_1_2_1_12_2 Spalding M. A. (e_1_2_1_23_2) 2003; 49 Spalding M. A. (e_1_2_1_2_2) 2001 e_1_2_1_10_2 e_1_2_1_15_2 e_1_2_1_16_2 e_1_2_1_13_2 McCullough T. W. (e_1_2_1_6_2) 1992; 38 e_1_2_1_14_2 e_1_2_1_19_2 Somers S. A. (e_1_2_1_21_2) 2002; 48 e_1_2_1_8_2 e_1_2_1_9_2 |
| References_xml | – reference: A. J. Bur, M. G. Vangel, and S. Roth, Applied Spectroscopy, 56, 174 (2002). – reference: J. A. Myers and R. A. Barr, SPE ANTEC Tech. Papers, 48, 154 (2002). – reference: T. A. Hogan, M. A. Spalding, K. S. Cho, and C. I. Chung, SPE ANTEC Tech. Papers, 48, 384 (2002). – reference: K. B. Migler and A. J. Bur, Polym. Eng. Sci., 38, 213 (1998). – reference: Z. Tadmor and I. Klein, in Engineering Principles of Plasticating Extrusion, Van Nostrand Reinhold Co., New York (1970). – reference: S. A. Somers, M. A. Spalding, J. Dooley, and K. S. Hyun, SPE ANTEC Tech. Papers, 48, 307 (2002). – reference: H. Kim and E. Collins, Polym. Eng. Sci., 11, 83 (1971). – reference: T. W. McCullough and B. Hilton, SPE ANTEC Tech. Papers, 38, 927 (1992). – reference: A. L. Kelly, E. C. Brown, and P. D. Coates, SPE ANTEC Tech. Papers, 49, 82 (2003). – reference: A. J. Bur, M. G. Vangel, and S. C. Roth, Polym. Eng. Sci., 41, 1380 (2001). – reference: M. A. Spalding, J. Dooley, K. S. Hyun, and S. R. Strand, SPE ANTEC Tech. Papers, 39, 1533 (1993). – reference: E. C. Brown, A. L. Kelly, and P. D. Coates, SPE ANTEC Tech. Papers, 49, 77 (2003). – reference: J. vanLeeuwen, Polym. Eng. Sci., 7, 98 (1967). – reference: T. W. McCullough and M. A. Spalding, J. Reinforced Plastics and Composites, 16, 1622 (1997). – reference: M. Esseghir and V. Sernas, Adv. Polym. Technol., 13, 133 (1994). – reference: E. Haberstroh, L. Jakisch, E. Henssge, and P. Schwarz, Macromolecular Materials and Engineering, 287, 203 (2002). – reference: C. Maier, Polym. Eng. Sci., 36, 1502 (1996). – reference: M. A. Spalding and K. S. Hyun, SPE ANTEC Tech. Papers, 49, 229 (2003). – volume: 7 start-page: 98 year: 1967 publication-title: Polym. Eng. Sci. – volume: 38 start-page: 213 year: 1998 publication-title: Polym. Eng. Sci. – year: 1983 – volume: 48 start-page: 154 year: 2002 publication-title: SPE ANTEC Tech. Papers – volume: 36 start-page: 1502 year: 1996 publication-title: Polym. Eng. Sci. – volume: 13 start-page: 133 year: 1994 publication-title: Adv. Polym. Technol. – volume: 56 start-page: 174 year: 2002 publication-title: Applied Spectroscopy – volume: 41 start-page: 1380 year: 2001 publication-title: Polym. Eng. Sci. – year: 2001 – volume: 48 start-page: 307 year: 2002 publication-title: SPE ANTEC Tech. Papers – volume: 11 start-page: 83 year: 1971 publication-title: Polym. Eng. Sci. – volume: 49 start-page: 229 year: 2003 publication-title: SPE ANTEC Tech. Papers – year: 1970 – volume: 49 start-page: 77 year: 2003 publication-title: SPE ANTEC Tech. Papers – volume: 38 start-page: 927 year: 1992 publication-title: SPE ANTEC Tech. Papers – volume: 48 start-page: 384 year: 2002 publication-title: SPE ANTEC Tech. Papers – volume: 39 start-page: 1533 year: 1993 publication-title: SPE ANTEC Tech. Papers – volume: 49 start-page: 82 year: 2003 publication-title: SPE ANTEC Tech. Papers – volume: 287 start-page: 203 year: 2002 publication-title: Macromolecular Materials and Engineering – volume: 16 start-page: 1622 year: 1997 publication-title: J. Reinforced Plastics and Composites – ident: e_1_2_1_8_2 doi: 10.1002/pen.760070208 – ident: e_1_2_1_13_2 doi: 10.1002/pen.10838 – volume: 49 start-page: 77 year: 2003 ident: e_1_2_1_3_2 publication-title: SPE ANTEC Tech. Papers – volume: 49 start-page: 82 year: 2003 ident: e_1_2_1_4_2 publication-title: SPE ANTEC Tech. Papers – volume: 48 start-page: 154 year: 2002 ident: e_1_2_1_20_2 publication-title: SPE ANTEC Tech. Papers – volume: 16 start-page: 1622 year: 1997 ident: e_1_2_1_7_2 publication-title: J. Reinforced Plastics and Composites doi: 10.1177/073168449701601708 – ident: e_1_2_1_11_2 doi: 10.1002/1439-2054(20020301)287:3<203::AID-MAME203>3.0.CO;2-8 – ident: e_1_2_1_14_2 doi: 10.1366/0003702021954638 – ident: e_1_2_1_12_2 doi: 10.1002/pen.10545 – ident: e_1_2_1_16_2 – volume-title: The SPE Guide on Extrusion Technology and Troubleshooting year: 2001 ident: e_1_2_1_2_2 – ident: e_1_2_1_9_2 doi: 10.1002/pen.760110203 – volume: 39 start-page: 1533 year: 1993 ident: e_1_2_1_18_2 publication-title: SPE ANTEC Tech. Papers – volume: 48 start-page: 384 year: 2002 ident: e_1_2_1_17_2 publication-title: SPE ANTEC Tech. Papers – ident: e_1_2_1_19_2 – ident: e_1_2_1_5_2 doi: 10.1002/pen.760110203 – volume: 38 start-page: 927 year: 1992 ident: e_1_2_1_6_2 publication-title: SPE ANTEC Tech. Papers – ident: e_1_2_1_10_2 doi: 10.1002/adv.1994.060130204 – volume-title: Engineering Principles of Plasticating Extrusion year: 1970 ident: e_1_2_1_22_2 – volume: 48 start-page: 307 year: 2002 ident: e_1_2_1_21_2 publication-title: SPE ANTEC Tech. Papers – volume: 49 start-page: 229 year: 2003 ident: e_1_2_1_23_2 publication-title: SPE ANTEC Tech. Papers – ident: e_1_2_1_15_2 doi: 10.1002/pen.10182 |
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| Snippet | We used a temperature‐sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved... We used a temperature-sensitive fluorescent dye, perylene, to monitor the true resin temperature during extrusion of polycarbonate. The measurement involved... The temperature of a molten polymer stream is a key processing prameters for many processes. We used a temperature-sensitive fluorescent dye, perylene, to... |
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| SubjectTerms | Analysis Applied sciences Chemical engineering Chemical processes Exact sciences and technology Extruders Extrusion moulding Fluorescence Machinery and processing Moulding Plastics Polycarbonate resins Polymer industry, paints, wood Technology of polymers Temperature |
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| Title | Temperature gradients in the channels of a single-screw extruder |
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