Measurement of the Thermophysical Properties of a Thermoplastic Ceramic Paste Across its Solidification Range Using Power-Compensated Differential Scanning Calorimeter
The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power‐compensated, differential scanning calorimeter (DSC) using the heat capacity spectral analysis method developed by Merzlyakov and Schick for measuring these paramet...
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| Published in | Journal of the American Ceramic Society Vol. 88; no. 11; pp. 3116 - 3124 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford, UK
Blackwell Science Inc
01.11.2005
Blackwell Wiley Subscription Services, Inc |
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| Abstract | The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power‐compensated, differential scanning calorimeter (DSC) using the heat capacity spectral analysis method developed by Merzlyakov and Schick for measuring these parameters on low thermal conductivity solids. The paste features an ultra‐fine zinc oxide powder (a number‐length mean diameter, D1,0, of 85 nm) as the discrete phase, and a thermoplastic continuous phase comprising a blend of organic waxes with a melting range of ca. 30°–70°C. This paste is formulated with a solids loading of 50 vol% and is currently used in a novel continuous casting process to manufacture pharmaceutical products. The properties of the paste were investigated over a temperature range encompassing the melt and solid states, and for solid loadings from 0 to 70 vol%. The results compare favorably with those obtained using transient line source and transient plane methods. |
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| AbstractList | The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power‐compensated, differential scanning calorimeter (DSC) using the heat capacity spectral analysis method developed by Merzlyakov and Schick for measuring these parameters on low thermal conductivity solids. The paste features an ultra‐fine zinc oxide powder (a number‐length mean diameter,
D
1,0
, of 85 nm) as the discrete phase, and a thermoplastic continuous phase comprising a blend of organic waxes with a melting range of ca. 30°–70°C. This paste is formulated with a solids loading of 50 vol% and is currently used in a novel continuous casting process to manufacture pharmaceutical products. The properties of the paste were investigated over a temperature range encompassing the melt and solid states, and for solid loadings from 0 to 70 vol%. The results compare favorably with those obtained using transient line source and transient plane methods. The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated using a power-compensated DSC using the heat capacity spectral analysis method developed by Merzlyakov and Schick for measuring these parameters on low thermal conductivity solids. The paste features an ultra-fine zinc oxide powder (a number-length mean diameter of 85 nm) as the discrete phase, and a thermoplastic continuous phase comprising a blend of organic waxes with a melting range of about 30-70 C. This paste is formulated with a solids loading of 50 vol% and is currently used in a novel continuous casting process to manufacture pharmaceutical products. The properties of the paste were investigated over a temperature range encompassing the melt and solid states, and for solids loadings from 0 to 70 vol%. The results compare favourably with those obtained using transient line source and transient plane methods. 20 refs. The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power-compensated, differential scanning calorimeter (DSC) using the heat capacity spectral analysis method developed by Merzlyakov and Schick for measuring these parameters on low thermal conductivity solids. The paste features an ultra-fine zinc oxide powder (a number-length mean diameter, D^sub 1,0^, of 85 nm) as the discrete phase, and a thermoplastic continuous phase comprising a blend of organic waxes with a melting range of ca. 30°-70°C. This paste is formulated with a solids loading of 50 vol% and is currently used in a novel continuous casting process to manufacture pharmaceutical products. The properties of the paste were investigated over a temperature range encompassing the melt and solid states, and for solid loadings from 0 to 70 vol%. The results compare favorably with those obtained using transient line source and transient plane methods. [PUBLICATION ABSTRACT] The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power‐compensated, differential scanning calorimeter (DSC) using the heat capacity spectral analysis method developed by Merzlyakov and Schick for measuring these parameters on low thermal conductivity solids. The paste features an ultra‐fine zinc oxide powder (a number‐length mean diameter, D1,0, of 85 nm) as the discrete phase, and a thermoplastic continuous phase comprising a blend of organic waxes with a melting range of ca. 30°–70°C. This paste is formulated with a solids loading of 50 vol% and is currently used in a novel continuous casting process to manufacture pharmaceutical products. The properties of the paste were investigated over a temperature range encompassing the melt and solid states, and for solid loadings from 0 to 70 vol%. The results compare favorably with those obtained using transient line source and transient plane methods. |
| Author | Barker, Dean A. Ian Wilson, D. |
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| Keywords | Differential scanning calorimetry Green properties Ceramic body Heat capacity Thermal diffusivity Experimental study Oxide ceramics Solidification Thermal conductivity Technical ceramics Zinc oxide Manufacturing Thermophysical properties |
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| References_xml | – volume: 93 start-page: 12 year: 1990 article-title: The Melting Behavior of Organic Materials Confined in Porous Solids publication-title: J. Chem. Phys. – volume: 23 start-page: 2 year: 1994 article-title: Thermal‐Diffusivity, Specific‐Heat, and Thermal‐Conductivity Of (Ca ,Mg )Zr (Po ) Ceramic publication-title: Mater. Sci. Eng. B-Solid State Mater. Adv. Technol. – volume: 377 start-page: 183 issue: 1–2 year: 2001 end-page: 91 article-title: Thermal Conductivity from Dynamic Response of DSC publication-title: Thermochim. Acta – year: 2001 – volume: 74 start-page: 14 year: 1999 article-title: Thermal Conductivity, Elastic Modulus, and Coefficient of Thermal Expansion of Polymer Composites Filled With Ceramic Particles for Electronic Packaging publication-title: J. Appl. Polym. Sci. – volume: 33 start-page: 8 year: 2002 article-title: Thermal and Electrical Properties of Magnetite Filled Polymers publication-title: Compos. Pt. A-Appl. Sci. Manuf. – year: 2000 – year: 1996 – volume: 419 start-page: 1 year: 2004 end-page: 2 article-title: Heat Capacity, Thermal Conductivity, and Thermal Expansion of Barium Titanate‐Based Ceramics publication-title: Thermochim. Acta – year: 1975 – volume: 33 start-page: 1 year: 1997 end-page: 2 article-title: Modelling the Thermal Conductivity of Starch‐Water Gels publication-title: J. Food Eng. – volume: 36 start-page: 3 year: 2005 article-title: Cooling Behaviour of Particle Filled Polypropylene During Injection Moulding Process publication-title: Compos. Pt. A-Appl. Sci. Manuf. – year: 1994 – volume: 62 start-page: 3 year: 1991 article-title: Transient Plane Source Techniques for Thermal‐Conductivity and Thermal‐Diffusivity Measurements of Solid Materials publication-title: Rev. Sci. Instrum. – volume: 18 start-page: 4 year: 1995 article-title: A Methodology for Laser‐Based Thermal Diffusivity Measurement of Advanced Multichip Module Ceramic Materials publication-title: IEEE Trans Compon. Packag. Manuf. Technol. Pt. A – year: 1999 – volume-title: CRC Handbook of Chemistry and Physics year: 1996 ident: e_1_2_6_19_2 contributor: fullname: Frederikse H. P. R. – volume-title: Benefits and Applications of the Power Compensated Pyris 1 DSC year: 2000 ident: e_1_2_6_17_2 contributor: fullname: Sichina W. J. – ident: e_1_2_6_18_2 doi: 10.1063/1.459240 – ident: e_1_2_6_5_2 doi: 10.1016/j.tca.2004.02.008 – ident: e_1_2_6_8_2 doi: 10.1016/0921-5107(94)90340-9 – ident: e_1_2_6_10_2 – ident: e_1_2_6_4_2 doi: 10.1016/S1359-835X(02)00085-4 – ident: e_1_2_6_6_2 doi: 10.1002/(SICI)1097-4628(19991227)74:14<3396::AID-APP13>3.0.CO;2-3 – volume: 18 start-page: 4 year: 1995 ident: e_1_2_6_7_2 article-title: A Methodology for Laser‐Based Thermal Diffusivity Measurement of Advanced Multichip Module Ceramic Materials publication-title: IEEE Trans Compon. Packag. Manuf. Technol. Pt. A contributor: fullname: Kehoe L. – volume-title: KD2 User's Manual version 1.0 Thermal Properties Analyzer year: 2001 ident: e_1_2_6_14_2 contributor: fullname: Decagon Devices Inc. – ident: e_1_2_6_21_2 doi: 10.1016/S0260-8774(97)00043-5 – volume-title: Thermal Conductivity of Solids year: 1975 ident: e_1_2_6_20_2 contributor: fullname: Parrott J. E. – ident: e_1_2_6_2_2 doi: 10.1016/S0040-6031(01)00553-6 – ident: e_1_2_6_3_2 doi: 10.1016/j.compositesa.2004.07.002 – volume-title: Polymer Extrusion year: 1994 ident: e_1_2_6_11_2 contributor: fullname: Rauwendaal C. – volume-title: A Stepwise Specific Heat Technique for Dynamic DSC year: 2000 ident: e_1_2_6_12_2 contributor: fullname: Cassel B – ident: e_1_2_6_15_2 – ident: e_1_2_6_16_2 doi: 10.1063/1.1142087 – ident: e_1_2_6_9_2 – volume-title: Pyris Software for Windows, ver. 3.81 year: 1999 ident: e_1_2_6_13_2 contributor: fullname: Perkin‐Elmer Inc. |
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| Snippet | The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power‐compensated,... The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated on a power-compensated,... The specific heat capacity, thermal conductivity, and thermal diffusivity of a thermoplastic ceramic paste were investigated using a power-compensated DSC... |
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| SubjectTerms | Applied sciences Building materials. Ceramics. Glasses Ceramic industries Ceramics Chemical industry and chemicals Differential scanning calorimetry Exact sciences and technology General studies Solidification Technical ceramics Temperature effects Thermoplastics |
| Title | Measurement of the Thermophysical Properties of a Thermoplastic Ceramic Paste Across its Solidification Range Using Power-Compensated Differential Scanning Calorimeter |
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