An Americium‐Containing Metal–Organic Framework: A Platform for Studying Transplutonium Elements
The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation and structure of Am‐GWMOF‐6, [Am2(C6H8O4)3(H2O)2][(C10H8N2)], is analogous to that of the isostructural trivalent lanthanide‐only containing material G...
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| Published in | Angewandte Chemie (International ed.) Vol. 58; no. 46; pp. 16508 - 16511 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Wiley Subscription Services, Inc
11.11.2019
Wiley Blackwell (John Wiley & Sons) |
| Edition | International ed. in English |
| Subjects | |
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| Abstract | The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation and structure of Am‐GWMOF‐6, [Am2(C6H8O4)3(H2O)2][(C10H8N2)], is analogous to that of the isostructural trivalent lanthanide‐only containing material GWMOF‐6. The presented MOF architecture is used as a platform to probe Am3+ coordination chemistry and guest‐enhanced luminescent emission, whereas the framework itself provides a means to monitor the effects of self‐irradiation upon crystallinity over time. Presented here is a discussion of these properties and the opportunities that MOFs provide in the structural and spectroscopic study of actinides.
The first transplutonium metal–organic framework (MOF), containing the trivalent actinide americium ([Am2(C6H8O4)3(H2O)2]⋅(C10H8N2)), is presented as Am‐GWMOF‐6, a structurally analogous compound to that of the trivalent lanthanide‐only containing material GWMOF‐6. The presented MOF architecture is used as a platform to probe Am3+ coordination chemistry and guest‐enhanced luminescent emission. |
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| AbstractList | The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation and structure of Am‐GWMOF‐6, [Am2(C6H8O4)3(H2O)2][(C10H8N2)], is analogous to that of the isostructural trivalent lanthanide‐only containing material GWMOF‐6. The presented MOF architecture is used as a platform to probe Am3+ coordination chemistry and guest‐enhanced luminescent emission, whereas the framework itself provides a means to monitor the effects of self‐irradiation upon crystallinity over time. Presented here is a discussion of these properties and the opportunities that MOFs provide in the structural and spectroscopic study of actinides. Abstract The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation and structure of Am‐GWMOF‐6, [Am 2 (C 6 H 8 O 4 ) 3 (H 2 O) 2 ][(C 10 H 8 N 2 )], is analogous to that of the isostructural trivalent lanthanide‐only containing material GWMOF‐6. The presented MOF architecture is used as a platform to probe Am 3+ coordination chemistry and guest‐enhanced luminescent emission, whereas the framework itself provides a means to monitor the effects of self‐irradiation upon crystallinity over time. Presented here is a discussion of these properties and the opportunities that MOFs provide in the structural and spectroscopic study of actinides. The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation and structure of Am‐GWMOF‐6, [Am2(C6H8O4)3(H2O)2][(C10H8N2)], is analogous to that of the isostructural trivalent lanthanide‐only containing material GWMOF‐6. The presented MOF architecture is used as a platform to probe Am3+ coordination chemistry and guest‐enhanced luminescent emission, whereas the framework itself provides a means to monitor the effects of self‐irradiation upon crystallinity over time. Presented here is a discussion of these properties and the opportunities that MOFs provide in the structural and spectroscopic study of actinides. The first transplutonium metal–organic framework (MOF), containing the trivalent actinide americium ([Am2(C6H8O4)3(H2O)2]⋅(C10H8N2)), is presented as Am‐GWMOF‐6, a structurally analogous compound to that of the trivalent lanthanide‐only containing material GWMOF‐6. The presented MOF architecture is used as a platform to probe Am3+ coordination chemistry and guest‐enhanced luminescent emission. The synthesis, structure, and spectroscopic characterization of the first transplutonium metal-organic framework (MOF) is described. The preparation and structure of Am-GWMOF-6, [Am (C H O ) (H O) ][(C H N )], is analogous to that of the isostructural trivalent lanthanide-only containing material GWMOF-6. The presented MOF architecture is used as a platform to probe Am coordination chemistry and guest-enhanced luminescent emission, whereas the framework itself provides a means to monitor the effects of self-irradiation upon crystallinity over time. Presented here is a discussion of these properties and the opportunities that MOFs provide in the structural and spectroscopic study of actinides. |
| Author | Koury, Daniel Surbella, Robert G. Gelis, Artem V. Ridenour, J. August Czerwinski, Kenneth R. Poineau, Frederic Cahill, Christopher L. |
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| Keywords | X-ray diffraction transplutonium luminescence americium metal-organic frameworks |
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| Snippet | The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation and... The synthesis, structure, and spectroscopic characterization of the first transplutonium metal-organic framework (MOF) is described. The preparation and... Abstract The synthesis, structure, and spectroscopic characterization of the first transplutonium metal–organic framework (MOF) is described. The preparation... |
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| SubjectTerms | Actinides Americium Irradiation luminescence Metal-organic frameworks Metals Organic chemistry Radiation Structural analysis transplutonium X-ray diffraction |
| Title | An Americium‐Containing Metal–Organic Framework: A Platform for Studying Transplutonium Elements |
| URI | https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fanie.201909988 https://www.ncbi.nlm.nih.gov/pubmed/31536176 https://www.proquest.com/docview/2311480064 https://search.proquest.com/docview/2293970137 https://www.osti.gov/biblio/1567890 |
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