The formation of onion-like carbon-encapsulated cobalt carbide core/shell nanoparticles by the laser ablation of metallic cobalt in acetone
We developed a new approach to obtain onion-like carbon-encapsulated cobalt carbide (Co3C) core/shell nanoparticles (NPs) by the laser ablation of cobalt in acetone. The as-synthesized core/shell NPs were then characterized by transmission electron microscopy (TEM), X-ray diffraction, Raman spectros...
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| Published in | Carbon (New York) Vol. 55; pp. 108 - 115 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
01.04.2013
Elsevier |
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| Abstract | We developed a new approach to obtain onion-like carbon-encapsulated cobalt carbide (Co3C) core/shell nanoparticles (NPs) by the laser ablation of cobalt in acetone. The as-synthesized core/shell NPs were then characterized by transmission electron microscopy (TEM), X-ray diffraction, Raman spectroscopy, superconducting quantum interference device magnetometer and fluorescence spectrophotometer. TEM observation reveals that the Co3C core is encapsulated by graphitized carbon layers. The number of carbon layers shows certain relationship with the size of the core Co3C NPs. The as-derived core/shell NPs presents unique superparamagnetic property and excitation wavelength-dependent fluorescence. The formation of the carbide and carbon layer can be explained by the laser-induced catalytic cracking of the carbon-rich precursor, acetone molecules. The supersaturated carbon atoms in carbide core tend to be excluded and automatically grow as carbon layers during the subsequent rapid quenching process. |
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| AbstractList | We developed a new approach to obtain onion-like carbon-encapsulated cobalt carbide (Co3C) core/shell nanoparticles (NPs) by the laser ablation of cobalt in acetone. The as-synthesized core/shell NPs were then characterized by transmission electron microscopy (TEM), X-ray diffraction, Raman spectroscopy, superconducting quantum interference device magnetometer and fluorescence spectrophotometer. TEM observation reveals that the Co3C core is encapsulated by graphitized carbon layers. The number of carbon layers shows certain relationship with the size of the core Co3C NPs. The as-derived core/shell NPs presents unique superparamagnetic property and excitation wavelength-dependent fluorescence. The formation of the carbide and carbon layer can be explained by the laser-induced catalytic cracking of the carbon-rich precursor, acetone molecules. The supersaturated carbon atoms in carbide core tend to be excluded and automatically grow as carbon layers during the subsequent rapid quenching process. We developed a new approach to obtain onion-like carbon-encapsulated cobalt carbide (Co₃C) core/shell nanoparticles (NPs) by the laser ablation of cobalt in acetone. The as-synthesized core/shell NPs were then characterized by transmission electron microscopy (TEM), X-ray diffraction, Raman spectroscopy, superconducting quantum interference device magnetometer and fluorescence spectrophotometer. TEM observation reveals that the Co₃C core is encapsulated by graphitized carbon layers. The number of carbon layers shows certain relationship with the size of the core Co₃C NPs. The as-derived core/shell NPs presents unique superparamagnetic property and excitation wavelength-dependent fluorescence. The formation of the carbide and carbon layer can be explained by the laser-induced catalytic cracking of the carbon-rich precursor, acetone molecules. The supersaturated carbon atoms in carbide core tend to be excluded and automatically grow as carbon layers during the subsequent rapid quenching process. |
| Author | Liang, Changhao Tian, Zhenfei Zhang, Hemin Shao, Guosheng Liu, Jun |
| Author_xml | – sequence: 1 givenname: Hemin surname: Zhang fullname: Zhang, Hemin organization: Key Laboratory of Materials Physics and Anhui Key Laboratory of Nanomaterials and Nanotechnology, Institute of Solid State Physics, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China – sequence: 2 givenname: Changhao surname: Liang fullname: Liang, Changhao email: chliang@issp.ac.cn organization: Key Laboratory of Materials Physics and Anhui Key Laboratory of Nanomaterials and Nanotechnology, Institute of Solid State Physics, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China – sequence: 3 givenname: Jun surname: Liu fullname: Liu, Jun organization: Key Laboratory of Materials Physics and Anhui Key Laboratory of Nanomaterials and Nanotechnology, Institute of Solid State Physics, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China – sequence: 4 givenname: Zhenfei surname: Tian fullname: Tian, Zhenfei organization: Key Laboratory of Materials Physics and Anhui Key Laboratory of Nanomaterials and Nanotechnology, Institute of Solid State Physics, Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China – sequence: 5 givenname: Guosheng surname: Shao fullname: Shao, Guosheng organization: Institute for Renewable Energy and Environmental Technologies. University of Bolton, Bolton BL3 5AB, UK |
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| Keywords | Encapsulation Raman spectra Ketones Cobalt carbide Core shell structure Pulsed laser deposition Laser ablation technique Superparamagnetism XRD Carbon Acetone |
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| Snippet | We developed a new approach to obtain onion-like carbon-encapsulated cobalt carbide (Co3C) core/shell nanoparticles (NPs) by the laser ablation of cobalt in... We developed a new approach to obtain onion-like carbon-encapsulated cobalt carbide (Co₃C) core/shell nanoparticles (NPs) by the laser ablation of cobalt in... |
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| SubjectTerms | Acetone Carbides Carbon catalytic cracking Cobalt Condensed matter: electronic structure, electrical, magnetic, and optical properties Cross-disciplinary physics: materials science; rheology Exact sciences and technology Fluorescence Laser ablation Magnetic properties and materials Magnetic properties of nanostructures Materials science Nanocrystalline materials nanoparticles Nanoscale materials and structures: fabrication and characterization Physics Raman spectroscopy Shells Transmission electron microscopy X-ray diffraction |
| Title | The formation of onion-like carbon-encapsulated cobalt carbide core/shell nanoparticles by the laser ablation of metallic cobalt in acetone |
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