Effect of sintering temperatures on the elastic properties of Mn (1%) added MgCuZn ferrites

Polycrystalline samples of Mn (1%) added MgCuZn ferrites were prepared by conventional solid-state reaction method. Samples were sintered at different temperatures in the range of 975–1175°C for 10h. The longitudinal wave velocity (Vl) and shear wave velocity (Vs) were measured using ultrasonic puls...

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Published inJournal of magnetism and magnetic materials Vol. 355; pp. 100 - 103
Main Authors Bhaskar, Ankam, Murthy, S.R.
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 01.04.2014
Elsevier
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Abstract Polycrystalline samples of Mn (1%) added MgCuZn ferrites were prepared by conventional solid-state reaction method. Samples were sintered at different temperatures in the range of 975–1175°C for 10h. The longitudinal wave velocity (Vl) and shear wave velocity (Vs) were measured using ultrasonic pulse transition technique. The values of Vl and Vs were increased with an increase in sintering temperature. Using these values of velocities; longitudinal modulus, rigidity modulus, bulk modulus, Young's modulus and Poisson's ratio were calculated. The values of elastic moduli were increased with an increase in sintering temperature. Poisson's ratio was constant for all the samples. The elastic moduli of samples were corrected to zero porosity using well-known models. Debye temperature and average sound velocity were calculated. Debye temperature and average sound velocity were increased with an increase in sintering temperature. A linear relationship between Debye temperature and average sound velocity was observed. These results suggest that sintering condition has a prominent effect on the elastic properties. •The bulk density increases and porosity decreases with an increase in sintering temperature.•The elastic moduli of samples increase with an increase in sintering temperature.•Poisson's ratio is constant for all the samples.•A linear relationship between average sound velocity and Debye temperature is observed.
AbstractList Polycrystalline samples of Mn (1%) added MgCuZn ferrites were prepared by conventional solid-state reaction method. Samples were sintered at different temperatures in the range of 975–1175°C for 10h. The longitudinal wave velocity (Vl) and shear wave velocity (Vs) were measured using ultrasonic pulse transition technique. The values of Vl and Vs were increased with an increase in sintering temperature. Using these values of velocities; longitudinal modulus, rigidity modulus, bulk modulus, Young's modulus and Poisson's ratio were calculated. The values of elastic moduli were increased with an increase in sintering temperature. Poisson's ratio was constant for all the samples. The elastic moduli of samples were corrected to zero porosity using well-known models. Debye temperature and average sound velocity were calculated. Debye temperature and average sound velocity were increased with an increase in sintering temperature. A linear relationship between Debye temperature and average sound velocity was observed. These results suggest that sintering condition has a prominent effect on the elastic properties. •The bulk density increases and porosity decreases with an increase in sintering temperature.•The elastic moduli of samples increase with an increase in sintering temperature.•Poisson's ratio is constant for all the samples.•A linear relationship between average sound velocity and Debye temperature is observed.
Polycrystalline samples of Mn (1%) added MgCuZn ferrites were prepared by conventional solid-state reaction method. Samples were sintered at different temperatures in the range of 975-1175 degree C for 10 h. The longitudinal wave velocity (V sub(l)) and shear wave velocity (V sub(s)) were measured using ultrasonic pulse transition technique. The values of V sub(l) and V sub(s) were increased with an increase in sintering temperature. Using these values of velocities; longitudinal modulus, rigidity modulus, bulk modulus, Young's modulus and Poisson's ratio were calculated. The values of elastic moduli were increased with an increase in sintering temperature. Poisson's ratio was constant for all the samples. The elastic moduli of samples were corrected to zero porosity using well-known models. Debye temperature and average sound velocity were calculated. Debye temperature and average sound velocity were increased with an increase in sintering temperature. A linear relationship between Debye temperature and average sound velocity was observed. These results suggest that sintering condition has a prominent effect on the elastic properties.
Polycrystalline samples of Mn (1%) added MgCuZn ferrites were prepared by conventional solid-state reaction method. Samples were sintered at different temperatures in the range of 975-1175 [degrees]C for 10 h. The longitudinal wave velocity (V sub(I)) and shear wave velocity (V sub(s)) were measured using ultrasonic pulse transition technique. The values of V sub(I) and V sub(s) were increased with an increase in sintering temperature. Using these values of velocities; longitudinal modulus, rigidity modulus, bulk modulus. Young's modulus and Poisson's ratio were calculated. The values of elastic moduli were increased with an increase in sintering temperature. Poisson's ratio was constant for all the samples. The elastic moduli of samples were corrected to zero porosity using well-known models. Debye temperature and average sound velocity were calculated. Debye temperature and average sound velocity were increased with an increase in sintering temperature. A linear relationship between Debye temperature and average sound velocity was observed. These results suggest that sintering condition has a prominent effect on the elastic properties.
Author Bhaskar, Ankam
Murthy, S.R.
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Keywords Ferrites
Debye temperature
Elastic properties
Sintering
Elastic modulus
Pulse techniques
Doping
Interatomic interaction
Manganese additions
Fabrication property relation
Sound velocity
Strain wave
Porosity
Ultrasonic method
Strain rate
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Snippet Polycrystalline samples of Mn (1%) added MgCuZn ferrites were prepared by conventional solid-state reaction method. Samples were sintered at different...
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SubjectTerms Condensed matter: structure, mechanical and thermal properties
Debye temperature
Elastic constants
Elastic properties
Elasticity, elastic constants
Exact sciences and technology
Ferrites
Manganese
Mathematical models
Mechanical and acoustical properties of condensed matter
Mechanical properties of solids
Modulus of elasticity
Physics
Poissons ratio
Sintering
Sintering (powder metallurgy)
Sound velocity
Title Effect of sintering temperatures on the elastic properties of Mn (1%) added MgCuZn ferrites
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Volume 355
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