The Differentiation of the Volatile Organic Signatures of Individuals Through SPME-GC/MS of Characteristic Human Scent Compounds
: Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an indi...
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| Published in | Journal of forensic sciences Vol. 55; no. 1; pp. 50 - 57 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford, UK
Blackwell Publishing Ltd
01.01.2010
Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0022-1198 1556-4029 1556-4029 |
| DOI | 10.1111/j.1556-4029.2009.01236.x |
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| Abstract | : Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an individual’s “primary odor” compounds utilized to determine a reproducible and individualizing profile which can be stored in a searchable database for a proof of concept of human scent as a biometric measure. Triplicate hand odor samples were evaluated from 10 subjects utilizing solid phase micro‐extraction gas chromatography/mass spectrometry (SPME‐GC/MS) and compared via Spearman Rank Correlations. Narrowing the compounds considered for each subject to only those common in all three samples, or a subject’s “primary odor constituents,” produced a greater degree of both individualization and discrimination; at both correlation thresholds of 0.9 and 0.8, the individuals were correctly discriminated and identified in 99.54% of the cases. |
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| AbstractList | : Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an individual’s “primary odor” compounds utilized to determine a reproducible and individualizing profile which can be stored in a searchable database for a proof of concept of human scent as a biometric measure. Triplicate hand odor samples were evaluated from 10 subjects utilizing solid phase micro‐extraction gas chromatography/mass spectrometry (SPME‐GC/MS) and compared via Spearman Rank Correlations. Narrowing the compounds considered for each subject to only those common in all three samples, or a subject’s “primary odor constituents,” produced a greater degree of both individualization and discrimination; at both correlation thresholds of 0.9 and 0.8, the individuals were correctly discriminated and identified in 99.54% of the cases. Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an individual's "primary odor" compounds utilized to determine a reproducible and individualizing profile which can be stored in a searchable database for a proof of concept of human scent as a biometric measure. Triplicate hand odor samples were evaluated from 10 subjects utilizing solid phase micro-extraction gas chromatography/mass spectrometry (SPME-GC/MS) and compared via Spearman Rank Correlations. Narrowing the compounds considered for each subject to only those common in all three samples, or a subject's "primary odor constituents," produced a greater degree of both individualization and discrimination; at both correlation thresholds of 0.9 and 0.8, the individuals were correctly discriminated and identified in 99.54% of the cases. [PUBLICATION ABSTRACT] Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an individual's "primary odor" compounds utilized to determine a reproducible and individualizing profile which can be stored in a searchable database for a proof of concept of human scent as a biometric measure. Triplicate hand odor samples were evaluated from 10 subjects utilizing solid phase micro-extraction gas chromatography/mass spectrometry (SPME-GC/MS) and compared via Spearman Rank Correlations. Narrowing the compounds considered for each subject to only those common in all three samples, or a subject's "primary odor constituents," produced a greater degree of both individualization and discrimination; at both correlation thresholds of 0.9 and 0.8, the individuals were correctly discriminated and identified in 99.54% of the cases. Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an individual's "primary odor" compounds utilized to determine a reproducible and individualizing profile which can be stored in a searchable database for a proof of concept of human scent as a biometric measure. Triplicate hand odor samples were evaluated from 10 subjects utilizing solid phase micro-extraction gas chromatography/mass spectrometry (SPME-GC/MS) and compared via Spearman Rank Correlations. Narrowing the compounds considered for each subject to only those common in all three samples, or a subject's "primary odor constituents," produced a greater degree of both individualization and discrimination; at both correlation thresholds of 0.9 and 0.8, the individuals were correctly discriminated and identified in 99.54% of the cases.Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing characteristic. This study describes the development of what is effectively a human scent barcode consisting of the relative ratios of an individual's "primary odor" compounds utilized to determine a reproducible and individualizing profile which can be stored in a searchable database for a proof of concept of human scent as a biometric measure. Triplicate hand odor samples were evaluated from 10 subjects utilizing solid phase micro-extraction gas chromatography/mass spectrometry (SPME-GC/MS) and compared via Spearman Rank Correlations. Narrowing the compounds considered for each subject to only those common in all three samples, or a subject's "primary odor constituents," produced a greater degree of both individualization and discrimination; at both correlation thresholds of 0.9 and 0.8, the individuals were correctly discriminated and identified in 99.54% of the cases. |
| Author | Prada, Paola A. Curran, Allison M. Furton, Kenneth G. |
| Author_xml | – sequence: 1 givenname: Allison M. surname: Curran fullname: Curran, Allison M. organization: Department of Chemistry and Biochemistry, International Forensic Research Institute, Florida International University, University Park, CP 345, Miami, FL 33199 – sequence: 2 givenname: Paola A. surname: Prada fullname: Prada, Paola A. organization: Department of Chemistry and Biochemistry, International Forensic Research Institute, Florida International University, University Park, CP 345, Miami, FL 33199 – sequence: 3 givenname: Kenneth G. surname: Furton fullname: Furton, Kenneth G. organization: Department of Chemistry and Biochemistry, International Forensic Research Institute, Florida International University, University Park, CP 345, Miami, FL 33199 |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/20002268$$D View this record in MEDLINE/PubMed |
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| Snippet | : Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing... Human scent evidence is utilized as an investigative tool through canine scent discriminations based on the premise that human scent is an individualizing... |
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| StartPage | 50 |
| SubjectTerms | Adolescent Adult Biometry - methods Chromatography Female Forensic chemistry Forensic Medicine - methods forensic science Gas Chromatography-Mass Spectrometry Hand human scent evidence Humans individualization Male Mass spectrometry Odorants Odors primary odor solid phase micro-extraction gas chromatography/mass spectrometry Solid Phase Microextraction Spearman Rank Correlations VOCs Volatile organic compounds |
| Title | The Differentiation of the Volatile Organic Signatures of Individuals Through SPME-GC/MS of Characteristic Human Scent Compounds |
| URI | https://api.istex.fr/ark:/67375/WNG-4XB0TGMW-0/fulltext.pdf https://onlinelibrary.wiley.com/doi/abs/10.1111%2Fj.1556-4029.2009.01236.x https://www.ncbi.nlm.nih.gov/pubmed/20002268 https://www.proquest.com/docview/219691433 https://www.proquest.com/docview/733909442 |
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