Efficient electrochemical production of glucaric acid and H2 via glucose electrolysis
Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeO x ) and nitride (NiFeN x ) catalysts, synthesized from NiFe layered double hydroxide nan...
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| Published in | Nature communications Vol. 11; no. 1; pp. 265 - 11 |
|---|---|
| Main Authors | , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
14.01.2020
Nature Publishing Group Nature Portfolio |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeO
x
) and nitride (NiFeN
x
) catalysts, synthesized from NiFe layered double hydroxide nanosheet arrays on three-dimensional Ni foams, demonstrate a high activity and selectivity towards anodic glucose oxidation. The electrolytic cell assembled with these two catalysts can deliver 100 mA cm
−2
at 1.39 V. A faradaic efficiency of 87% and glucaric acid yield of 83% are obtained from the glucose electrolysis, which takes place via a guluronic acid pathway evidenced by in-situ infrared spectroscopy. A rigorous process model combined with a techno-economic analysis shows that the electrochemical reduction of glucose produces glucaric acid at a 54% lower cost than the current chemical approach. This work suggests that glucose electrolysis is an energy-saving and cost-effective approach for H
2
production and biomass valorization.
Renewable biomass conversion may afford high-value products from common materials, but catalysts usually require expensive metals and exhibit poor selectivities. Here, authors employ nickel-iron oxide and nitride electrocatalysts to produce H
2
and to convert glucose to glucaric acid selectively. |
|---|---|
| AbstractList | Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeO
x
) and nitride (NiFeN
x
) catalysts, synthesized from NiFe layered double hydroxide nanosheet arrays on three-dimensional Ni foams, demonstrate a high activity and selectivity towards anodic glucose oxidation. The electrolytic cell assembled with these two catalysts can deliver 100 mA cm
−2
at 1.39 V. A faradaic efficiency of 87% and glucaric acid yield of 83% are obtained from the glucose electrolysis, which takes place via a guluronic acid pathway evidenced by in-situ infrared spectroscopy. A rigorous process model combined with a techno-economic analysis shows that the electrochemical reduction of glucose produces glucaric acid at a 54% lower cost than the current chemical approach. This work suggests that glucose electrolysis is an energy-saving and cost-effective approach for H
2
production and biomass valorization.
Renewable biomass conversion may afford high-value products from common materials, but catalysts usually require expensive metals and exhibit poor selectivities. Here, authors employ nickel-iron oxide and nitride electrocatalysts to produce H
2
and to convert glucose to glucaric acid selectively. Renewable biomass conversion may afford high-value products from common materials, but catalysts usually require expensive metals and exhibit poor selectivities. Here, authors employ nickel-iron oxide and nitride electrocatalysts to produce H2 and to convert glucose to glucaric acid selectively. Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeOx) and nitride (NiFeNx) catalysts, synthesized from NiFe layered double hydroxide nanosheet arrays on three-dimensional Ni foams, demonstrate a high activity and selectivity towards anodic glucose oxidation. The electrolytic cell assembled with these two catalysts can deliver 100 mA cm-2 at 1.39 V. A faradaic efficiency of 87% and glucaric acid yield of 83% are obtained from the glucose electrolysis, which takes place via a guluronic acid pathway evidenced by in-situ infrared spectroscopy. A rigorous process model combined with a techno-economic analysis shows that the electrochemical reduction of glucose produces glucaric acid at a 54% lower cost than the current chemical approach. This work suggests that glucose electrolysis is an energy-saving and cost-effective approach for H2 production and biomass valorization.Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeOx) and nitride (NiFeNx) catalysts, synthesized from NiFe layered double hydroxide nanosheet arrays on three-dimensional Ni foams, demonstrate a high activity and selectivity towards anodic glucose oxidation. The electrolytic cell assembled with these two catalysts can deliver 100 mA cm-2 at 1.39 V. A faradaic efficiency of 87% and glucaric acid yield of 83% are obtained from the glucose electrolysis, which takes place via a guluronic acid pathway evidenced by in-situ infrared spectroscopy. A rigorous process model combined with a techno-economic analysis shows that the electrochemical reduction of glucose produces glucaric acid at a 54% lower cost than the current chemical approach. This work suggests that glucose electrolysis is an energy-saving and cost-effective approach for H2 production and biomass valorization. Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeOx) and nitride (NiFeNx) catalysts, synthesized from NiFe layered double hydroxide nanosheet arrays on three-dimensional Ni foams, demonstrate a high activity and selectivity towards anodic glucose oxidation. The electrolytic cell assembled with these two catalysts can deliver 100 mA cm−2 at 1.39 V. A faradaic efficiency of 87% and glucaric acid yield of 83% are obtained from the glucose electrolysis, which takes place via a guluronic acid pathway evidenced by in-situ infrared spectroscopy. A rigorous process model combined with a techno-economic analysis shows that the electrochemical reduction of glucose produces glucaric acid at a 54% lower cost than the current chemical approach. This work suggests that glucose electrolysis is an energy-saving and cost-effective approach for H2 production and biomass valorization.Renewable biomass conversion may afford high-value products from common materials, but catalysts usually require expensive metals and exhibit poor selectivities. Here, authors employ nickel-iron oxide and nitride electrocatalysts to produce H2 and to convert glucose to glucaric acid selectively. Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules. Here we report that nanostructured NiFe oxide (NiFeO x ) and nitride (NiFeN x ) catalysts, synthesized from NiFe layered double hydroxide nanosheet arrays on three-dimensional Ni foams, demonstrate a high activity and selectivity towards anodic glucose oxidation. The electrolytic cell assembled with these two catalysts can deliver 100 mA cm −2 at 1.39 V. A faradaic efficiency of 87% and glucaric acid yield of 83% are obtained from the glucose electrolysis, which takes place via a guluronic acid pathway evidenced by in-situ infrared spectroscopy. A rigorous process model combined with a techno-economic analysis shows that the electrochemical reduction of glucose produces glucaric acid at a 54% lower cost than the current chemical approach. This work suggests that glucose electrolysis is an energy-saving and cost-effective approach for H 2 production and biomass valorization. |
| ArticleNumber | 265 |
| Author | Fan, Zhi-Yong Liu, Wu-Jun Xu, Zhuoran Li, Hong-Chao Huber, George W. Yu, Han-Qing Zhao, Dongting Jin, Song Pan, Xiao-Qiang Wang, Wei-Kang Hu, Xiao Zhao, Guo-Hua |
| Author_xml | – sequence: 1 givenname: Wu-Jun orcidid: 0000-0002-5696-1180 surname: Liu fullname: Liu, Wu-Jun organization: CAS Key Laboratory of Urban Pollutant Conversion, Department of Applied Chemistry, University of Science & Technology of China, Department of Chemical and Biological Engineering, University of Wisconsin-Madison – sequence: 2 givenname: Zhuoran surname: Xu fullname: Xu, Zhuoran organization: Department of Chemical and Biological Engineering, University of Wisconsin-Madison – sequence: 3 givenname: Dongting surname: Zhao fullname: Zhao, Dongting organization: Department of Chemical and Biological Engineering, University of Wisconsin-Madison – sequence: 4 givenname: Xiao-Qiang surname: Pan fullname: Pan, Xiao-Qiang organization: CAS Key Laboratory of Urban Pollutant Conversion, Department of Applied Chemistry, University of Science & Technology of China – sequence: 5 givenname: Hong-Chao orcidid: 0000-0002-8081-0980 surname: Li fullname: Li, Hong-Chao organization: CAS Key Laboratory of Urban Pollutant Conversion, Department of Applied Chemistry, University of Science & Technology of China – sequence: 6 givenname: Xiao surname: Hu fullname: Hu, Xiao organization: CAS Key Laboratory of Urban Pollutant Conversion, Department of Applied Chemistry, University of Science & Technology of China – sequence: 7 givenname: Zhi-Yong orcidid: 0000-0001-6138-179X surname: Fan fullname: Fan, Zhi-Yong organization: School of Chemical Science and Engineering, Tongji University – sequence: 8 givenname: Wei-Kang orcidid: 0000-0003-0090-3122 surname: Wang fullname: Wang, Wei-Kang organization: School of Chemical Science and Engineering, Tongji University – sequence: 9 givenname: Guo-Hua surname: Zhao fullname: Zhao, Guo-Hua organization: School of Chemical Science and Engineering, Tongji University – sequence: 10 givenname: Song orcidid: 0000-0001-8693-7010 surname: Jin fullname: Jin, Song organization: Department of Chemistry, University of Wisconsin-Madison – sequence: 11 givenname: George W. orcidid: 0000-0002-7838-6893 surname: Huber fullname: Huber, George W. email: gwhuber@wisc.edu organization: Department of Chemical and Biological Engineering, University of Wisconsin-Madison – sequence: 12 givenname: Han-Qing orcidid: 0000-0001-5247-6244 surname: Yu fullname: Yu, Han-Qing email: hqyu@ustc.edu.cn organization: CAS Key Laboratory of Urban Pollutant Conversion, Department of Applied Chemistry, University of Science & Technology of China |
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| Snippet | Glucose electrolysis offers a prospect of value-added glucaric acid synthesis and energy-saving hydrogen production from the biomass-based platform molecules.... Renewable biomass conversion may afford high-value products from common materials, but catalysts usually require expensive metals and exhibit poor... |
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| Title | Efficient electrochemical production of glucaric acid and H2 via glucose electrolysis |
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