Galvanic exchange platinization reveals laser-inscribed pattern in 3D-LAM-printed steel
Galvanic exchange involving dissolution of iron and the simultaneous growth of platinum onto 316 L stainless steel was investigated for specimens manufactured by 3D-printing, and the behavior was compared to conventional stainless steel. Novel phenomena associated with the 3D-printed steel, but not...
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| Published in | Journal of solid state electrochemistry Vol. 22; no. 6; pp. 1755 - 1762 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Berlin/Heidelberg
Springer Berlin Heidelberg
01.06.2018
Springer Nature B.V |
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| Abstract | Galvanic exchange involving dissolution of iron and the simultaneous growth of platinum onto 316 L stainless steel was investigated for specimens manufactured by 3D-printing, and the behavior was compared to conventional stainless steel. Novel phenomena associated with the 3D-printed steel, but not conventional steel, reacting in three distinct phases were observed: first, with low platinum loading, a bright etching pattern linked to the laser-manufacturing process is revealed at the steel surface; second, a nanostructured pore pattern with platinum nano-deposits forms; and third, a darker platinum film coating of typically 500-nm thickness forms and then peels off the steel surface with further platinum growth underneath. Unlike the conventional steel (and mainly due to residual porosity), 3D-printed steel supports well-adhered platinum films for potential application in electrocatalysis, as demonstrated for alkaline methanol oxidation.
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| AbstractList | Galvanic exchange involving dissolution of iron and the simultaneous growth of platinum onto 316 L stainless steel was investigated for specimens manufactured by 3D-printing, and the behavior was compared to conventional stainless steel. Novel phenomena associated with the 3D-printed steel, but not conventional steel, reacting in three distinct phases were observed: first, with low platinum loading, a bright etching pattern linked to the laser-manufacturing process is revealed at the steel surface; second, a nanostructured pore pattern with platinum nano-deposits forms; and third, a darker platinum film coating of typically 500-nm thickness forms and then peels off the steel surface with further platinum growth underneath. Unlike the conventional steel (and mainly due to residual porosity), 3D-printed steel supports well-adhered platinum films for potential application in electrocatalysis, as demonstrated for alkaline methanol oxidation. Galvanic exchange involving dissolution of iron and the simultaneous growth of platinum onto 316 L stainless steel was investigated for specimens manufactured by 3D-printing, and the behavior was compared to conventional stainless steel. Novel phenomena associated with the 3D-printed steel, but not conventional steel, reacting in three distinct phases were observed: first, with low platinum loading, a bright etching pattern linked to the laser-manufacturing process is revealed at the steel surface; second, a nanostructured pore pattern with platinum nano-deposits forms; and third, a darker platinum film coating of typically 500-nm thickness forms and then peels off the steel surface with further platinum growth underneath. Unlike the conventional steel (and mainly due to residual porosity), 3D-printed steel supports well-adhered platinum films for potential application in electrocatalysis, as demonstrated for alkaline methanol oxidation. Graphical abstract ᅟ |
| Author | Litherland, Alex G. M. Spurway, Lee M. Matilainen, Ville-Pekka Marken, Frank Vuorema, Anne Gordeev, Sergey N. Hovilehto, Mikko Wain, Andrew J. O’Connell, Michael A. Piili, Heidi Aaronson, Barak D. B. |
| Author_xml | – sequence: 1 givenname: Alex G. M. surname: Litherland fullname: Litherland, Alex G. M. organization: Department of Physics, University of Bath – sequence: 2 givenname: Lee M. surname: Spurway fullname: Spurway, Lee M. organization: Department of Physics, University of Bath – sequence: 3 givenname: Sergey N. surname: Gordeev fullname: Gordeev, Sergey N. organization: Department of Physics, University of Bath – sequence: 4 givenname: Barak D. B. surname: Aaronson fullname: Aaronson, Barak D. B. organization: Department of Chemistry, University of Bath – sequence: 5 givenname: Andrew J. surname: Wain fullname: Wain, Andrew J. organization: National Physical Laboratory – sequence: 6 givenname: Michael A. surname: O’Connell fullname: O’Connell, Michael A. organization: National Physical Laboratory – sequence: 7 givenname: Heidi surname: Piili fullname: Piili, Heidi organization: Laser Processing Research Group, Lappeenranta University of Technology – sequence: 8 givenname: Mikko surname: Hovilehto fullname: Hovilehto, Mikko organization: Laser Processing Research Group, Lappeenranta University of Technology – sequence: 9 givenname: Ville-Pekka surname: Matilainen fullname: Matilainen, Ville-Pekka organization: Laser Processing Research Group, Lappeenranta University of Technology – sequence: 10 givenname: Anne surname: Vuorema fullname: Vuorema, Anne organization: LUT RE-SOURCE Research Platform, Lappeenranta University of Technology – sequence: 11 givenname: Frank orcidid: 0000-0003-3177-4562 surname: Marken fullname: Marken, Frank email: f.marken@bath.ac.uk organization: Department of Chemistry, University of Bath |
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| SubjectTerms | Analytical Chemistry Austenitic stainless steels Bright plating Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Condensed Matter Physics Electrochemistry Energy Storage Original Paper Oxidation Physical Chemistry Platinum Porosity Stainless steel Steel industry Steel structures Three dimensional printing |
| Title | Galvanic exchange platinization reveals laser-inscribed pattern in 3D-LAM-printed steel |
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