Kinetics and product distribution of end of life tyres (ELTs) pyrolysis: A novel approach in polyisoprene and SBR thermal cracking
Thermo-chemical treatments (mainly pyrolysis) directed towards energy and products recovery provide a very promising alternative to open space disposal or landfilling, reducing in the process hazardous waste and potential contamination to soil and water resources. In this communication, we present r...
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Published in | Journal of hazardous materials Vol. 172; no. 2; pp. 1690 - 1694 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
Kidlington
Elsevier B.V
30.12.2009
Elsevier |
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Abstract | Thermo-chemical treatments (mainly pyrolysis) directed towards energy and products recovery provide a very promising alternative to open space disposal or landfilling, reducing in the process hazardous waste and potential contamination to soil and water resources. In this communication, we present results of end of life tyres (ELTs) pyrolysis via isothermal and dynamic thermogravimetry of two ELT grades. The aim of this study is to demonstrate the possibility of utilizing a pre-set temperature (
T
c
=
500
°C) pyrolysis process (conversion time,
t
c, of 120
s), to the benefit of intensifying the global product yields recovered. A novel engineering kinetics approach was undertaken to propose a thermal cracking scheme of four primary and two secondary side reactions. Thermal degradation of ELTs was taken from a depolymerization approach of the present polyisoprene polymer in the tyres, resulting in a high regression of 0.959. The products of ELTs pyrolysis were lumped into four categories, namely aromatics, liquids, char and gases. The thermal cracking model evaluation of kinetic rate constants and lumped products showed a regression ranging between 0.90 and 0.94. Dynamic runs were performed to extend the model derived, taking into account heating rate (
β) influence and products prediction and interaction. The results obtained can be used in designing industrial ELTs pyrolysis units. |
---|---|
AbstractList | Thermo-chemical treatments (mainly pyrolysis) directed towards energy and products recovery provide a very promising alternative to open space disposal or landfilling, reducing in the process hazardous waste and potential contamination to soil and water resources. In this communication, we present results of end of life tyres (ELTs) pyrolysis via isothermal and dynamic thermogravimetry of two ELT grades. The aim of this study is to demonstrate the possibility of utilizing a pre-set temperature (T(c)=500 degrees C) pyrolysis process (conversion time, t(c), of 120 s), to the benefit of intensifying the global product yields recovered. A novel engineering kinetics approach was undertaken to propose a thermal cracking scheme of four primary and two secondary side reactions. Thermal degradation of ELTs was taken from a depolymerization approach of the present polyisoprene polymer in the tyres, resulting in a high regression of 0.959. The products of ELTs pyrolysis were lumped into four categories, namely aromatics, liquids, char and gases. The thermal cracking model evaluation of kinetic rate constants and lumped products showed a regression ranging between 0.90 and 0.94. Dynamic runs were performed to extend the model derived, taking into account heating rate (beta) influence and products prediction and interaction. The results obtained can be used in designing industrial ELTs pyrolysis units. Thermo-chemical treatments (mainly pyrolysis) directed towards energy and products recovery provide a very promising alternative to open space disposal or landfilling, reducing in the process hazardous waste and potential contamination to soil and water resources. In this communication, we present results of end of life tyres (ELTs) pyrolysis via isothermal and dynamic thermogravimetry of two ELT grades. The aim of this study is to demonstrate the possibility of utilizing a pre-set temperature (T sub(c)=500 super(o)C) pyrolysis process (conversion time, t sub(c), of 120s), to the benefit of intensifying the global product yields recovered. A novel engineering kinetics approach was undertaken to propose a thermal cracking scheme of four primary and two secondary side reactions. Thermal degradation of ELTs was taken from a depolymerization approach of the present polyisoprene polymer in the tyres, resulting in a high regression of 0.959. The products of ELTs pyrolysis were lumped into four categories, namely aromatics, liquids, char and gases. The thermal cracking model evaluation of kinetic rate constants and lumped products showed a regression ranging between 0.90 and 0.94. Dynamic runs were performed to extend the model derived, taking into account heating rate (b) influence and products prediction and interaction. The results obtained can be used in designing industrial ELTs pyrolysis units. Thermo-chemical treatments (mainly pyrolysis) directed towards energy and products recovery provide a very promising alternative to open space disposal or landfilling, reducing in the process hazardous waste and potential contamination to soil and water resources. In this communication, we present results of end of life tyres (ELTs) pyrolysis via isothermal and dynamic thermogravimetry of two ELT grades. The aim of this study is to demonstrate the possibility of utilizing a pre-set temperature (T(c)=500(o)C) pyrolysis process (conversion time, t(c), of 120s), to the benefit of intensifying the global product yields recovered. A novel engineering kinetics approach was undertaken to propose a thermal cracking scheme of four primary and two secondary side reactions. Thermal degradation of ELTs was taken from a depolymerization approach of the present polyisoprene polymer in the tyres, resulting in a high regression of 0.959. The products of ELTs pyrolysis were lumped into four categories, namely aromatics, liquids, char and gases. The thermal cracking model evaluation of kinetic rate constants and lumped products showed a regression ranging between 0.90 and 0.94. Dynamic runs were performed to extend the model derived, taking into account heating rate (b) influence and products prediction and interaction. The results obtained can be used in designing industrial ELTs pyrolysis units. Thermo-chemical treatments (mainly pyrolysis) directed towards energy and products recovery provide a very promising alternative to open space disposal or landfilling, reducing in the process hazardous waste and potential contamination to soil and water resources. In this communication, we present results of end of life tyres (ELTs) pyrolysis via isothermal and dynamic thermogravimetry of two ELT grades. The aim of this study is to demonstrate the possibility of utilizing a pre-set temperature ( T c = 500 °C) pyrolysis process (conversion time, t c, of 120 s), to the benefit of intensifying the global product yields recovered. A novel engineering kinetics approach was undertaken to propose a thermal cracking scheme of four primary and two secondary side reactions. Thermal degradation of ELTs was taken from a depolymerization approach of the present polyisoprene polymer in the tyres, resulting in a high regression of 0.959. The products of ELTs pyrolysis were lumped into four categories, namely aromatics, liquids, char and gases. The thermal cracking model evaluation of kinetic rate constants and lumped products showed a regression ranging between 0.90 and 0.94. Dynamic runs were performed to extend the model derived, taking into account heating rate ( β) influence and products prediction and interaction. The results obtained can be used in designing industrial ELTs pyrolysis units. |
Author | Baeyens, J. Lettieri, P. Al-Salem, S.M. |
Author_xml | – sequence: 1 givenname: S.M. surname: Al-Salem fullname: Al-Salem, S.M. email: s.al-salem@ucl.ac.uk organization: Centre for CO 2 Technology, Department of Chemical Engineering, University College London (UCL), Torrington Place, London WC1E 7JE, UK – sequence: 2 givenname: P. surname: Lettieri fullname: Lettieri, P. organization: Centre for CO 2 Technology, Department of Chemical Engineering, University College London (UCL), Torrington Place, London WC1E 7JE, UK – sequence: 3 givenname: J. surname: Baeyens fullname: Baeyens, J. organization: School of Engineering, University of Warwick, Coventry CV4 7AL, UK |
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Cites_doi | 10.1016/S0014-3057(01)00255-5 10.1016/0166-3097(87)90003-4 10.1016/S0141-3910(98)00036-6 10.1021/ef9801524 10.1016/S0165-2370(99)00017-0 10.1021/ef990155w 10.1016/0016-2361(90)90193-T 10.1016/j.jaap.2008.05.004 10.1016/j.scitotenv.2009.05.044 10.1016/S0016-2361(99)00087-3 10.1016/S0956-053X(02)00083-1 10.1016/S0165-2370(97)00085-5 10.1002/app.2104 10.1252/jcej.36.1016 10.1016/j.jaap.2004.10.007 10.1016/0361-3658(83)90033-4 10.1016/S0032-5910(97)03268-3 |
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Keywords | Pyrolysis Hazardous waste Kinetics ELTs Thermogravimetry Thermochemical treatment Thermal cracking Heating rate Prediction Modeling Contamination Tyre Pollution Aromatic compound Rate constant Water resources Thermal degradation |
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SubjectTerms | Applied sciences Conservation of Natural Resources - methods ELTs Exact sciences and technology Hazardous waste Hemiterpenes - analysis Hot Temperature Incineration Kinetics Latex - analysis Pollution Pyrolysis Thermogravimetry Waste Management |
Title | Kinetics and product distribution of end of life tyres (ELTs) pyrolysis: A novel approach in polyisoprene and SBR thermal cracking |
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