SPPEK/TPA composite membrane as a separator of vanadium redox flow battery
To improve the performance of a low cost sulfonated poly(phthalazinone ether ketone) (SPPEK) membrane in vanadium redox flow battery (VRFB), composite membranes composed of SPPEK and tungstophosphoric acid (TPA) with 8–25wt% concentration were prepared by solution casting. The results of scanning el...
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| Published in | Journal of membrane science Vol. 437; pp. 114 - 121 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
15.06.2013
Elsevier |
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| Online Access | Get full text |
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| Abstract | To improve the performance of a low cost sulfonated poly(phthalazinone ether ketone) (SPPEK) membrane in vanadium redox flow battery (VRFB), composite membranes composed of SPPEK and tungstophosphoric acid (TPA) with 8–25wt% concentration were prepared by solution casting. The results of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD) of the SPPEK/TPA composite membrane revealed that TPA had excellent compatibility with SPPEK in the bulk of the membrane. The effect of the TPA concentration on the primary properties, permeability of vanadium ions and ionic selectivity, and chemical stability of the composite membrane was investigated. The single cell tests showed that the VRFB employing the SPPEK–TPA-17 membrane with 17wt% TPA exhibited a higher coulombic efficiency (98.75% vs. 92.81%) and energy efficiency (74.58% vs. 73.83%) than those of the Nafion system. Cycling and chemical stability tests indicated that the SPPEK/TPA composite membrane had high stability in the VRFB system.
► A SPPEK/TPA composite membrane by the solution casting method was investigated in VRFB application. ► The introduction of TPA (8–25wt%) can improve the proton conductivity. ► VRFB with the composite membrane exhibited superior performance compared with Nafion membrane. |
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| AbstractList | To improve the performance of a low cost sulfonated poly(phthalazinone ether ketone) (SPPEK) membrane in vanadium redox flow battery (VRFB), composite membranes composed of SPPEK and tungstophosphoric acid (TPA) with 8–25wt% concentration were prepared by solution casting. The results of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD) of the SPPEK/TPA composite membrane revealed that TPA had excellent compatibility with SPPEK in the bulk of the membrane. The effect of the TPA concentration on the primary properties, permeability of vanadium ions and ionic selectivity, and chemical stability of the composite membrane was investigated. The single cell tests showed that the VRFB employing the SPPEK–TPA-17 membrane with 17wt% TPA exhibited a higher coulombic efficiency (98.75% vs. 92.81%) and energy efficiency (74.58% vs. 73.83%) than those of the Nafion system. Cycling and chemical stability tests indicated that the SPPEK/TPA composite membrane had high stability in the VRFB system. To improve the performance of a low cost sulfonated poly(phthalazinone ether ketone) (SPPEK) membrane in vanadium redox flow battery (VRFB), composite membranes composed of SPPEK and tungstophosphoric acid (TPA) with 8–25wt% concentration were prepared by solution casting. The results of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD) of the SPPEK/TPA composite membrane revealed that TPA had excellent compatibility with SPPEK in the bulk of the membrane. The effect of the TPA concentration on the primary properties, permeability of vanadium ions and ionic selectivity, and chemical stability of the composite membrane was investigated. The single cell tests showed that the VRFB employing the SPPEK–TPA-17 membrane with 17wt% TPA exhibited a higher coulombic efficiency (98.75% vs. 92.81%) and energy efficiency (74.58% vs. 73.83%) than those of the Nafion system. Cycling and chemical stability tests indicated that the SPPEK/TPA composite membrane had high stability in the VRFB system. ► A SPPEK/TPA composite membrane by the solution casting method was investigated in VRFB application. ► The introduction of TPA (8–25wt%) can improve the proton conductivity. ► VRFB with the composite membrane exhibited superior performance compared with Nafion membrane. To improve the performance of a low cost sulfonated poly(phthalazinone ether ketone) (SPPEK) membrane in vanadium redox flow battery (VRFB), composite membranes composed of SPPEK and tungstophosphoric acid (TPA) with 8a25 wt% concentration were prepared by solution casting. The results of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and X-ray diffraction (XRD) of the SPPEK/TPA composite membrane revealed that TPA had excellent compatibility with SPPEK in the bulk of the membrane. The effect of the TPA concentration on the primary properties, permeability of vanadium ions and ionic selectivity, and chemical stability of the composite membrane was investigated. The single cell tests showed that the VRFB employing the SPPEKaTPA-17 membrane with 17 wt% TPA exhibited a higher coulombic efficiency (98.75% vs. 92.81%) and energy efficiency (74.58% vs. 73.83%) than those of the Nafion system. Cycling and chemical stability tests indicated that the SPPEK/TPA composite membrane had high stability in the VRFB system. |
| Author | Yu, Jingang Wang, Nanfang Fang, Dong Zhou, Zhi Liu, Suqin Liu, Younian |
| Author_xml | – sequence: 1 givenname: Nanfang surname: Wang fullname: Wang, Nanfang email: cdwnf@126.com organization: School of Chemistry and Chemical Engineering, Hunan Institute of Engineering, 88 Fuxing East Road, Xiangtan 411104, China – sequence: 2 givenname: Jingang surname: Yu fullname: Yu, Jingang organization: Key Laboratory of Resources Chemistry of Nonferrous Metals, Ministry of Education, College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China – sequence: 3 givenname: Zhi surname: Zhou fullname: Zhou, Zhi organization: Key Laboratory of Resources Chemistry of Nonferrous Metals, Ministry of Education, College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China – sequence: 4 givenname: Dong surname: Fang fullname: Fang, Dong organization: Key Laboratory of Green Processing and Functional Textiles of New Textile Materials, Ministry of Education, College of Materials Science and Engineering, Wuhan Textile University, 430073 Wuhan, China – sequence: 5 givenname: Suqin surname: Liu fullname: Liu, Suqin email: sqliu2003@126.com organization: Key Laboratory of Resources Chemistry of Nonferrous Metals, Ministry of Education, College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China – sequence: 6 givenname: Younian surname: Liu fullname: Liu, Younian organization: Key Laboratory of Resources Chemistry of Nonferrous Metals, Ministry of Education, College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China |
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| Keywords | Vanadium permeability Ionic selectivity Vanadium redox flow battery Low cost SPPEK/TPA composite membrane Membrane separation Heteropolyacid Polymeric membrane Battery Vanadium Transition metal Permeability |
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| Snippet | To improve the performance of a low cost sulfonated poly(phthalazinone ether ketone) (SPPEK) membrane in vanadium redox flow battery (VRFB), composite... |
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| SubjectTerms | Applied sciences artificial membranes batteries Battery Chemistry Colloidal state and disperse state Corrosion resistance Diffraction Direct energy conversion and energy accumulation Electrical engineering. Electrical power engineering Electrical power engineering Electrochemical conversion: primary and secondary batteries, fuel cells energy efficiency Energy management energy-dispersive X-ray analysis Ethers Exact sciences and technology Exchange resins and membranes Forms of application and semi-finished materials General and physical chemistry Ionic selectivity ions Low cost Membranes permeability phosphotungstic acid Polymer industry, paints, wood Scanning electron microscopy spectroscopy SPPEK/TPA composite membrane Technology of polymers Vanadium Vanadium permeability Vanadium redox flow battery X-radiation X-ray diffraction |
| Title | SPPEK/TPA composite membrane as a separator of vanadium redox flow battery |
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