Characteristics of the Water- and Alkali-Soluble Hemicelluloses Fractionated by Sequential Acidification and Graded-Ethanol from Sweet Maize Stems

Sweet maize stems were treated with hot water and potassium hydroxide to fractionate hemicellulosic polymers. The results showed that the water-soluble hemicelluloses were mainly composed of glucose (27.83%), xylose (27.32%), and galactose (16.81%). In comparison, alkali-soluble hemicelluloses fract...

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Published inMolecules (Basel, Switzerland) Vol. 24; no. 1; p. 212
Main Authors Peng, Xiaopeng, Nie, Shuangxi, Li, Xiaoping, Huang, Xiong, Li, Quanzi
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 08.01.2019
MDPI
Subjects
Acidification
Acids
Cellulose
Chromatography
Ethanol
Fractionation
Glucose
graded ethanol precipitation
hemicelluloses
Laboratories
Lignin
Lignocellulose
Solvents
structural features
sweet maize stems
United States > US
structural features
sweet maize stems
fractionation
hemicelluloses
graded ethanol precipitation
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Abstract Sweet maize stems were treated with hot water and potassium hydroxide to fractionate hemicellulosic polymers. The results showed that the water-soluble hemicelluloses were mainly composed of glucose (27.83%), xylose (27.32%), and galactose (16.81%). In comparison, alkali-soluble hemicelluloses fractionated by acidification and a graded ethanol solution (10%, 20%, 35%, 50%, 65%, and 80%) were mainly composed of xylose (69.73 to 88.62%) and arabinose (5.41 to 16.20%). More highly branched hemicelluloses tended to be precipitated in a higher concentration of ethanol solution, as revealed by the decreasing xylose to arabinose ratio from 16.43 to 4.21. Structural characterizations indicated that alkali-soluble hemicelluloses fractionated from sweet maize stems were mainly arabinoxylans. The results provided fundamental information on hemicelluloses composition and structure and their potential utilization in the fields of biofuels, biochemicals, and biomaterials.
AbstractList Sweet maize stems were treated with hot water and potassium hydroxide to fractionate hemicellulosic polymers. The results showed that the water-soluble hemicelluloses were mainly composed of glucose (27.83%), xylose (27.32%), and galactose (16.81%). In comparison, alkali-soluble hemicelluloses fractionated by acidification and a graded ethanol solution (10%, 20%, 35%, 50%, 65%, and 80%) were mainly composed of xylose (69.73 to 88.62%) and arabinose (5.41 to 16.20%). More highly branched hemicelluloses tended to be precipitated in a higher concentration of ethanol solution, as revealed by the decreasing xylose to arabinose ratio from 16.43 to 4.21. Structural characterizations indicated that alkali-soluble hemicelluloses fractionated from sweet maize stems were mainly arabinoxylans. The results provided fundamental information on hemicelluloses composition and structure and their potential utilization in the fields of biofuels, biochemicals, and biomaterials.Sweet maize stems were treated with hot water and potassium hydroxide to fractionate hemicellulosic polymers. The results showed that the water-soluble hemicelluloses were mainly composed of glucose (27.83%), xylose (27.32%), and galactose (16.81%). In comparison, alkali-soluble hemicelluloses fractionated by acidification and a graded ethanol solution (10%, 20%, 35%, 50%, 65%, and 80%) were mainly composed of xylose (69.73 to 88.62%) and arabinose (5.41 to 16.20%). More highly branched hemicelluloses tended to be precipitated in a higher concentration of ethanol solution, as revealed by the decreasing xylose to arabinose ratio from 16.43 to 4.21. Structural characterizations indicated that alkali-soluble hemicelluloses fractionated from sweet maize stems were mainly arabinoxylans. The results provided fundamental information on hemicelluloses composition and structure and their potential utilization in the fields of biofuels, biochemicals, and biomaterials.
Sweet maize stems were treated with hot water and potassium hydroxide to fractionate hemicellulosic polymers. The results showed that the water-soluble hemicelluloses were mainly composed of glucose (27.83%), xylose (27.32%), and galactose (16.81%). In comparison, alkali-soluble hemicelluloses fractionated by acidification and a graded ethanol solution (10%, 20%, 35%, 50%, 65%, and 80%) were mainly composed of xylose (69.73 to 88.62%) and arabinose (5.41 to 16.20%). More highly branched hemicelluloses tended to be precipitated in a higher concentration of ethanol solution, as revealed by the decreasing xylose to arabinose ratio from 16.43 to 4.21. Structural characterizations indicated that alkali-soluble hemicelluloses fractionated from sweet maize stems were mainly arabinoxylans. The results provided fundamental information on hemicelluloses composition and structure and their potential utilization in the fields of biofuels, biochemicals, and biomaterials.
Author Li, Quanzi
Huang, Xiong
Nie, Shuangxi
Peng, Xiaopeng
Li, Xiaoping
AuthorAffiliation 1 State Key Laboratory of Tree Genetics and Breeding, Chinese Academy of Forestry, Beijing 100091, China; huangxiong0839@163.com
3 Research Institute of Forestry, Chinese Academy of Forestry, Beijing 100091, China
4 Jiangsu Key Laboratory for Poplar Germplasm Innovation and Variety Improvement, Nanjing Forestry University, Nanjing 210037, China; xpli@njfu.edu.cn
2 Guangxi Key Laboratory of Clean Pulp & Papermaking and Pollution Control, Nanning 530004, China; cppkl@gxu.edu.cn
AuthorAffiliation_xml – name: 3 Research Institute of Forestry, Chinese Academy of Forestry, Beijing 100091, China
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– name: 2 Guangxi Key Laboratory of Clean Pulp & Papermaking and Pollution Control, Nanning 530004, China; cppkl@gxu.edu.cn
– name: 4 Jiangsu Key Laboratory for Poplar Germplasm Innovation and Variety Improvement, Nanjing Forestry University, Nanjing 210037, China; xpli@njfu.edu.cn
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/30626118$$D View this record in MEDLINE/PubMed
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Keywords structural features
sweet maize stems
fractionation
hemicelluloses
graded ethanol precipitation
Language English
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Snippet Sweet maize stems were treated with hot water and potassium hydroxide to fractionate hemicellulosic polymers. The results showed that the water-soluble...
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StartPage 212
SubjectTerms Acidification
Acids
Cellulose
Chromatography
Ethanol
Fractionation
Glucose
graded ethanol precipitation
hemicelluloses
Laboratories
Lignin
Lignocellulose
Solvents
structural features
sweet maize stems
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Title Characteristics of the Water- and Alkali-Soluble Hemicelluloses Fractionated by Sequential Acidification and Graded-Ethanol from Sweet Maize Stems
URI https://www.ncbi.nlm.nih.gov/pubmed/30626118
https://www.proquest.com/docview/2549017648
https://www.proquest.com/docview/2179321997
https://pubmed.ncbi.nlm.nih.gov/PMC6337417
https://doaj.org/article/e5c991667e8742748dbd63338d5a6084
Volume 24
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