Preparation and characterization of a quaternary ammonium derivative of konjac glucomannan
Cationic derivatives of konjac glucomannan (KGM) were prepared by reacting KGM with 3-chloro-2-hydroxypropyltrimethylammonium chloride (CHPTAC) in presence of sodium hydroxide. The chemical structures of derivative were characterized by use of elemental analysis, FTIR and 13C NMR spectroscopy and st...
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| Published in | Carbohydrate polymers Vol. 69; no. 1; pp. 29 - 40 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
01.05.2007
Elsevier Science |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Cationic derivatives of konjac glucomannan (KGM) were prepared by reacting KGM with 3-chloro-2-hydroxypropyltrimethylammonium chloride (CHPTAC) in presence of sodium hydroxide. The chemical structures of derivative were characterized by use of elemental analysis, FTIR and
13C NMR spectroscopy and static light scattering technique. The results revealed that the degree of substitution (DS) of quaternized konjac glucomannan (QKGM) could be controlled by adjusting the weight ratio of CHPTAC to KGM and the degradation of KGM molecules occurred during quaternization. Thermogravimetric analysis showed that the thermal stability of QKGM was lower than that of KGM. Rheological properties of KGM and QKGM were evaluated in steady and dynamic shear. The flow data were fitted fairly well by the Cross equations and various parameters were calculated. Dynamic shear tests demonstrate that highly modified KGM behaved like dilute solution, while unmodified KGM displayed entanglement network behavior. Significant shear-thinning effects and deviations from the Cox–Merz rule are observed in present study.
In vitro antimicrobial activity assessment exhibited QKGM showed pronounced inhibitory effect against the three bacteria and four fungi investigated, but no
Pseudomonas aeruginosa and
Aspergillus niger inhibition. The improved functionalities of the derivative might be explained by its polycationic characteristics. |
|---|---|
| AbstractList | Cationic derivatives of konjac glucomannan (KGM) were prepared by reacting KGM with 3-chloro-2-hydroxypropyltrimethylammonium chloride (CHPTAC) in presence of sodium hydroxide. The chemical structures of derivative were characterized by use of elemental analysis, FTIR and 13C NMR spectroscopy and static light scattering technique. The results revealed that the degree of substitution (DS) of quaternized konjac glucomannan (QKGM) could be controlled by adjusting the weight ratio of CHPTAC to KGM and the degradation of KGM molecules occurred during quaternization. Thermogravimetric analysis showed that the thermal stability of QKGM was lower than that of KGM. Rheological properties of KGM and QKGM were evaluated in steady and dynamic shear. The flow data were fitted fairly well by the Cross equations and various parameters were calculated. Dynamic shear tests demonstrate that highly modified KGM behaved like dilute solution, while unmodified KGM displayed entanglement network behavior. Significant shear-thinning effects and deviations from the Cox–Merz rule are observed in present study. In vitro antimicrobial activity assessment exhibited QKGM showed pronounced inhibitory effect against the three bacteria and four fungi investigated, but no Pseudomonas aeruginosa and Aspergillus niger inhibition. The improved functionalities of the derivative might be explained by its polycationic characteristics. Cationic derivatives of konjac glucomannan (KGM) were prepared by reacting KGM with 3-chloro-2-hydroxypropyltrimethylammonium chloride (CHPTAC) in presence of sodium hydroxide. The chemical structures of derivative were characterized by use of elemental analysis, FTIR and 13C NMR spectroscopy and static light scattering technique. The results revealed that the degree of substitution (DS) of quaternized konjac glucomannan (QKGM) could be controlled by adjusting the weight ratio of CHPTAC to KGM and the degradation of KGM molecules occurred during quaternization. Thermogravimetric analysis showed that the thermal stability of QKGM was lower than that of KGM. Rheological properties of KGM and QKGM were evaluated in steady and dynamic shear. The flow data were fitted fairly well by the Cross equations and various parameters were calculated. Dynamic shear tests demonstrate that highly modified KGM behaved like dilute solution, while unmodified KGM displayed entanglement network behavior. Significant shear-thinning effects and deviations from the Cox–Merz rule are observed in present study. In vitro antimicrobial activity assessment exhibited QKGM showed pronounced inhibitory effect against the three bacteria and four fungi investigated, but no Pseudomonas aeruginosa and Aspergillus niger inhibition. The improved functionalities of the derivative might be explained by its polycationic characteristics. |
| Author | Ying, Hou Huang, Yihong Xiao, Chaobo Yu, Huiqun |
| Author_xml | – sequence: 1 givenname: Huiqun surname: Yu fullname: Yu, Huiqun organization: College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, People’s Republic of China – sequence: 2 givenname: Yihong surname: Huang fullname: Huang, Yihong organization: College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, People’s Republic of China – sequence: 3 givenname: Hou surname: Ying fullname: Ying, Hou organization: College of Life Sciences, Henan Normal University, Xinxiang 453002, People’s Republic of China – sequence: 4 givenname: Chaobo surname: Xiao fullname: Xiao, Chaobo email: CBXiao@whu.edu.cn organization: College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, People’s Republic of China |
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| Keywords | Rheological property Konjac glucomannan Antimicrobial activity Quaternization Biological properties Viscoelasticity Fungicidal effect Shear flow Konjac Experimental study Antimicrobial agent Shear thinning Thermal stability Bactericidal effect Chemical coupling Quaternary ammonium compound Polyelectrolyte Chemical modification Preparation Aqueous solution Flow curve Quaternary ammonium polymer Glucomannan |
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| Snippet | Cationic derivatives of konjac glucomannan (KGM) were prepared by reacting KGM with 3-chloro-2-hydroxypropyltrimethylammonium chloride (CHPTAC) in presence of... |
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| SubjectTerms | anti-infective properties Antimicrobial activity Applied sciences Aspergillus niger bacteria chemical structure equations Exact sciences and technology Fourier transform infrared spectroscopy fungi Konjac glucomannan konjac mannan light scattering Natural polymers nuclear magnetic resonance spectroscopy Physicochemistry of polymers Pseudomonas aeruginosa Quaternization rheological properties Rheological property sodium hydroxide Starch and polysaccharides thermal stability thermogravimetry |
| Title | Preparation and characterization of a quaternary ammonium derivative of konjac glucomannan |
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