A thermodynamic investigation of the Li–Sb system
Many standard thermodynamic data in the binary system Li–Sb can be found in literature; however, they are often derived from electrochemical measurements taken at higher temperatures. The uncertainties associated with the extrapolation of these high-temperature data to room temperature are, however,...
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Published in | Journal of thermal analysis and calorimetry Vol. 131; no. 3; pp. 2673 - 2686 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
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Dordrecht
Springer Netherlands
01.03.2018
Springer Springer Nature B.V |
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Abstract | Many standard thermodynamic data in the binary system Li–Sb can be found in literature; however, they are often derived from electrochemical measurements taken at higher temperatures. The uncertainties associated with the extrapolation of these high-temperature data to room temperature are, however, inherently large. Therefore, a comprehensive investigation of the thermodynamic properties in the Li–Sb system was conducted in this work to generate more reliable data. Four different experimental techniques were used for the investigations. The heat capacities for both binary compounds, Li
2
Sb and Li
3
Sb, were measured for the very first time. In addition, the enthalpies of formation for both compounds were determined by drop solution and direct reaction calorimetry. Furthermore, Knudsen effusion mass spectrometry was performed to measure partial enthalpies and activities of Sb. |
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AbstractList | Many standard thermodynamic data in the binary system Li–Sb can be found in literature; however, they are often derived from electrochemical measurements taken at higher temperatures. The uncertainties associated with the extrapolation of these high-temperature data to room temperature are, however, inherently large. Therefore, a comprehensive investigation of the thermodynamic properties in the Li–Sb system was conducted in this work to generate more reliable data. Four different experimental techniques were used for the investigations. The heat capacities for both binary compounds, Li
2
Sb and Li
3
Sb, were measured for the very first time. In addition, the enthalpies of formation for both compounds were determined by drop solution and direct reaction calorimetry. Furthermore, Knudsen effusion mass spectrometry was performed to measure partial enthalpies and activities of Sb. Many standard thermodynamic data in the binary system Li-Sb can be found in literature; however, they are often derived from electrochemical measurements taken at higher temperatures. The uncertainties associated with the extrapolation of these high-temperature data to room temperature are, however, inherently large. Therefore, a comprehensive investigation of the thermodynamic properties in the Li-Sb system was conducted in this work to generate more reliable data. Four different experimental techniques were used for the investigations. The heat capacities for both binary compounds, Li.sub.2Sb and Li.sub.3Sb, were measured for the very first time. In addition, the enthalpies of formation for both compounds were determined by drop solution and direct reaction calorimetry. Furthermore, Knudsen effusion mass spectrometry was performed to measure partial enthalpies and activities of Sb. Many standard thermodynamic data in the binary system Li–Sb can be found in literature; however, they are often derived from electrochemical measurements taken at higher temperatures. The uncertainties associated with the extrapolation of these high-temperature data to room temperature are, however, inherently large. Therefore, a comprehensive investigation of the thermodynamic properties in the Li–Sb system was conducted in this work to generate more reliable data. Four different experimental techniques were used for the investigations. The heat capacities for both binary compounds, Li2Sb and Li3Sb, were measured for the very first time. In addition, the enthalpies of formation for both compounds were determined by drop solution and direct reaction calorimetry. Furthermore, Knudsen effusion mass spectrometry was performed to measure partial enthalpies and activities of Sb. |
Audience | Academic |
Author | Cupid, D. Henriques, D. Flandorfer, H. Motalov, V. Markus, T. Beutl, A. |
Author_xml | – sequence: 1 givenname: A. surname: Beutl fullname: Beutl, A. email: alexander.beutl@univie.ac.at organization: Institute of Inorganic Chemistry – Functional Materials, University of Vienna – sequence: 2 givenname: D. surname: Henriques fullname: Henriques, D. organization: Institute for Thermo - and Fluiddynamics, Mannheim University of Applied Sciences – sequence: 3 givenname: V. surname: Motalov fullname: Motalov, V. organization: Institute for Energy and Climate Research (IEK, Forschungszentrum Jülich GmbH-2), Research Institute of Thermodynamics and Kinetics, Ivanovo State University of Chemistry and Technology – sequence: 4 givenname: D. surname: Cupid fullname: Cupid, D. organization: Institute for Applied Materials - Applied Materials Physics (IAM-AWP), Karlsruhe Institute of Technology (KIT) – sequence: 5 givenname: T. surname: Markus fullname: Markus, T. organization: Institute for Thermo - and Fluiddynamics, Mannheim University of Applied Sciences – sequence: 6 givenname: H. surname: Flandorfer fullname: Flandorfer, H. organization: Institute of Inorganic Chemistry – Functional Materials, University of Vienna |
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Cites_doi | 10.1016/j.electacta.2016.07.126 10.1002/zaac.19562860302 10.1016/S0966-9795(03)00149-3 10.1016/j.jct.2013.05.018 10.1002/bbpc.19870910707 10.1021/acsami.6b02576 10.1016/j.jallcom.2016.10.230 10.1016/j.jct.2015.01.004 10.1149/1.2131401 10.1351/pac200678071455 10.1002/9783527618347 10.1016/j.jallcom.2016.02.235 10.1016/j.jallcom.2013.09.010 10.1149/2.0671503jes 10.1016/j.jallcom.2016.12.399 10.1016/0364-5916(91)90030-N 10.1107/S0365110X63001262 10.1016/S0040-6031(01)00739-0 10.1515/znb-1965-1017 10.1515/znb-1977-0326 |
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Keywords | Thermodynamics Calorimetry Li–Sb KEMS Cp |
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Snippet | Many standard thermodynamic data in the binary system Li–Sb can be found in literature; however, they are often derived from electrochemical measurements taken... Many standard thermodynamic data in the binary system Li-Sb can be found in literature; however, they are often derived from electrochemical measurements taken... |
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SubjectTerms | Analytical Chemistry Chemistry Chemistry and Materials Science Enthalpy Inorganic Chemistry Knudsen effusion Mass spectrometry Measurement Science and Instrumentation Physical Chemistry Polymer Sciences Thermodynamic properties Thermodynamics |
Title | A thermodynamic investigation of the Li–Sb system |
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