Electrochemical performance of Na2Ti3O7/C negative electrode in ionic liquid electrolyte for sodium secondary batteries

In this study, carbon-coated Na2Ti3O7 (Na2Ti3O7/C) is synthesized by a solid-state reaction method, and its charge-discharge characteristics as a negative electrode material in an ionic liquid electrolyte, Na[FSA]-[C3C1pyrr][FSA] (FSA = bis(fluorosulfonyl)amide; C3C1pyrr = N-methyl-N-propylpyrrolidi...

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Published inJournal of Power Sources Vol. 354; pp. 10 - 15
Main Authors Ding, Changsheng, Nohira, Toshiyuki, Hagiwara, Rika
Format Journal Article
LanguageEnglish
Published Elsevier B.V 30.06.2017
Elsevier BV
Subjects
Charge-discharge characteristics
Ionic liquid electrolyte
Na2Ti3O7/C
Negative electrode
Sodium secondary battery
Sodium secondary battery
Negative electrode
Ionic liquid electrolyte
Na2Ti3O7/C
Charge-discharge characteristics
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Abstract In this study, carbon-coated Na2Ti3O7 (Na2Ti3O7/C) is synthesized by a solid-state reaction method, and its charge-discharge characteristics as a negative electrode material in an ionic liquid electrolyte, Na[FSA]-[C3C1pyrr][FSA] (FSA = bis(fluorosulfonyl)amide; C3C1pyrr = N-methyl-N-propylpyrrolidinium), are investigated at 363 K. The Na2Ti3O7/C negative electrode shows an initial discharge capacity of 215 mAh (g-Na2Ti3O7/C)−1 at a current rate of 20 mA (g-Na2Ti3O7/C)−1 in the voltage range 0.01–2.5 V. The high discharge capacity of the Na2Ti3O7/C negative electrode is attributed to the high operation temperature in the Na[FSA]-[C3C1pyrr][FSA] ionic liquid electrolyte. Although high discharge capacity is achieved, the Na2Ti3O7/C negative electrode shows relatively poor cycle performance because of the irreversible insertion of some Na ions and the formation of cracks. •Na2Ti3O7/C negative electrode was investigated in ionic liquid electrolyte.•The Na2Ti3O7/C electrode showed a high reversible capacity of 215 mAh g−1 at 363 K.•The formation of Na4.8Ti3O7 is suggested in the charged Na2Ti3O7/C electrode.•Some Na irreversible insertion and crack formation result in capacity degradation.
AbstractList In this study, carbon-coated Na2Ti3O7 (Na2Ti3O7/C) is synthesized by a solid-state reaction method, and its charge-discharge characteristics as a negative electrode material in an ionic liquid electrolyte, Na[FSA]-[C3C1pyrr][FSA] (FSA = bis(fluorosulfonyl)amide; C3C1pyrr = N-methyl-N-propylpyrrolidinium), are investigated at 363 K. The Na2Ti3O7/C negative electrode shows an initial discharge capacity of 215 mAh (g-Na2Ti3O7/C)−1 at a current rate of 20 mA (g-Na2Ti3O7/C)−1 in the voltage range 0.01–2.5 V. The high discharge capacity of the Na2Ti3O7/C negative electrode is attributed to the high operation temperature in the Na[FSA]-[C3C1pyrr][FSA] ionic liquid electrolyte. Although high discharge capacity is achieved, the Na2Ti3O7/C negative electrode shows relatively poor cycle performance because of the irreversible insertion of some Na ions and the formation of cracks. •Na2Ti3O7/C negative electrode was investigated in ionic liquid electrolyte.•The Na2Ti3O7/C electrode showed a high reversible capacity of 215 mAh g−1 at 363 K.•The formation of Na4.8Ti3O7 is suggested in the charged Na2Ti3O7/C electrode.•Some Na irreversible insertion and crack formation result in capacity degradation.
Author Ding, Changsheng
Hagiwara, Rika
Nohira, Toshiyuki
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  surname: Ding
  fullname: Ding, Changsheng
  organization: Graduate School of Energy Science, Kyoto University, Sakyo-ku, Kyoto 606-8501, Japan
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  givenname: Toshiyuki
  surname: Nohira
  fullname: Nohira, Toshiyuki
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  givenname: Rika
  surname: Hagiwara
  fullname: Hagiwara, Rika
  email: hagiwara@energy.kyoto-u.ac.jp
  organization: Graduate School of Energy Science, Kyoto University, Sakyo-ku, Kyoto 606-8501, Japan
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Keywords Sodium secondary battery
Negative electrode
Ionic liquid electrolyte
Na2Ti3O7/C
Charge-discharge characteristics
Language English
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Snippet In this study, carbon-coated Na2Ti3O7 (Na2Ti3O7/C) is synthesized by a solid-state reaction method, and its charge-discharge characteristics as a negative...
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SubjectTerms Charge-discharge characteristics
Ionic liquid electrolyte
Na2Ti3O7/C
Negative electrode
Sodium secondary battery
Title Electrochemical performance of Na2Ti3O7/C negative electrode in ionic liquid electrolyte for sodium secondary batteries
URI https://dx.doi.org/10.1016/j.jpowsour.2017.04.027
https://cir.nii.ac.jp/crid/1873398392693864448
Volume 354
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