Uniform patchy and hollow rectangular platelet micelles from crystallizable polymer blends
The preparation of colloidally stable, self-assembled materials with tailorable solid or hollow two-dimensional (2D) structures represents a major challenge. We describe the formation of uniform, monodisperse rectangular platelet micelles of controlled size by means of seeded-growth methods that inv...
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| Published in | Science (American Association for the Advancement of Science) Vol. 352; no. 6286; pp. 697 - 701 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Association for the Advancement of Science
06.05.2016
The American Association for the Advancement of Science |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The preparation of colloidally stable, self-assembled materials with tailorable solid or hollow two-dimensional (2D) structures represents a major challenge. We describe the formation of uniform, monodisperse rectangular platelet micelles of controlled size by means of seeded-growth methods that involve the addition of blends of crystalline-coil block copolymers and the corresponding crystalline homopolymer to cylindrical micelle seeds. Sequential addition of different blends yields solid platelet block comicelles with concentric rectangular patches with distinct coronal chemistries. These complex nano-objects can be subject to spatially selective processing that allows their disassembly to form perforated platelets, such as well-defined hollow rectangular rings. The solid and hollow 2D micelles provide a tunable platform for further functionalization and potential for a variety of applications. |
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| AbstractList | The growth of patterned objects usually requires a template to aid the positioning of multiple materials. Qiu et al. used the seeded growth of a crystallizable block copolymer and a homopolymer to produce highly uniform rectangular structures (see the Perspective by Ballauff). Chemical etching, or dissolution, of uncross-linked regions of the rectangular structures produced perforated platelet micelles. The sequential addition of different blends and cross-linking/dissolution strategies allowed the formation of well-defined hollow rectangular micelles, which can be functionalized in a variety of ways. Science, this issue p. 697; see also p. 656 The preparation of colloidally stable, self-assembled materials with tailorable solid or hollow two-dimensional (2D) structures represents a major challenge. We describe the formation of uniform, monodisperse rectangular platelet micelles of controlled size by means of seeded-growth methods that involve the addition of blends of crystalline-coil block copolymers and the corresponding crystalline homopolymer to cylindrical micelle seeds. Sequential addition of different blends yields solid platelet block comicelles with concentric rectangular patches with distinct coronal chemistries. These complex nano-objects can be subject to spatially selective processing that allows their disassembly to form perforated platelets, such as well-defined hollow rectangular rings. The solid and hollow 2D micelles provide a tunable platform for further functionalization and potential for a variety of applications. The preparation of colloidally stable, self-assembled materials with tailorable solid or hollow two-dimensional (2D) structures represents a major challenge. We describe the formation of uniform, monodisperse rectangular platelet micelles of controlled size by means of seeded-growth methods that involve the addition of blends of crystalline-coil block copolymers and the corresponding crystalline homopolymer to cylindrical micelle seeds. Sequential addition of different blends yields solid platelet block comicelles with concentric rectangular patches with distinct coronal chemistries. These complex nano-objects can be subject to spatially selective processing that allows their disassembly to form perforated platelets, such as well-defined hollow rectangular rings. The solid and hollow 2D micelles provide a tunable platform for further functionalization and potential for a variety of applications. The growth of patterned objects usually requires a template to aid the positioning of multiple materials. Qiu et al. used the seeded growth of a crystallizable block copolymer and a homopolymer to produce highly uniform rectangular structures (see the Perspective by Ballauff). Chemical etching, or dissolution, of uncross-linked regions of the rectangular structures produced perforated platelet micelles. The sequential addition of different blends and cross-linking/dissolution strategies allowed the formation of well-defined hollow rectangular micelles, which can be functionalized in a variety of ways. Science , this issue p. 697 ; see also p. 656 Crystallization-driven living supramolecular polymerization can selectively form rectangular objects. The preparation of colloidally stable, self-assembled materials with tailorable solid or hollow two-dimensional (2D) structures represents a major challenge. We describe the formation of uniform, monodisperse rectangular platelet micelles of controlled size by means of seeded-growth methods that involve the addition of blends of crystalline-coil block copolymers and the corresponding crystalline homopolymer to cylindrical micelle seeds. Sequential addition of different blends yields solid platelet block comicelles with concentric rectangular patches with distinct coronal chemistries. These complex nano-objects can be subject to spatially selective processing that allows their disassembly to form perforated platelets, such as well-defined hollow rectangular rings. The solid and hollow 2D micelles provide a tunable platform for further functionalization and potential for a variety of applications. |
| Author | Qiu, Huibin Boott, Charlotte E. Webb, Stephen E. D. Manners, Ian Miles, Mervyn J. Winnik, Mitchell A. Gould, Oliver E. C. Gao, Yang Harniman, Robert L. |
| Author_xml | – sequence: 1 givenname: Huibin surname: Qiu fullname: Qiu, Huibin – sequence: 2 givenname: Yang surname: Gao fullname: Gao, Yang – sequence: 3 givenname: Charlotte E. surname: Boott fullname: Boott, Charlotte E. – sequence: 4 givenname: Oliver E. C. surname: Gould fullname: Gould, Oliver E. C. – sequence: 5 givenname: Robert L. surname: Harniman fullname: Harniman, Robert L. – sequence: 6 givenname: Mervyn J. surname: Miles fullname: Miles, Mervyn J. – sequence: 7 givenname: Stephen E. D. surname: Webb fullname: Webb, Stephen E. D. – sequence: 8 givenname: Mitchell A. surname: Winnik fullname: Winnik, Mitchell A. – sequence: 9 givenname: Ian surname: Manners fullname: Manners, Ian |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/27151866$$D View this record in MEDLINE/PubMed |
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| ContentType | Journal Article |
| Copyright | Copyright © 2016 American Association for the Advancement of Science Copyright © 2016, American Association for the Advancement of Science. Copyright © 2016, American Association for the Advancement of Science |
| Copyright_xml | – notice: Copyright © 2016 American Association for the Advancement of Science – notice: Copyright © 2016, American Association for the Advancement of Science. – notice: Copyright © 2016, American Association for the Advancement of Science |
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| DOI | 10.1126/science.aad9521 |
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| Snippet | The preparation of colloidally stable, self-assembled materials with tailorable solid or hollow two-dimensional (2D) structures represents a major challenge.... The growth of patterned objects usually requires a template to aid the positioning of multiple materials. Qiu et al. used the seeded growth of a crystallizable... The growth of patterned objects usually requires a template to aid the positioning of multiple materials. Qiu et al. used the seeded growth of a crystallizable... |
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| Title | Uniform patchy and hollow rectangular platelet micelles from crystallizable polymer blends |
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