Non‐Interpenetrated Single‐Crystal Covalent Organic Frameworks
Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open‐structured single‐crystal COFs prevents the exploration of structure‐oriented applications. Herein we report for the first time a non‐interpenetrated single‐crystal COF, LZU‐306, which p...
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| Published in | Angewandte Chemie International Edition Vol. 59; no. 41; pp. 17991 - 17995 |
|---|---|
| Main Authors | , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley Subscription Services, Inc
05.10.2020
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| Edition | International ed. in English |
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| Online Access | Get full text |
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| Abstract | Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open‐structured single‐crystal COFs prevents the exploration of structure‐oriented applications. Herein we report for the first time a non‐interpenetrated single‐crystal COF, LZU‐306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU‐306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation‐induced‐emission moiety. Solid‐state 2H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0×104 Hz at 203 K to 1.5×107 Hz at 293 K. This research not only explores a new paradigm for single‐crystal growth of open frameworks, but also provides a unique matrix‐isolation platform to reticulate functional moieties into a well‐defined and isolated state.
A 3D single‐crystal COF with a non‐interpenetrated structure was constructed for the first time. The highly open framework provides a unique matrix‐isolation platform to investigate the intrinsic dynamics of individual AIE moiety. |
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| AbstractList | Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open‐structured single‐crystal COFs prevents the exploration of structure‐oriented applications. Herein we report for the first time a non‐interpenetrated single‐crystal COF, LZU‐306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU‐306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation‐induced‐emission moiety. Solid‐state
2
H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0×10
4
Hz at 203 K to 1.5×10
7
Hz at 293 K. This research not only explores a new paradigm for single‐crystal growth of open frameworks, but also provides a unique matrix‐isolation platform to reticulate functional moieties into a well‐defined and isolated state. Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open-structured single-crystal COFs prevents the exploration of structure-oriented applications. Herein we report for the first time a non-interpenetrated single-crystal COF, LZU-306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU-306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation-induced-emission moiety. Solid-state 2 H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0×104 Hz at 203 K to 1.5×107 Hz at 293 K. This research not only explores a new paradigm for single-crystal growth of open frameworks, but also provides a unique matrix-isolation platform to reticulate functional moieties into a well-defined and isolated state.Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open-structured single-crystal COFs prevents the exploration of structure-oriented applications. Herein we report for the first time a non-interpenetrated single-crystal COF, LZU-306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU-306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation-induced-emission moiety. Solid-state 2 H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0×104 Hz at 203 K to 1.5×107 Hz at 293 K. This research not only explores a new paradigm for single-crystal growth of open frameworks, but also provides a unique matrix-isolation platform to reticulate functional moieties into a well-defined and isolated state. Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open-structured single-crystal COFs prevents the exploration of structure-oriented applications. Herein we report for the first time a non-interpenetrated single-crystal COF, LZU-306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU-306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation-induced-emission moiety. Solid-state(2)H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0x10(4) Hz at 203 K to 1.5x10(7) Hz at 293 K. This research not only explores a new paradigm for single-crystal growth of open frameworks, but also provides a unique matrix-isolation platform to reticulate functional moieties into a well-defined and isolated state. Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open‐structured single‐crystal COFs prevents the exploration of structure‐oriented applications. Herein we report for the first time a non‐interpenetrated single‐crystal COF, LZU‐306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU‐306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation‐induced‐emission moiety. Solid‐state 2H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0×104 Hz at 203 K to 1.5×107 Hz at 293 K. This research not only explores a new paradigm for single‐crystal growth of open frameworks, but also provides a unique matrix‐isolation platform to reticulate functional moieties into a well‐defined and isolated state. A 3D single‐crystal COF with a non‐interpenetrated structure was constructed for the first time. The highly open framework provides a unique matrix‐isolation platform to investigate the intrinsic dynamics of individual AIE moiety. Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open‐structured single‐crystal COFs prevents the exploration of structure‐oriented applications. Herein we report for the first time a non‐interpenetrated single‐crystal COF, LZU‐306, which possesses the open structure constructed exclusively via covalent assembly. With a high void volume of 80 %, LZU‐306 was applied to investigate the intrinsic dynamics of reticulated tetraphenylethylene (TPE) as the individual aggregation‐induced‐emission moiety. Solid‐state 2H NMR investigation has determined that the rotation of benzene rings in TPE, being the freest among the reported cases, is as fast as 1.0×104 Hz at 203 K to 1.5×107 Hz at 293 K. This research not only explores a new paradigm for single‐crystal growth of open frameworks, but also provides a unique matrix‐isolation platform to reticulate functional moieties into a well‐defined and isolated state. |
| Author | Wang, Wei Yu, Wei Ma, Tianqiong Qiu, Yi Zhang, Lei Niu, Jing Wang, Wei David Han, Jing Luo, Yi Wang, Zhi‐Peng Ni, Jianwei Sun, Junliang Liang, Lin Yin, Guan‐Lin |
| Author_xml | – sequence: 1 givenname: Lin surname: Liang fullname: Liang, Lin organization: Lanzhou University – sequence: 2 givenname: Yi surname: Qiu fullname: Qiu, Yi organization: Peking University – sequence: 3 givenname: Wei David surname: Wang fullname: Wang, Wei David organization: Lanzhou University – sequence: 4 givenname: Jing surname: Han fullname: Han, Jing organization: Lanzhou University – sequence: 5 givenname: Yi surname: Luo fullname: Luo, Yi organization: Stockholm University – sequence: 6 givenname: Wei surname: Yu fullname: Yu, Wei organization: Lanzhou University – sequence: 7 givenname: Guan‐Lin surname: Yin fullname: Yin, Guan‐Lin organization: Lanzhou University – sequence: 8 givenname: Zhi‐Peng surname: Wang fullname: Wang, Zhi‐Peng organization: Lanzhou University – sequence: 9 givenname: Lei surname: Zhang fullname: Zhang, Lei organization: Peking University – sequence: 10 givenname: Jianwei surname: Ni fullname: Ni, Jianwei organization: Lanzhou University – sequence: 11 givenname: Jing surname: Niu fullname: Niu, Jing organization: Lanzhou University – sequence: 12 givenname: Junliang surname: Sun fullname: Sun, Junliang email: junliang.sun@pku.edu.cn organization: Peking University – sequence: 13 givenname: Tianqiong surname: Ma fullname: Ma, Tianqiong email: tianqiongma@pku.edu.cn organization: Peking University – sequence: 14 givenname: Wei orcidid: 0000-0002-9263-7927 surname: Wang fullname: Wang, Wei email: wang_wei@lzu.edu.cn organization: Lanzhou University |
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| Snippet | Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open‐structured single‐crystal COFs prevents the... Growth of covalent organic frameworks (COFs) as single crystals is extremely challenging. Inaccessibility of open-structured single-crystal COFs prevents the... |
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| SubjectTerms | 3D COFs Benzene Covalence Crystal growth Crystal structure Crystals Emission analysis matrix isolation NMR non-interpenetrated frameworks Nuclear magnetic resonance Single crystals solid-state NMR |
| Title | Non‐Interpenetrated Single‐Crystal Covalent Organic Frameworks |
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