Polymerization shrinkage and shrinkage stress development in ultra-rapid photo-polymerized bulk fill resin composites
To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites. Two ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill cont...
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| Published in | Dental materials Vol. 37; no. 4; pp. 559 - 567 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Elsevier Inc
01.04.2021
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0109-5641 1879-0097 1879-0097 |
| DOI | 10.1016/j.dental.2021.02.012 |
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| Abstract | To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites.
Two ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill contains an addition fragmentation chain transfer (AFCT) agent. The URPBR materials were irradiated using two different 3 s high irradiance protocols (3000 and 3200 mW/cm2 based on Bluephase PowerCure and VALO LCUs, respectively) and one 10 s standard protocol (1200 mW/cm2 based on a Bluephase PowerCure LCU). Bonded disk and Bioman II instruments were used to measure Polymerization shrinkage % and shrinkage stress MPa, respectively, for 60 min at 23 ± 1 °C (n = 5). Maximum shrinkage-rate and maximum shrinkage stress-rate were also calculated for 15 s via numerical differentiation. The data were analyzed via multiple One-way ANOVA and Tukey post-hoc tests (α = 0.05).
PFill groups, regardless of their irradiance protocol, showed significantly lower PS than the comparator, ECeram (p < 0.05). However, PFlow irradiated via different protocols, was comparable to EFlow and ECeram (p > 0.05). PFill consistently produced stress results which were significantly lower than ECeram (p < 0.05) and were comparable for both high irradiance protocols (p > 0.05). PFlow only exhibited significantly higher shrinkage stress when polymerized with the 3 sVALO protocol (p < 0.05).
The maximum shrinkage strain-rate (%/s) was significantly lower in PFill-10s and PFill-3s groups (using PowerCure LCU) compared to ECeram. However, no differences were seen between PFlow and EFlow (p > 0.05). The maximum shrinkage stress-rate of PFill and PFlow was comparable between different irradiation protocols, as well as to their comparator ECeram (p > 0.05).
High irradiation protocols over ultra-short periods led to slightly lower shrinkage strain but slightly higher stress, possibly due to reduced network mobility. The AFCT agent incorporated in PFill composite seemed to reduce shrinkage stress development, even with high irradiance protocols. |
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| AbstractList | To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites.OBJECTIVETo determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites.Two ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill contains an addition fragmentation chain transfer (AFCT) agent. The URPBR materials were irradiated using two different 3 s high irradiance protocols (3000 and 3200 mW/cm2 based on Bluephase PowerCure and VALO LCUs, respectively) and one 10 s standard protocol (1200 mW/cm2 based on a Bluephase PowerCure LCU). Bonded disk and Bioman II instruments were used to measure Polymerization shrinkage % and shrinkage stress MPa, respectively, for 60 min at 23 ± 1 °C (n = 5). Maximum shrinkage-rate and maximum shrinkage stress-rate were also calculated for 15 s via numerical differentiation. The data were analyzed via multiple One-way ANOVA and Tukey post-hoc tests (α = 0.05).METHODSTwo ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill contains an addition fragmentation chain transfer (AFCT) agent. The URPBR materials were irradiated using two different 3 s high irradiance protocols (3000 and 3200 mW/cm2 based on Bluephase PowerCure and VALO LCUs, respectively) and one 10 s standard protocol (1200 mW/cm2 based on a Bluephase PowerCure LCU). Bonded disk and Bioman II instruments were used to measure Polymerization shrinkage % and shrinkage stress MPa, respectively, for 60 min at 23 ± 1 °C (n = 5). Maximum shrinkage-rate and maximum shrinkage stress-rate were also calculated for 15 s via numerical differentiation. The data were analyzed via multiple One-way ANOVA and Tukey post-hoc tests (α = 0.05).PFill groups, regardless of their irradiance protocol, showed significantly lower PS than the comparator, ECeram (p < 0.05). However, PFlow irradiated via different protocols, was comparable to EFlow and ECeram (p > 0.05). PFill consistently produced stress results which were significantly lower than ECeram (p < 0.05) and were comparable for both high irradiance protocols (p > 0.05). PFlow only exhibited significantly higher shrinkage stress when polymerized with the 3 sVALO protocol (p < 0.05). The maximum shrinkage strain-rate (%/s) was significantly lower in PFill-10s and PFill-3s groups (using PowerCure LCU) compared to ECeram. However, no differences were seen between PFlow and EFlow (p > 0.05). The maximum shrinkage stress-rate of PFill and PFlow was comparable between different irradiation protocols, as well as to their comparator ECeram (p > 0.05).RESULTSPFill groups, regardless of their irradiance protocol, showed significantly lower PS than the comparator, ECeram (p < 0.05). However, PFlow irradiated via different protocols, was comparable to EFlow and ECeram (p > 0.05). PFill consistently produced stress results which were significantly lower than ECeram (p < 0.05) and were comparable for both high irradiance protocols (p > 0.05). PFlow only exhibited significantly higher shrinkage stress when polymerized with the 3 sVALO protocol (p < 0.05). The maximum shrinkage strain-rate (%/s) was significantly lower in PFill-10s and PFill-3s groups (using PowerCure LCU) compared to ECeram. However, no differences were seen between PFlow and EFlow (p > 0.05). The maximum shrinkage stress-rate of PFill and PFlow was comparable between different irradiation protocols, as well as to their comparator ECeram (p > 0.05).High irradiation protocols over ultra-short periods led to slightly lower shrinkage strain but slightly higher stress, possibly due to reduced network mobility. The AFCT agent incorporated in PFill composite seemed to reduce shrinkage stress development, even with high irradiance protocols.SIGNIFICANCEHigh irradiation protocols over ultra-short periods led to slightly lower shrinkage strain but slightly higher stress, possibly due to reduced network mobility. The AFCT agent incorporated in PFill composite seemed to reduce shrinkage stress development, even with high irradiance protocols. To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites. Two ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill contains an addition fragmentation chain transfer (AFCT) agent. The URPBR materials were irradiated using two different 3 s high irradiance protocols (3000 and 3200 mW/cm2 based on Bluephase PowerCure and VALO LCUs, respectively) and one 10 s standard protocol (1200 mW/cm2 based on a Bluephase PowerCure LCU). Bonded disk and Bioman II instruments were used to measure Polymerization shrinkage % and shrinkage stress MPa, respectively, for 60 min at 23 ± 1 °C (n = 5). Maximum shrinkage-rate and maximum shrinkage stress-rate were also calculated for 15 s via numerical differentiation. The data were analyzed via multiple One-way ANOVA and Tukey post-hoc tests (α = 0.05). PFill groups, regardless of their irradiance protocol, showed significantly lower PS than the comparator, ECeram (p < 0.05). However, PFlow irradiated via different protocols, was comparable to EFlow and ECeram (p > 0.05). PFill consistently produced stress results which were significantly lower than ECeram (p < 0.05) and were comparable for both high irradiance protocols (p > 0.05). PFlow only exhibited significantly higher shrinkage stress when polymerized with the 3 sVALO protocol (p < 0.05). The maximum shrinkage strain-rate (%/s) was significantly lower in PFill-10s and PFill-3s groups (using PowerCure LCU) compared to ECeram. However, no differences were seen between PFlow and EFlow (p > 0.05). The maximum shrinkage stress-rate of PFill and PFlow was comparable between different irradiation protocols, as well as to their comparator ECeram (p > 0.05). High irradiation protocols over ultra-short periods led to slightly lower shrinkage strain but slightly higher stress, possibly due to reduced network mobility. The AFCT agent incorporated in PFill composite seemed to reduce shrinkage stress development, even with high irradiance protocols. Objective To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites. Methods Two ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill contains an addition fragmentation chain transfer (AFCT) agent. The URPBR materials were irradiated using two different 3 s high irradiance protocols (3000 and 3200 mW/cm2 based on Bluephase PowerCure and VALO LCUs, respectively) and one 10 s standard protocol (1200 mW/cm2 based on a Bluephase PowerCure LCU). Bonded disk and Bioman II instruments were used to measure Polymerization shrinkage % and shrinkage stress MPa, respectively, for 60 min at 23 ± 1 °C (n = 5). Maximum shrinkage-rate and maximum shrinkage stress-rate were also calculated for 15 s via numerical differentiation. The data were analyzed via multiple One-way ANOVA and Tukey post-hoc tests (α = 0.05). Results PFill groups, regardless of their irradiance protocol, showed significantly lower PS than the comparator, ECeram (p < 0.05). However, PFlow irradiated via different protocols, was comparable to EFlow and ECeram (p > 0.05). PFill consistently produced stress results which were significantly lower than ECeram (p < 0.05) and were comparable for both high irradiance protocols (p > 0.05). PFlow only exhibited significantly higher shrinkage stress when polymerized with the 3 sVALO protocol (p < 0.05). The maximum shrinkage strain-rate (%/s) was significantly lower in PFill-10s and PFill-3s groups (using PowerCure LCU) compared to ECeram. However, no differences were seen between PFlow and EFlow (p > 0.05). The maximum shrinkage stress-rate of PFill and PFlow was comparable between different irradiation protocols, as well as to their comparator ECeram (p > 0.05). Significance High irradiation protocols over ultra-short periods led to slightly lower shrinkage strain but slightly higher stress, possibly due to reduced network mobility. The AFCT agent incorporated in PFill composite seemed to reduce shrinkage stress development, even with high irradiance protocols. To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites. Two ultra-rapid photo-polymerized bulk fill (URPBF) materials: PFill and PFlow were studied, along with their comparators ECeram and EFlow. PFill contains an addition fragmentation chain transfer (AFCT) agent. The URPBR materials were irradiated using two different 3 s high irradiance protocols (3000 and 3200 mW/cm based on Bluephase PowerCure and VALO LCUs, respectively) and one 10 s standard protocol (1200 mW/cm based on a Bluephase PowerCure LCU). Bonded disk and Bioman II instruments were used to measure Polymerization shrinkage % and shrinkage stress MPa, respectively, for 60 min at 23 ± 1 °C (n = 5). Maximum shrinkage-rate and maximum shrinkage stress-rate were also calculated for 15 s via numerical differentiation. The data were analyzed via multiple One-way ANOVA and Tukey post-hoc tests (α = 0.05). PFill groups, regardless of their irradiance protocol, showed significantly lower PS than the comparator, ECeram (p < 0.05). However, PFlow irradiated via different protocols, was comparable to EFlow and ECeram (p > 0.05). PFill consistently produced stress results which were significantly lower than ECeram (p < 0.05) and were comparable for both high irradiance protocols (p > 0.05). PFlow only exhibited significantly higher shrinkage stress when polymerized with the 3 sVALO protocol (p < 0.05). The maximum shrinkage strain-rate (%/s) was significantly lower in PFill-10s and PFill-3s groups (using PowerCure LCU) compared to ECeram. However, no differences were seen between PFlow and EFlow (p > 0.05). The maximum shrinkage stress-rate of PFill and PFlow was comparable between different irradiation protocols, as well as to their comparator ECeram (p > 0.05). High irradiation protocols over ultra-short periods led to slightly lower shrinkage strain but slightly higher stress, possibly due to reduced network mobility. The AFCT agent incorporated in PFill composite seemed to reduce shrinkage stress development, even with high irradiance protocols. |
| Author | Algamaiah, Hamad Silikas, Nikolaos Watts, David C. |
| Author_xml | – sequence: 1 givenname: Hamad surname: Algamaiah fullname: Algamaiah, Hamad email: dr.algamaiah@gmail.com organization: Biomaterials Science, Division of Dentistry, School of Medical Sciences, University of Manchester, UK – sequence: 2 givenname: Nikolaos surname: Silikas fullname: Silikas, Nikolaos organization: Biomaterials Science, Division of Dentistry, School of Medical Sciences, University of Manchester, UK – sequence: 3 givenname: David C. orcidid: 0000-0002-9105-2775 surname: Watts fullname: Watts, David C. email: David.watts@manchester.ac.uk organization: Biomaterials Science, Division of Dentistry, School of Medical Sciences, University of Manchester, UK |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/33685651$$D View this record in MEDLINE/PubMed |
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| Copyright | 2021 The Academy of Dental Materials Copyright © 2021 The Academy of Dental Materials. Published by Elsevier Inc. All rights reserved. Copyright Elsevier BV Apr 2021 |
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| Keywords | URPBF Bioman II Photopolymerization Polymerization AFCT Resin composite Bulk fill Shrinkage Stress |
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| Snippet | To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites.
Two... Objective To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin composites.... To determine the polymerization shrinkage (%) and shrinkage stress (MPa) characteristics of ultra-rapid photo-polymerized bulk fill resin... |
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| StartPage | 559 |
| SubjectTerms | AFCT Bioman II Bulk fill Bulk polymerization Chain transfer Comparators Composite materials Composite Resins Dental Materials Irradiance Irradiation Materials Testing Numerical differentiation Photopolymerization Polymerization Protocol Reagents Resin composite Resins Shrinkage Strain rate Stress URPBF Variance analysis |
| Title | Polymerization shrinkage and shrinkage stress development in ultra-rapid photo-polymerized bulk fill resin composites |
| URI | https://www.clinicalkey.com/#!/content/1-s2.0-S0109564121000749 https://dx.doi.org/10.1016/j.dental.2021.02.012 https://www.ncbi.nlm.nih.gov/pubmed/33685651 https://www.proquest.com/docview/2515754252 https://www.proquest.com/docview/2499386410 |
| Volume | 37 |
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