NMR Spectra of Triterpenoids. II. Hopenes and Migrated Hopenes
The 1H- and 13C-NMR signals of eleven triterpenoid hydrocarbons belonging to the hopene and migrated hopene groups were completely assigned by the application of modern NMR techniques, and the conformations are discussed on the basis of Chem3D Plus and MM2 calculations, and nuclear Overhauser effect...
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| Published in | Chem. Pharm. Bull Vol. 42; no. 1; pp. 39 - 44 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Tokyo
The Pharmaceutical Society of Japan
1994
公益社団法人日本薬学会 Maruzen Japan Science and Technology Agency |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0009-2363 1347-5223 |
| DOI | 10.1248/cpb.42.39 |
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| Abstract | The 1H- and 13C-NMR signals of eleven triterpenoid hydrocarbons belonging to the hopene and migrated hopene groups were completely assigned by the application of modern NMR techniques, and the conformations are discussed on the basis of Chem3D Plus and MM2 calculations, and nuclear Overhauser effect spectroscopy spectra. |
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| AbstractList | The 1H- and 13C-NMR signals of eleven triterpenoid hydrocarbons belonging to the hopene and migrated hopene groups were completely assigned by the application of modern NMR techniques, and the conformations are discussed on the basis of Chem3D Plus and MM2 calculations, and nuclear Overhauser effect spectroscopy spectra. The ^1H- and ^ C-NMR signals of eleven triterpenoid hydrocarbons belonging to the hopene and migrated hopene groups were completely assigned by the application of modern NMR techniques, and the conformations are discussed on the basis of Chem3D Plus and MM2 calculations, and nuclear Overhauser effect spectroscopy spectra. |
| Author | ARAI, Yoko AGETA, Hiroyuki SUZUKI, Hideki SHIOJIMA, Kenji KIYOTANI, Tamiko |
| Author_FL | SUZUKI Hideki AGETA H ARAI Yoko SHIOJIMA Kenji KIYOTANI Tamiko |
| Author_FL_xml | – sequence: 1 fullname: AGETA H – sequence: 2 fullname: SHIOJIMA Kenji – sequence: 3 fullname: ARAI Yoko – sequence: 4 fullname: SUZUKI Hideki – sequence: 5 fullname: KIYOTANI Tamiko |
| Author_xml | – sequence: 1 fullname: ARAI, Yoko – sequence: 1 fullname: SUZUKI, Hideki – sequence: 1 fullname: AGETA, Hiroyuki – sequence: 1 fullname: SHIOJIMA, Kenji – sequence: 1 fullname: KIYOTANI, Tamiko |
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| Copyright | The Pharmaceutical Society of Japan 1994 INIST-CNRS Copyright Japan Science and Technology Agency 1994 |
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| Keywords | Terpenoid Overhauser effect Force field method Plant origin Triterpene Theoretical study NMR spectrometry Structural analysis |
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| References | 13) K. Shiojima, Y. Sasaki, H. Ageta, Chem. Pharm. Bull., 41, 268 (1993). 3) K. Shiojima, H. Ageta, Chem. Pharm. Bull., 38, 347 (1990). 16) K. Shiojima, Y. Arai, T. Kasama, H. Ageta, Chem. Pharm. Bull., 41, 262 (1993). 1) H. Ageta, K. Shojima, H. Suzuki, S. Nakamura, Chem. Pharm. Bull., 41, 1939 (1993). 2) H. Ageta, Y, Arai, Phytochemistry, 22, 1801 (1983). 11) H. Ageta, K. Shiojima, Y. Arai, T. Kasama, K. Kajii, Tetrahedron Lett., 1975, 3297. 5) K. Shiojima, K. Masuda, H. Ageta, Chem. Pharm. Bull., 38, 79 (1990). 12) A.L. Wilkins, P.W. Bird, P.M. Jager, Magn. Reson. Chem., 25, 503 (1987). 6) H. Ageta, K. Iwata, S. Natori, Tetrahedron Lett., 1963, 1447. 7) H. Ageta, K. Iwata, S. Natori, Tetrahedron Lett., 1964, 3413. 8) R. Kamaya, T. Mori, K. Shoji, H. Ageta, H.-C. Chang, H.-Y. Hsu, Yakugaku Zasshi, 111, 120 (1991). 10) H. Ageta, K. Shiojima, Y. Arai, Chem. Pharm. Bull., 35, 2705 (1987). 14) H. Ageta, Y. Arai, Shoyakugaku Zasshi, 38, 46 (1984). 15) Y. Arai, K. Masuda, H. Ageta, Shoyakugaku Zasshi, 38, 53 (1984). 4) H. Ageta, K. Shiojima, Y. Arai, Chem. Commun., 1968, 1105. |
| References_xml | – reference: 6) H. Ageta, K. Iwata, S. Natori, Tetrahedron Lett., 1963, 1447. – reference: 7) H. Ageta, K. Iwata, S. Natori, Tetrahedron Lett., 1964, 3413. – reference: 5) K. Shiojima, K. Masuda, H. Ageta, Chem. Pharm. Bull., 38, 79 (1990). – reference: 3) K. Shiojima, H. Ageta, Chem. Pharm. Bull., 38, 347 (1990). – reference: 12) A.L. Wilkins, P.W. Bird, P.M. Jager, Magn. Reson. Chem., 25, 503 (1987). – reference: 8) R. Kamaya, T. Mori, K. Shoji, H. Ageta, H.-C. Chang, H.-Y. Hsu, Yakugaku Zasshi, 111, 120 (1991). – reference: 13) K. Shiojima, Y. Sasaki, H. Ageta, Chem. Pharm. Bull., 41, 268 (1993). – reference: 1) H. Ageta, K. Shojima, H. Suzuki, S. Nakamura, Chem. Pharm. Bull., 41, 1939 (1993). – reference: 14) H. Ageta, Y. Arai, Shoyakugaku Zasshi, 38, 46 (1984). – reference: 2) H. Ageta, Y, Arai, Phytochemistry, 22, 1801 (1983). – reference: 16) K. Shiojima, Y. Arai, T. Kasama, H. Ageta, Chem. Pharm. Bull., 41, 262 (1993). – reference: 10) H. Ageta, K. Shiojima, Y. Arai, Chem. Pharm. Bull., 35, 2705 (1987). – reference: 11) H. Ageta, K. Shiojima, Y. Arai, T. Kasama, K. Kajii, Tetrahedron Lett., 1975, 3297. – reference: 15) Y. Arai, K. Masuda, H. Ageta, Shoyakugaku Zasshi, 38, 53 (1984). – reference: 4) H. Ageta, K. Shiojima, Y. Arai, Chem. Commun., 1968, 1105. |
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| Snippet | The 1H- and 13C-NMR signals of eleven triterpenoid hydrocarbons belonging to the hopene and migrated hopene groups were completely assigned by the application... The ^1H- and ^ C-NMR signals of eleven triterpenoid hydrocarbons belonging to the hopene and migrated hopene groups were completely assigned by the application... |
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| SubjectTerms | 1H-NMR Biological and medical sciences C-NMR conformation General pharmacology hopene Medical sciences migrated hopene Pharmacognosy. Homeopathy. Health food Pharmacology. Drug treatments triterpenoid |
| Title | NMR Spectra of Triterpenoids. II. Hopenes and Migrated Hopenes |
| URI | https://www.jstage.jst.go.jp/article/cpb1958/42/1/42_1_39/_article/-char/en https://cir.nii.ac.jp/crid/1572543027232534144 https://www.proquest.com/docview/1460265613 |
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